scholarly journals Shear Bond Strength of Self-Adhesive Composite Containing TiO2 and SiO2 Nanoparticles with an Additional Etching Step for Orthodontic Brackets Bonding to Enamel

Folia Medica ◽  
2021 ◽  
Vol 63 (6) ◽  
pp. 865-874
Author(s):  
Soheil Nikpour ◽  
Atefe Saffar Shahroudi ◽  
Aida Saffarpour ◽  
Azam Akhavan ◽  
Ahmad Sodagar

Introduction: Recently, nanoparticles such as nano-TiO2 have been added to some dental materials for enhancing dental carries prevention due to their antibacterial activity. Aim: This study aimed to assess the shear bond strength of a self-adhesive composite containing TiO2 and SiO2 nanoparticles for orthodontic bracket bonding. Materials and methods: This in vitro, experimental study was done on 70 extracted human premolars divided into 7 groups. Six groups of Vertise Flow self-adhesive composite samples were prepared: without any nanoparticles, with 0.5% and 1% TiO2 nanoparticles, 0.5% and 1% SiO2 nanoparticles, and 1% mixture of TiO2 and SiO2 nanoparticles so that nano-hybrid composites were prepared. Metal brackets were bonded with these samples as well as Transbond XT as the control group. The shear bond strength of the brackets to enamel was measured using a universal testing machine. The adhesive remnant index (ARI) score was also determined by a stereomicroscope. Data were analyzed by one-way ANOVA, Tukey&rsquo;s test and Kruskal-Wallis test. Results: The shear bond strength of the groups was significantly different (p=0.000). Pairwise comparisons revealed that the bond strength of Transbond XT group was significantly higher than others (p<0.05), followed by the 1% TiO2 group with significant differences with Vertise Flow and 0.5% TiO2 groups. The lowest value belonged to Vertise Flow with no nanoparticles. The ARI scores was different in the control group (p=0.000). Conclusions: Adding TiO2 and SiO2 nanoparticles to Vertise Flow self-adhesive composite not only did not adversely affect its shear bond strength, but also slightly increased it. Overall, the self-adhesive nano-hybrid composite containing TiO2 and/or SiO2 nanoparticles, following an additional etching step would be acceptable for bracket bonding and can be used clinically to benefit from the antimicrobial activity of these nanoparticles.

2016 ◽  
Vol 2016 ◽  
pp. 1-10 ◽  
Author(s):  
Andreas Hellak ◽  
Jennifer Ebeling ◽  
Michael Schauseil ◽  
Steffen Stein ◽  
Matthias Roggendorf ◽  
...  

Objective.The aim of this in vitro study was to determine the shear bond strength (SBS) and adhesive remnant index (ARI) score of two self-etching no-mix adhesives (iBond™and Scotchbond™) on different prosthetic surfaces and enamel, in comparison with the commonly used total etch system Transbond XT™.Materials and Methods. A total of 270 surfaces (1 enamel and 8 restorative surfaces,n=30) were randomly divided into three adhesive groups. In group 1 (control) brackets were bonded with Transbond XT primer. In the experimental groups iBond adhesive (group 2) and Scotchbond Universal adhesive (group 3) were used. The SBS was measured using a Zwicki 1120™testing machine. The ARI and SBS were compared statistically using the Kruskal–Wallis test (P≤0.05).Results. Significant differences in SBS and ARI were found between the control group and experimental groups.Conclusions. Transbond XT showed the highest SBS on human enamel. Scotchbond Universal on average provides the best bonding on all other types of surface (metal, composite, and porcelain), with no need for additional primers. It might therefore be helpful for simplifying bonding in orthodontic procedures on restorative materials in patients. If metal brackets have to be bonded to a metal surface, the use of a dual-curing resin is recommended.


2021 ◽  
Author(s):  
Ladan Ranjbar Omrani ◽  
Saba Tohidkhah ◽  
Elham Ahmadi ◽  
Mahdi Abbasi ◽  
Reza Morvaridi Farimani

Abstract Background: The aim of the current study was to evaluate and compare the influence of Dycal, Lime-lite, Theracal LC, Biodentine, Resin-modified glass ionomer cement (RMGIC), and Activa Bioactive as the pulp capping material on the shear bond strength of resin composite to dentin.Methods: A total of 70 extracted caries-free molars were randomly assigned to seven groups. Six test groups were covered with various protective liners: Dycal (GD), Theracal LC (GT), lime-lite (GL), Activa Bioactive (GA), Biodentine (GB), RMGIC (GR). The control group (GC)received no liner pretreatment. Each sample was bonded to resin composite using the total-etch tetric N bond adhesive. The samples were then tested for shear bond strength using the universal testing machine at a cross-head speed of 1 mm/min until bond failure occurred. The data were analyzed using the one-way ANOVA test followed by the Tamhane post-hoc test for pairwise comparisons of the groupsResults: Independent of the type of the applied liner, all groups exhibited inferior SBS to dentine compared to the control group. GT and GR showed significantly higher shear bond strength than GB and GD, which showed the lowest shear bond strength. GL and GA also had significantly lower SBS results than GT. The mode of fracture was predominantly cohesive in GD, GB, and GT and adhesive in GA.Conclusion: This present study concludes that the bond strength of resin-composite to dentine can be affected differently using various types of liners.


2014 ◽  
Vol 1025-1026 ◽  
pp. 385-390
Author(s):  
Niwat Anuwongnukroh ◽  
Surachai Dechkunakorn ◽  
Jirawat Arunakol ◽  
Wassana Wichai

One of the problems that often occurred during orthodontic treatment is bracket failure. This is usually the result either of the patient’s accidentally, applying inappropriate forces to the bracket or of a poor bonding technique. Thus, a significant number of teeth have to be rebonded in an orthodontic practice. Objective: The aim of this study was to evaluate the in vitro initial repeated shear bond strength of the three adhesive systems at two and five minutes after placement of a bracket. Materials and Methods: The three bonding agent adhesives are System1+, Rely-a-bond, Unite. Two hundred and forty human premolar teeth were divided into two groups, a control and an experimental group. Each group was further divided into three subgroups for bonding brackets with the three different adhesives. Only the teeth in the experimental group were sequentially bonded and debonded two times with the same adhesive. The teeth in control and experimental groups were tested for shear bond strength (at two and five minutes after the bracket was bonded) with an Instron testing machine. Results: The studies were found that : (1) there were differences between the shear bond strength of each adhesive in the control and experimental group. Unite had the highest shear bond strength followed by Rely-a-bond and System1+ at two minutes and five minutes, (2) the experiment group ( rebonded brackets) had higher shear bond strength than control group and Unite had in significant difference (p<0.05) of initial repeated bond strength with System1+ and Rely-a-bond at two minutes and five minutes and (3) there were mostly significant difference (p<0.05) between repeated shear bond strength at two minutes and repeated shear bond strength at five minutes. Conclusion: There were significant difference of the initial repeated shear bond strength of each adhesive. The orthodontists should be aware of applying force for tooth movement into the repeated bonding brackets.


Author(s):  
Zahra Khamverdi ◽  
Naemeh Karimian ◽  
Maryam Farhadian ◽  
Hamed Gheitouli

Objectives: Bond strength of composite restorations plays an important role in their success. This in vitro study evaluated the effect of a hemostatic agent on shear bond strength of universal adhesives. Materials and Methods: Thirty-six extracted human molars were used in this study. Buccal and lingual surfaces were reduced to obtain flat dentin surfaces and were ground with a silicone paper. The samples were randomly divided into three groups (n=12) based on the application of hemostatic agent: group 1: no contamination (control), group 2: aluminum chloride application, and group 3: ferric sulfate application. Each group was then divided into two subgroups (n=6) for using G-Premio and Single Bond Universal. Resin cylinders (Filtek Z550) were bonded to dentin surfaces according to the manufacturer’s instructions. After 1000 thermal cycles, shear load was applied to the specimens using a universal testing machine at a crosshead speed of 1 mm/min until failure. Data were statistically analyzed using two-way ANOVA and Tukey’s post-hoc test (α=0.05). Results: There were statistically significant differences in shear bond strength of the three main groups for both G-Premio and Single Bond Universal (P<0.05). When the adhesive systems were compared with each other, G-Premio showed higher shear bond strength than Single Bond Universal (P<0.05). Conclusion: Contamination with hemostatic agents had an adverse effect on the shear bond strength of universal adhesives. Moreover, G-Premio yielded a higher bond strength than Single Bond Universal.


2012 ◽  
Vol 3 (1) ◽  
pp. 41-49
Author(s):  
BM Shivalinga ◽  
H Jyothikiran ◽  
Amit Goyal

ABSTRACT Aims To determine the effect of self-etchant pH on shear bond strength of orthodontic brackets; to compare the shear bond strengths of brackets bonded with three SEPs and brackets bonded with conventional etch, rinse, bond method and to find the brackets/adhesive failure mode. Materials and methods One hundred and twenty premolar teeth were cleaned, mounted, and randomly divided into four groups of 30 samples each- Transbond XT conventional etch and bond system (control), Adper SE Plus SEP (3M ESPE) with a pH of 0.9 to 1.0, Transbond Plus SEP (3M Unitek) with a pH of about 1.0 and Clearfil SE Bond SEP (Kuraray America) with a pH of around 2.0. All teeth were bonded with Transbond XT paste (3M Unitek). The teeth were debonded within half an hour after initial bonding by using a universal testing machine. The residual adhesive on each tooth was evaluated. ANOVA was used to compare the shear bond strength (SBS) of the three groups, and the Chi-square test was used to compare the adhesive remnant index (ARI) scores for the three groups. Results ANOVA indicated significant differences between the groups. Clearfil attained the SBS (6.5 ± 0.6689 MPa) closest to the control group, whereas Adper inspite of being the most aggressive recorded the lowest SBS (5.7 ± 0.5695 MPa). Transbond self-etching primer achieved a mean SBS of 6.1 ± 0.6211 MPa. However, all the three SEPs recorded SBS which was significantly less than that of Transbond conventional etch, rinse and bond system (11.8027 ± 0.8059 MPa). The comparisons of the ARI scores between the three groups indicated that bracket failure mode was significantly different between the three groups (p < 0.05). Conclusion These findings show that factors other than pH, such as the ability of the bonding adhesive to form a chemical bond to enamel and the strength of the bonding adhesive itself, significantly influence the SBS of orthodontic brackets. How to cite this article Goyal A, Jyothikiran H, Shivalinga BM. Effect of Self-etchant pH on Shear Bond Strength of Orthodontic Brackets: An in vitro Study. World J Dent 2012;3(1):41-49.


2021 ◽  
Vol 2021 ◽  
pp. 1-7
Author(s):  
Suliman Y Shahin ◽  
Tahani H. Abu Showmi ◽  
Sadeem H. Alzaghran ◽  
Hoda Albaqawi ◽  
Latifah Alrashoudi ◽  
...  

Background. The number of patients seeking orthodontic treatment has been consistently increasing. During orthodontic treatment, it is recommended to place the provisional restoration and to delay the final restoration until completion of orthodontic treatment. Recurrent bracket debonding necessitates orthodontists to prepare the bonding area with special measures. Objective. This study aimed to evaluate the effect of different grit sizes of diamond burs and sandblasting surface treatment on the shear bond strength of orthodontic brackets to provisional crowns. Materials and Methods. A total of 75 discs were fabricated from a bisacrylic composite and divided into 5 groups (n = 15) according to surface treatment by black, blue, and green diamond burs and sandblasting in addition to a control group. Metal orthodontic brackets were bonded to discs in a standardized conventional manner. All specimens were subjected to thermocycling with 5000 cycles of alternating 5°C and 55°C waterbaths. The shear bond strength test was performed using a universal testing machine. A scanning electron microscope (SEM) was used to analyze the surface treatment effect and features of debonded surfaces. The amount of composite resin left on the specimen surfaces was analyzed and classified with the adhesive remnant index. One-way ANOVA was performed at α = 0.05. Results. The shear bond strength of specimens treated with sandblasting was significantly higher than that of the control group under thermal aging conditions ( p = 0.022 ), as well as blue burs ( p = 0.001 ), while no significant differences were found between different grit diamond burs and the controls ( p > 0.05 ). Conclusion. Under thermocycling conditions, sandblasting of provisional crowns increases the bond strength of orthodontic brackets.


2018 ◽  
Vol 7 (2) ◽  
pp. 28-31
Author(s):  
Varunjeet Chaudhary ◽  
Sanad Singh Solanki ◽  
Varsha Yadav ◽  
Seema Lahoti

Objective: To evaluate the shear bond strength of stainless steel brackets bonded with fluoride-releasing composite resins, comparing effect of adhesion booster and conventional primer.Materials & Method: Sixty extracted premolars were subjected to bracket bonding with fluoride-releasing composite resin; which were bonded by randomly divided into two groups of bonding agents: Group 1- conventional primer as control group, Group 2- adhesion booster. After bonding, the samples were thermocycled (500 cycles) at 5ºC and 55ºC temperatures. After 48 hours they were subjected to shear bond strength testing in occluso-gingival direction, using an MTS 810 Universal Testing Machine with load speed of 0.5 mm/min.Result: Mean shear bond strength was significantly more in samples bonded with adhesion booster (14.792±3.805 Mpa) as compared to conventional primers (11.327±4.047 Mpa). There was statistically significant difference in shear bond strength between the groups (p=0.001).Conclusion: The use of the adhesion booster significantly increased the bond strength of bracket bonded with fluoride-releasing composite.


2017 ◽  
Vol 46 (2) ◽  
pp. 61-65
Author(s):  
Eduardo Otero Amaral VARGAS ◽  
Cinthia Candemil NUERNBERG ◽  
José Vinicius Bolognesi MACIEL ◽  
Ana Maria BOLOGNESE

Abstract Objective The Primekote® (TP) polymer was incorporated to the of Orthodontic Bracket mesh base to improve bond strength and make it more efficient. The purpose of this study was to assess the shear bond strength and adhesive remnant index (ARI) of these brackets. Material and method The test sample consisted of thirty bovine incisors divided into 2 groups: with a group with TP® brackets (n=15), and a control group with Morelli® brackets (n=15) without Primekote® technology. The TransbondTM XT was used as adhesive system in both groups, following the same protocol and manufacturer’s instructions. Specimens were stored in distilled water for 24 hours and then submitted to shear bond strength test in a universal testing machine (EMIC DL2000). The assessment of ARI was performed under stereomicroscope by two calibrated examiners. Result No significant differences (p>0.05) in shear bond strength were found between the two groups according to the independent t-test. The Wilcoxon test was used to assess ARI data and statistical difference was found between Morelli® and TP® Nu-Edge brackets; the last one left less remaining adhesive on tooth surface. Conclusion TP® brackets had higher adherence to the adhesive system as shown by lower ARI scores, but this does not improve its clinical performance.


2021 ◽  
Author(s):  
Saba Tohidkhah ◽  
Elham Ahmadi ◽  
Mahdi Abbasi ◽  
Reza Morvaridi Farimani ◽  
Ladan Ranjbar Omrani

Abstract Background: The aim of current study was to evaluate and compare the influence of Dycal, Lime-lite, Theracal LC, Biodentine, Resin-modified glass ionomer cement (RMGIC), and Activa Bioactive as the pulp capping material on the shear bond strength of resin composite to dentin.Methods: A total of 70 extracted caries-free molars were randomly assigned to seven groups. Six test groups were covered with various protective liners: Dycal (GD), Theracal LC (GT), lime-lite (GL), Activa Bioactive (GA), Biodentine (GB), RMGIC (GR). The control group (GC)received no liner pretreatment. Each sample was bonded to resin composite using the total-etch tetric N bond adhesive. The samples were then tested for shear bond strength using the universal testing machine at a cross-head speed of 1 mm/min until bond failure occurred. The data were analyzed using the one-way ANOVA test followed by the Tamhane post-hoc test for pairwise comparisons of the groupsResults: Independent of the type of the applied liner, all groups exhibited inferior SBS to dentine compared to the control group. GT and GR showed significantly higher shear bond strength than GB and GD, which showed the lowest shear bond strength. GL and GA also had significantly lower SBS results than GT. The mode of fracture was predominantly cohesive in GD, GB, and GT and adhesive in GA.Conclusion: This present study concludes that the bond strength of resin-composite to dentine can be affected differently using various types of liners.


2020 ◽  
Vol 23 (1) ◽  
Author(s):  
Menna Ahmed ElGendy ◽  
Ihab Mosleh ◽  
Hanaa Zaghloul

Objective: the purpose of the study was to evaluate the micro-shear bond strength of different cements to translucent zirconia before and after thermocycling aging. Material and methods: Twelve translucent zirconia ceramic discs were used in the study. Specimens were sandblasted using 50 ‎μm aluminum oxide (Al2O3) particles. The specimens were divided into three groups (n = 4) according to the cement type: Panavia resin cement (control group), resin modified glass ionomer (RMGI), and Activa bioactive cement. Each group was further sub-divided into two equal subgroups (n = 2) according to whether the specimens were subjected to thermocycling or not. Thermocycling was performed in distilled water at 5000 cycles between 5 oC - 55 oC. The micro-shear bond strength test (μSBS) was measured using universal testing machine. Kruskal-Wallis test was used to compare between the three cements. Dunn’s test was used for pair-wise comparisons when Kruskal-Wallis test is significant. Mann-Whitney U test was used to compare between micro-shear bond strength before and after thermocycling P ≤ 0.05. Results: In non-aged subgroups, there was no significant difference between Panavia and Activa; both showed significantly the highest mean μSBS values (22.9 MPa, 31.3 MPa respectively). While, RMGI showed the lowest μSBS values (4.7 MPa).  In thermocycled subgroups, Panavia showed significantly the highest mean μSBS values (32.2 MPa). There was no significant difference between RMGI and Activa; both showed the lowest significant mean μSBS values (3.2 MPa and 8.7 MPa respectively). Conclusions: RMGI and Activa couldn’t be considered long-term reliable materials for cementing zirconia. However, Panavia provided the most durable bond to zirconia.KEYWORDSBioactive cement; Micro-shear bond strength; Resin cement; Translucent zirconia.


Sign in / Sign up

Export Citation Format

Share Document