Microstructure and Texture Evolution during Recrystallization of Interstitial Free Steel

2010 ◽  
Vol 146-147 ◽  
pp. 743-748
Author(s):  
Wei Mao ◽  
Hao Yu ◽  
Wei Hua Sun

The evolution of microstructure and texture due to recrystallization was investigated in cold rolled interstitial free (IF) steel. Samples taken from the cold band of a 0.07%Ti bearing IF steel with total cold rolling reduction of 75% were investigated by using optical microscopy, X-ray diffraction and electron back-scattered diffraction etc. The aim of this study was to obtain a real picture of the formation of the recrystallization texture of IF steel, which would contribute to proper texture control for improving deep drawability. The mechanism responsible for the evolution of texture is discussed experimentally from four aspects. First of all, the microstructure of partially annealed cold rolled specimen is obtained. The recrystallized grain form earlier in more darkly etched regions from the micrographs, which belong to the ND//<111> fiber components. In addition, the fractions of the {111}<110> and {111}<112> components increase slowly during the early stage of recrystallization, because the γ-fiber recrystallized texture is growing, while at the same time the γ-fiber deformed texture is being consumed. Moreover, The texture formation has been discussed taking into consideration of the stored energy and the misorientation between the orientation of the recrystallized grain and that of the surrounding deformed matrix. The work indicates that the recrystallized grains, which migrate into the deformed grains, are mainly with the high misorientation angles. The large percentage of the recrystallized grains, whose misorientation angles with deformed grains exceed 15°, are corresponding to the {111} transformation texture. Nucleation first starts at colonies that have the highest stored energy of deformation, which has the same orientation as the deformed grains. By analysis, the formation of recrystallization texture was well explained by oriented nucleation mechanism rather than by selective growth mechanism.

2014 ◽  
Vol 783-786 ◽  
pp. 1954-1960
Author(s):  
Toshiharu Morimoto ◽  
Y. Fuyuki ◽  
A. Yanagida ◽  
Jun Yanagimoto

T.M.C.P.(Thermo Mechanical Control Processing) has been widely used to improveplastic formability in steel strips. We have produced interstitial free steel(IF steel) strips and ferriticstainless-steel strips through T.M.C.P. rolling method. Optimizing conditions of hot rolling, hotrolled annealing, cold rolling and cold rolled annealing, we developed texture prediction model. Wecan predict rolling texture accurately using the conventional Taylor model. Moreover, we preciselypredict recrystallization texture classifying the total number of microscopic􀀁 slips which arecalculated using the Taylor model. We consider that these calculated results provednucleation-oriented model and two types of recrystallization and grain growth mechanisms exit inour studies. One mechanism is that grains which had the small total number of microscopic slips arepreferred orientation for the hot rolled and annealed ferritic stainless-steel strip. The othermechanism is that grains which had the high total number of microscopic slips are preferredorientation for the cold rolled and annealed IF steel strip.


2010 ◽  
Vol 638-642 ◽  
pp. 2781-2786
Author(s):  
Chang Shu He ◽  
Sadahiro Tsurekawa ◽  
Hiroyuki Kokawa ◽  
Xiang Zhao ◽  
Liang Zuo

An AC magnetic field (0.5Tesla) is applied with the field direction perpendicular to the rolling direction during annealing of a 76% cold-rolled IF steel sheet. Microstructure and texture evolution in the as-annealed specimens were determined using SEM based OIM technique. It is found that the recrystallization is noticeably retarded by AC magnetic field annealing. At the early stage of recrystallization (annealing at 650°C for 30min), the development of (111) <123> orientations was favored by the AC magnetic field. With progress of recrystallization (annealing at 700°C and 750°C for 30min), the applied AC magnetic field suppressed the development of γ-fiber recrystallization textures to some extent.


2005 ◽  
Vol 495-497 ◽  
pp. 417-422
Author(s):  
T. He ◽  
Y.D. Liu ◽  
Yan Wu ◽  
Q.W. Jiang ◽  
Gang Wang ◽  
...  

An experimental setup was designed to study the recrystallization kinetics of Interstitial Free (IF) steel in this work. The 80% cold rolled IF steel foils are heated rapidly to 680°C, 730°C and 780°C by a salt bath. The recrystallization kinetic curves were obtained by the quantitative analysis of texture components, microstructures and EBSP (electron back-scattering patterns) measurements. With the help of EBSD, the orientations of the recrystallization nuclei are determined. The growth rule of the recrystallization nuclei was analyzed statistically. The effect of nucleus orientation on the formation of the recrystallization texture was investigated.


2008 ◽  
Vol 575-578 ◽  
pp. 972-977
Author(s):  
He Tong ◽  
Yan Dong Liu ◽  
Q.W. Jiang ◽  
Y. Ren ◽  
G. Wang ◽  
...  

High-energy synchrotron diffraction offers great potential for experimental study of recrystallization kinetics. A fine experimental design to study the recrystallization mechanism of Interstitial Free (IF) steel was implemented in this work. In-situ annealing process of cold-rolled IF steel with 80% reduction was observed using high-energy X-ray diffraction. Results show that, the diffraction intensity of {001}<110> and {112}<110> belong to α-fiber texture component decreased with the annealing temperature increased while {111}<110> did nearly not change and {111}<112> increased; the FMTH decreasing and d-space changing with annealing temperature increasing indicated that the residual stress relaxed completely during recovery.


2005 ◽  
Vol 495-497 ◽  
pp. 465-470 ◽  
Author(s):  
Chang Shu He ◽  
Yu Dong Zhang ◽  
X. Zhao ◽  
Liang Zuo ◽  
Claude Esling

High magnetic field is applied with the field direction parallel to the rolling direction during annealing of a cold rolled IF steel sheet. Results of X-ray ODF analysis show that, magnetic field annealing retards the normal recrystallization texture evolution for the IF steel sheet. It is worth noting that an abnormal increase of orientation intensity at {100}<110> is found after magnetic annealing for 25min at 650°C. When the magnetic field strength is increased from 10 Tesla to 14 Tesla, the a-fiber is further strengthened, especially the {100}<110> component. Combined with EBSD analysis results, it is considered that the magnetic field does not change the mechanism of recrystallization texture evolution for the IF steel sheet in the present case.


2005 ◽  
Vol 495-497 ◽  
pp. 357-362 ◽  
Author(s):  
Kyoo Young Lee ◽  
Gyo Sung Kim ◽  
Leo Kestens

By applying a double cold rolling and annealing treatment, the evolution of the α and γ fiber components differed from the ones observed in conventional processing. This is attributed to the difference of the initial texture. An increased reduction of stored energy of the {111}<112> component was found by monitoring the change of the stored energy during annealing, indicating that the onset of the nucleation stage of recrystallization by relaxation and annihilation of dislocations occurred mainly on the {111}<112> component with its higher stored energy. The detailed texture evolution of the double cold rolled specimen during 2nd annealing is described by coupling the theory of oriented nucleation and orientation pinning, which is experimentally confirmed by OIM scan.


1994 ◽  
Vol 22 (4) ◽  
pp. 261-278 ◽  
Author(s):  
C. Schuman ◽  
C. Esling ◽  
M. J. Philippe ◽  
M. Hergesheimer ◽  
M. Jallon ◽  
...  

This study deals with the texture evolution during drawing of interstitial-free low carbon steels under different conditions to study the possible influence of the drawing direction, deformation rate and metal/die friction coefficient. The drawing has been carried out without intermediary annealing, with constant die angle and deformation rate per pass. In all cases, a 〈110〉 fibre texture has been observed at the early stage of deformation (a few percents). The drawing direction, whether alternate or unidirectional, has little effect on texture. Slight differences only in the intensity of peaks on pole figures (PFs) are noted. Alternate drawing leads to higher drawing limits. The grain size affects both the texture and the mechanical properties, which are improved by fine grains. For industrial drawing, i.e. at a high deformation rate, no texture gradient has been clearly observed. Nevertheless, slight differences have been noted in the PF intensities, with generally a slightly sharper texture in the core, compared to the surface. The microhardness tests show no hardness gradient. In slow drawing (low deformation rate), there is a weak texture gradient which disappears at larger deformation. In order to visualize the influence of the metal/die friction, we used a material covered with copper. Results show that at a given reduction rate, the material covered with copper shows peak intensities on the (110) PF which are half these of a material drawn under conventional conditions. The drawing textures of BCC materials always present a 〈110〉 fibre texture. A modeling of the texture evolution during drawing has also been carried out using the Taylor model.


Sign in / Sign up

Export Citation Format

Share Document