Effect of Initial Texture on the Evolution of Texture and Stored Energy during Recrystallization of Interstitial Free Steel

2005 ◽  
Vol 495-497 ◽  
pp. 357-362 ◽  
Author(s):  
Kyoo Young Lee ◽  
Gyo Sung Kim ◽  
Leo Kestens

By applying a double cold rolling and annealing treatment, the evolution of the α and γ fiber components differed from the ones observed in conventional processing. This is attributed to the difference of the initial texture. An increased reduction of stored energy of the {111}<112> component was found by monitoring the change of the stored energy during annealing, indicating that the onset of the nucleation stage of recrystallization by relaxation and annihilation of dislocations occurred mainly on the {111}<112> component with its higher stored energy. The detailed texture evolution of the double cold rolled specimen during 2nd annealing is described by coupling the theory of oriented nucleation and orientation pinning, which is experimentally confirmed by OIM scan.

2007 ◽  
Vol 558-559 ◽  
pp. 241-246
Author(s):  
Kyoo Young Lee ◽  
Gyo Sung Kim ◽  
Kwang Geun Chin ◽  
Leo Kestens

The evolution of texture and stored energy was studied for Ti bearing and Ti-Nb bearing IF high strength steel undergoing a double cold rolling and annealing treatment by using Orientation Imaging Microscopy. Ti bearing IF high strength steel showed a similar texture evolution of the α and γ fiber components to that of IF steel. On the contrary, Ti-Nb bearing IF high strength steel displayed a different texture evolution from the one observed in the former steels. The difference in texture and stored energy evolution between both high strength steels seemed to be affected by the segregation behavior of solute alloying elements such as P.


2010 ◽  
Vol 146-147 ◽  
pp. 743-748
Author(s):  
Wei Mao ◽  
Hao Yu ◽  
Wei Hua Sun

The evolution of microstructure and texture due to recrystallization was investigated in cold rolled interstitial free (IF) steel. Samples taken from the cold band of a 0.07%Ti bearing IF steel with total cold rolling reduction of 75% were investigated by using optical microscopy, X-ray diffraction and electron back-scattered diffraction etc. The aim of this study was to obtain a real picture of the formation of the recrystallization texture of IF steel, which would contribute to proper texture control for improving deep drawability. The mechanism responsible for the evolution of texture is discussed experimentally from four aspects. First of all, the microstructure of partially annealed cold rolled specimen is obtained. The recrystallized grain form earlier in more darkly etched regions from the micrographs, which belong to the ND//<111> fiber components. In addition, the fractions of the {111}<110> and {111}<112> components increase slowly during the early stage of recrystallization, because the γ-fiber recrystallized texture is growing, while at the same time the γ-fiber deformed texture is being consumed. Moreover, The texture formation has been discussed taking into consideration of the stored energy and the misorientation between the orientation of the recrystallized grain and that of the surrounding deformed matrix. The work indicates that the recrystallized grains, which migrate into the deformed grains, are mainly with the high misorientation angles. The large percentage of the recrystallized grains, whose misorientation angles with deformed grains exceed 15°, are corresponding to the {111} transformation texture. Nucleation first starts at colonies that have the highest stored energy of deformation, which has the same orientation as the deformed grains. By analysis, the formation of recrystallization texture was well explained by oriented nucleation mechanism rather than by selective growth mechanism.


2013 ◽  
Vol 551 ◽  
pp. 210-216 ◽  
Author(s):  
Alireza Ghaderi ◽  
Peter D. Hodgson ◽  
Matthew R. Barnett

This study focuses on the microstructure and texture evolution of a Ti-5Al-5Mo-5V-3Cr alloy during cold rolling and annealing treatments. Three samples with different initial microstructures were cold rolled to a 40% reduction in thickness. The starting microstructure of one sample was single β phase while two other specimens were α+β phases with different α particle sizes, distributed in β grains. For all three samples, the average size of primary β grains was 150 µm. The cold rolled specimens were then annealed at 860 °C (10 °C above the β transus temperature) for 5 minutes followed by water quenching. Microstructure development during cold rolling and recrystallization was studied by scanning electron microscopy (SEM) and electron backscatter diffraction (EBSD) technique. Microstructure investigations showed that massive amount of shear bands occurred during the cold rolling of the single β phase sample while only a few shear bands were observed in the α+β cold rolled microstructures. The cold rolled texture of the sample comprised of a single β phase contains a gamma fibre (//ND) and a partial alpha fibre (//RD). Annealing treatment decreased the intensity of the cold rolled texture in the single β phase sample. Also, it was found that the presence of α precipitates changes the common annealing texture observed in the single β phase specimen.


2019 ◽  
Vol 28 (4) ◽  
pp. 2228-2236 ◽  
Author(s):  
Siuli Dutta ◽  
V. Rajinikanth ◽  
Ashis K. Panda ◽  
Amitava Mitra ◽  
Subrata Chatterjee ◽  
...  

2010 ◽  
Vol 89-91 ◽  
pp. 244-249 ◽  
Author(s):  
Sujoy S. Hazra ◽  
Azdiar A. Gazder ◽  
Elena V. Pereloma

The evolution of stored energy and associated thermal behaviour was investigated for an ultrafine grained Ti-IF steel severely deformed by Equal Channel Angular Pressing (ECAP) followed by cold rolling at ambient and liquid nitrogen temperatures. Bulk stored energy measurements by Differential Scanning Calorimetry (DSC) returned 350-600 whereas local stored energy estimates from microhardness, Electron Back-Scattering Diffraction (EBSD) and X-ray line profile analysis resulted in 5-140 . Higher bulk stored energy values correspond to the enthalpy release from all sources of strain in the material volume as well as Ti precipitation during annealing while the lower local stored energy range alludes only to dislocation content or internal stresses. An apparent activation energy of 500-550 suggests sluggish recrystallisation due to excess of Ti in solid solution.


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