Compositional Effects on Indentation Mechanical Properties of Chemically Strengthened TiO2-Doped Soda Lime Silicate Glasses

TiO2 is an important oxide for property modifications in the conventional soda lime silicate glass family. It offers interesting optical and mechanical properties, for instance, by substituting heavy metals such as lead in consumer glasses. The compositional effects on the hardness, reduced elastic modulus and crack resistance as determined by indentation of chemically strengthened (CS) TiO2-doped soda lime silicate glass was studied in the current paper. The CS, which was performed by a K+ for Na+ ion exchange in a molten KNO3 salt bath at 450 °C for 15 h, yielded significant changes in the indentation mechanical properties. The hardness of the glass samples increased, and this was notably dependent on the SiO2, CaO and TiO2 content. The reduced elastic modulus was less affected by the CS but showed decrease for most samples. The crack resistance, an important property in many applications where glasses are subjected to contact damage, showed very different behaviors among the series. Only one of the series did significantly improve the crack resistance where low CaO content, high TiO2 content, high molar volume and increased elastic deformation favored an increased crack resistance.

Development and properties of austempered low alloyed white cast iron

This study examined the response of low-alloy white cast iron to austempering heat treatment. In addition, it investigated the microstructure and mechanical properties of austempered low-alloy white cast iron. The low-alloy white cast iron specimens were austenitized at 900 °C, followed by quick quenching into a salt bath at 375 °C, and held there for 15 to 120 minutes for austempering heat treatment. Microstructural features were studied by optical, scanning electron microscopes, and XRD analysis. The mechanical properties were determined by hardness and unnotched Charpy impact toughness tests. As a function of those austempering times, a microstructural map was constructed to show how the transformation products develop, quantitatively. The experimental results showed that the austempering heat treatment produced a microstructure consisting of eutectic carbides + ausferritic structure in low-alloy white cast iron. It can be concluded that the low-alloy white cast iron can be austempered, similar to ductile cast irons. Improved hardness and impact toughness values have been obtained in austempered low-alloy white cast iron.

Strain Hardening and Stretch Formability Behavior of Triple Phase (TP) Steel Strips

The current work explores the strain hardening and stretches formability behaviour of the developed Triple Phase (TP) steel. Double quenched TP steel strips posse three distinguished stages of strain hardening on tensile forming. 1st stage represents the highest n-value reflecting resistance to homogeneous deformation, where steel can be safely stretched. 2nd and 3rd stage reveals lower n-values, where localized thinning exist. On Erichsen testing, the relationship between punch forming force and punch stroke exhibits two forming regions. The 1st region is delineated by a straight line showing an ultra-high strain-hardening rate, which represents a reversible elastic stretch forming. The 2nd forming region continues to a higher Erichsen punch stroke than that of the 1st region and presents the permanent plastic stretch forming behaviour. It is found that bainite and martensite clusters created, by double quenching, in TP-steel exaggerated the elastic stretch forming limit 10 times higher than the as-hot rolled condition. 7 min. holding time of strips in the salt bath is considered the most effective for the creation of a useful volume fraction of the bainite phase. However, 21 min. holding time in salt bath grows martensite laths through the bainite aggregates, affecting negatively on stretch formability.

Effects of Austempering on the Microstructure, Corrosion and Mechanical Properties of AISI 1018 Steel

In this study, the effects of austempering on the microstructure, mechanical properties (micro hardness, impact energy and tensile strength) and corrosion behaviours of AISI 1018 low carbon steel were evaluated. The steel specimens were subjected to heat treatment by austenitizing at 830°C, maintained in this condition for 90 min before rapid cooling in a NaNO3 salt bath sustained at 300°C for isothermal transformation for additional 50 min and finally allowed to air cool to room temperature. The as-received and the austempered samples were tested for corrosion in both 0.5M aqueous acidic (HCl) and 0. 5M alkaline (NaOH) media. Microstructural investigation using scanning electron microscope (SEM) reveals transformation from ferrite/pearlite phases to bainite over the austempering process. Interestingly, significant improvements of 15.7% to 95.7% in the various mechanical properties (micro hardness, impact energy and tensile strength) and corrosion resistance in both media were observed.

Pengaruh Parameter Proses Milling pada Austempered Ductile Iron (ADI) Terhadap Kekasaran Permukaan Benda Kerja dan Chip Thickness Ratio

<p><em>Austempered ductile iron (ADI) is a difficult material for machining, </em><em>even though ADI is believed to have several advantages such as strength, ductility, high toughness, fatigue resistance, good dynamic wear resistance, has a good strength-to-weight ratio, easy to manufacture and easy to cast that causes it to be widely used in various applications. </em><em>This study investigates the effect of milling parameters on surface rougness and chip thickness ratio on milling of ADI. To produce ADI, ductile irons were first austenitized in furnace at 900^oC for 1 hour and then they were quenched in salt bath at 375^oC for 1 hour. The work material was machined with uncoated carbide tool. The tool was 20 mm in diameter. The cutting experiments were carried out in the dry mode. The feed was varied from 0.05 to 0.1 mm/tooth for cutting speed ranging from 15 m/min to 25 mm/min and depth of cut ranging from 0.1 mm to 0.3 mm. The surface roughness was measured using the Mitutoyo SJ-201, surface roughness machine. The chip thickness was measured using software Image J from the photograph produced by digital microscope endoscope. The results show that connected and loose chips were produced. Long and continuous chips were not found in this study. The effects of cutting speeds, feeds and depth of cut on surface roughness and chip thickness ratio are reported in this paper</em><em></em></p>

Carbon deposition mechanism of molten salt cleaning and optimization of multicomponent molten salt formula for remanufacturing

In remanufacturing engineering, cleaning is the key factor for subsequent blank inspection and parts repair. Molten salt has the characteristics of low viscosity, good fluidity, and strong chemical stability. Salt bath cleaning can be comprehensively applied to remove various organic pollutants. Molten salt has the function of self-cleaning. The dirt in the cleaning pool can be decomposed and reused. Moreover, the waste molten salt is massive, and the waste residue is easy to treat. The formation and adsorption mechanism of carbon deposition was explored, and the formation mechanism of carbon deposition was verified by experiments. Then, the existing formula was improved by mixing experiment and compared with the current cleaning method; the cleaning effect was excellent. A new molten salt formula is proposed on the basis of the research on solar thermal storage medium. The composition percentage and the optimal process parameters of the new molten salt formula were determined on the basis of the experimental design of mixture. The cleaning effect of the new formula is good.

Influence of Austempering Temperatures on the Microstructure and Mechanical Properties of Austempered Ductile Cast Iron

The influence of the austempering temperatures on the microstructure and mechanical properties of austempered ductile cast iron (ADI) was investigated. ADI is nodular graphite cast iron, which owing to higher strength and elongation, exceeds mechanical properties of conventional spheroidal graphite cast iron. Such a combination of properties is achieved by the heat treatment through austenitization, followed by austempering at different temperatures. The austenitization conditions were the same for all the samples: temperature 890 °C, duration 30 min, and quenching in a salt bath. The main focus of this research was on the influence of the austempering temperatures (270 °C, 300 °C, and 330 °C) on the microstructure evolution, elongation, toughness, and fatigue resistance of ADI modified by certain amounts of Ni, Cu, and Mo. The Vickers and Rockwell hardness decreased from 535.7 to 405.3 HV/1 (55.7 to 44.5 HRC) as the austempering temperature increased. Optical images showed the formation of graphite nodules and a matrix composed of ausferrite; the presence of these phases was confirmed by an XRD diffraction pattern. A fracture surface analysis revealed several types of the mechanisms: cleavage ductile, transgranular, and ductile dimple fracture. The stress-controlled mechanical fatigue experiments revealed that a 330 °C austempering temperature ensures the highest fatigue life of ADI.

MICROSTRUCTURE, MECHANICAL AND TRIBOLOGICAL BEHAVIOUR OF AISI 316L STAINLESS STEEL DURING SALT BATH NITRIDING

The aim of the current work was to analyse the impact of salt bath nitriding on the behavior of the tribological characteristics and surface microstructures of AISI 316L stainless steels. Nitriding was carried out at 580°C for 10 h. The tribological, structural behavior of the AISI 316L before and after salt bath nitriding was compared. The surface microstructures, tribological characteristics, as well as its surface hardness, were investigated using optical microscopy (OM), X-ray diffractometer (XRD), surface profilometer, pin-on-disk wear tester and microhardness tester. In the current work the experimental results showed that a great surface hardness could be achievable through salt bath nitriding technique because of the formation of the so-called expanded Austenite (S-phase), the nitrogen diffusion region. The surface hardness of AISI 316 stainless steel after nitriding process reached 1100 HV0.025 which was six times the untreated sample hardness. The S-phase is additionally expected to the improvement of wear resistance and decrease the friction coefficient.