recrystallization annealing
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Metals ◽  
2022 ◽  
Vol 12 (1) ◽  
pp. 137
Author(s):  
Kai Feng ◽  
Xiaxu Huang ◽  
Rui Wang ◽  
Wenli Xue ◽  
Yilei Fu ◽  
...  

Revealing the recrystallization behavior and mechanism of this new alloy is of great significance to subsequent research. In this study, the Ni-36.6W-15Co ternary medium heavy alloy was solution-treated at 1100–1200 °C for different lengths of time. The grain size change, microstructure and texture evolution as well as twin development during recrystallization annealing were analyzed using SEM, EBSD and TEM techniques. The study found that complete recrystallization occurs at 1150 °C/60 min. In addition, it takes a longer amount of time for complete recrystallization to occur at 1100 °C. The value of the activation energy Q1 of the studied alloys is 701 kJ/mol and the recrystallization process is relatively slow. By comparing the changes of microstructure and texture with superalloys, it is found that the recrystallization mechanism of the studied alloy is different from that of the superalloy. The development of annealing twins has a great influence on the recrystallization behavior and mechanism. The results show that the twin mechanism is considered as the dominant recrystallization mechanism of the studied alloy, although the formation and development of sub-grains appear in the early stage of recrystallization.


Metals ◽  
2022 ◽  
Vol 12 (1) ◽  
pp. 122
Author(s):  
Maxwell Hein ◽  
David Kokalj ◽  
Nelson Filipe Lopes Dias ◽  
Dominic Stangier ◽  
Hilke Oltmanns ◽  
...  

In biomedical engineering, laser powder bed fusion is an advanced manufacturing technology, which enables, for example, the production of patient-customized implants with complex geometries. Ti-6Al-7Nb shows promising improvements, especially regarding biocompatibility, compared with other titanium alloys. The biocompatible features are investigated employing cytocompatibility and antibacterial examinations on Al2O3-blasted and untreated surfaces. The mechanical properties of additively manufactured Ti-6Al-7Nb are evaluated in as-built and heat-treated conditions. Recrystallization annealing (925 °C for 4 h), β annealing (1050 °C for 2 h), as well as stress relieving (600 °C for 4 h) are applied. For microstructural investigation, scanning and transmission electron microscopy are performed. The different microstructures and the mechanical properties are compared. Mechanical behavior is determined based on quasi-static tensile tests and strain-controlled low cycle fatigue tests with total strain amplitudes εA of 0.35%, 0.5%, and 0.8%. The as-built and stress-relieved conditions meet the mechanical demands for the tensile properties of the international standard ISO 5832-11. Based on the Coffin–Manson–Basquin relation, fatigue strength and ductility coefficients, as well as exponents, are determined to examine fatigue life for the different conditions. The stress-relieved condition exhibits, overall, the best properties regarding monotonic tensile and cyclic fatigue behavior.


Author(s):  
І. Doschechkina

The aim of the work is to develop a method of increasing the technological plasticity while maintaining the strength and preventing aging of blanks of cold-rolled sheet steel 08Yu. The task of this work is research and determination of optimal temperature-time parameters of high-speed contact recrystallization annealing and subsequent aging of 08Yu steel sheet blanks to obtain the required level of mechanical properties that would improve their deformability and ability of very deep drawing during cold stamping of products. The optimal parameters of the speed mode are set recrystallization annealing of cold-rolled 08Yu sheet steel, which provides the best structure and properties for further cold pressure treatment. The temperature-time modes of further aging and possibilities to prevent the processes of its natural aging during prolonged operation or transportation have been studied. The method and modes of heat treatment of blanks from finished 08Yu sheet steel to facilitate their deformability and improve stamping in order to reduce waste in the manufacture of products by cold deformatiion with deep and complex drawing were suggested.


Materials ◽  
2021 ◽  
Vol 14 (21) ◽  
pp. 6559
Author(s):  
Linton Carvajal ◽  
María Sosa ◽  
Alfredo Artigas ◽  
Nelson Luco ◽  
Alberto Monsalve

The evolution of the elastic constants, , and Poisson’s ratio and acoustic birefringence of a Fe-0.5 wt% C-21.5 wt% Mn twinning-induced plasticity (TWIP) steel with reduction by cold rolling and recrystallization annealing was assessed from measurements of the times of flight of ultrasonic waves propagating along the thickness of the rolled plates. As the reduction increased, changes in the elastic constants resulted in a steadily increasing orthotropy, which was clearly shown by Poisson’s ratio and acoustic birefringence. Although optical metallography and hardness measurements showed that partial or full recrystallization is attained after annealing at 600 °C and 700 °C, the ultrasonic measurements revealed that a high level of orthotropy remains.


2021 ◽  
Vol 9 (10) ◽  
pp. 680-689
Author(s):  
Omer Beganovic ◽  
◽  
Belma Fakic ◽  
Branka Muminovic ◽  
◽  
...  

Additional strengthening of superalloy N07080 described in this work was achieved by warm rolling. Control of the ratio of strength and ductile properties of the superalloy is possible by appropriate selection of the amount of warm deformation and the appropriate selection of the partial recrystallization temperature. In addition, recrystallization annealing makes it possible to equalize the grain size across the cross section of the warm rolled bars, which before recrystallization differ significantly in size in the central and peripheral parts of the bars.


2021 ◽  
Vol 9 (09) ◽  
pp. 338-344
Author(s):  
B. Smyrak ◽  
◽  
B. Leszczynska Madej ◽  
P. Jalowy ◽  
M. Nowak ◽  
...  

Modern technological solutions in electrical applications require, above all, high energy efficiency. This means that in such applications, materials with the highest possible electrical conductivity should be used for conductive elements. Of all metals, copper is the natural choice. Copper cables or wires used in electrical networks and installations provide better electrical and thermal conductivity and guarantee reliability - which translates into the quality of electricity. And bad quality of energy means tangible financial losses. On the other hand, apart from physical properties, an important factor is the price of cables and wires, which is partially dependent on the price of copper on the stock exchange. The last 20 years have seen a high increase in copper prices on the markets and at the same time the price is unstable. Therefore, cheaper substitutes for copper are being sought. The natural choice is aluminum, which is currently widely used in overhead power lines. At the same time, in the case of long cables, copper products still dominate. The paper presents a synthetic comparative analysis of technological processing problems in industrial drawing processes of aluminum and copper wires used in electrical applications.. In particular, comparative analysis applied the susceptibility into formability in the wire drawing process and susceptibility to recrystallization annealing of copper and aluminum wires. The drawing process and the annealing process are simple processes for the production of wires used for electrical purposes.


Materials ◽  
2021 ◽  
Vol 14 (18) ◽  
pp. 5365
Author(s):  
Аikol M. Mairambekova ◽  
Anna Y. Eroshenko ◽  
Vladimir A. Oborin ◽  
Mikhail V. Bannikov ◽  
Valentina V. Chebodaeva ◽  
...  

The paper presents the results of fatigue-testing ultrafine-grained and coarse-grained Ti-45 wt.% Nb alloy samples under very high cycle fatigue (gigacycle regime), with the stress ratio R = −1. The ultrafine-grained (UFG) structure in the investigated alloy was formed by the two-stage SPD method, which included multidirectional forging (abc–forging) and multipass rolling in grooved rollers, with further recrystallization annealing. The UFG structure of the Ti-45 wt.% Nb alloy samples increased the fatigue limit under the high-cycle fatigue conditions up to 1.5 times compared with that of the coarse-grained (CG) samples. The infrared thermography method was applied to investigate the evolution of temperature fields in the samples under cyclic loading. Based on numerical morphology analysis, the scale invariance (the Hurst exponent) and qualitative differences for UFG and CG structures were determined. The latter resulted from the initiation and propagation of fatigue cracks in both ultra-fine grained and coarse-grained alloy samples under very high-cycle fatigue loading.


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