Effect of Beeswax on Functional and Structural Properties of Soy Protein Isolate Films

2010 ◽  
Vol 150-151 ◽  
pp. 1396-1399 ◽  
Author(s):  
Xi Hong Li ◽  
Kuan Guo ◽  
Xiao Yan Zhao

This paper explains and demonstrates the effects of beeswax on functional and structural properties of soy protein isolate films, containing different glycerol. The results showed that percentage elongation at break, water vapor permeability, and transparency of soy protein isolate films decreased when the beeswax content increased, but tensile strength and oxygen permeability increased. The higher the glycerol content, the higher the film water vapor permeability, oxygen permeability, and transparency. The results of differential scanning calorimetry and Fourier transform infrared spectroscopy suggested that beeswax cross-linked with soy protein isolate molecules via connecting with glycerol, composed the film matrix.

2021 ◽  
Author(s):  
Aritra Sinha

Abstract This study focuses on the development and characterization of a novel biodegradable edible film made from soy protein isolate enriched with alginate-glycyrrhizin nanogel(GL-ALG NGP). Nanoparticles of particle sizes below 100 nm were synthesized using glycyrrhizin(GL), calcium chloride and, sodium alginate(SA) through the reverse micro-emulsion/internal gelation method. Soy protein isolate (SPI) based films were prepared by a simple casting procedure by incorporating GL-ALG NGPs in SPI solution in different ratios of (SPI: GL-ALG NGPs) 5:0, 5:1, 2:1, 1:1, and 1:1.5. Glycerol was used as a plasticizer in the film-forming solution. The effects of the proportions of GL-ALG NGPs addition on the thickness, mechanical properties, water vapor permeability, UV barrier performance, antioxidant activity, and antimicrobial property of the obtained films were studied. The GL-ALG NGPs were analyzed using Dynamic Light Scattering. Microstructural studies of obtained films were performed using Scanning Electron microscopy. Results show incorporation of GL-ALG NGPs in soy protein-alginate complex produced smoother, compact, and more continuous matrices as compared to pure SPI films. The test results indicated that blending of SPI with GL-ALG NGPs in the ratio 1:1 increased tensile strength of obtained films by 185%, reduced water solubility to 23.59%, and water vapor permeability to 0.3087 g-mm/m2-d-kPa. Obtained films exhibited good UV barrier performance, antioxidant activity and inhibited the growth of E. coli, S. aureus, Enterobacter sakazakii, and A. niger. So, soy protein isolate-based films enriched with GL-ALG NGPs are active biodegradable edible films that can be used to extend the shelf life of food products.


2010 ◽  
Vol 96 ◽  
pp. 75-79 ◽  
Author(s):  
Jun Feng Su ◽  
Wen Long Xia ◽  
Wen Li ◽  
Ke Man Jin

The aim of the present work was to investigate the moisture sensitivity of soy protein isolate (SPI) films blending with poly (vinyl alcohol) (PVA) plasticized by glycerol. Water vapor permeability (WVP) was measured based on the contents of PVA and glycerol in films. WVP values of various SPI/PVA films with/without glycerol were in the range of 8.25 and 10.9 g mm/m2 h kPa. The results showed that WVP values decreased with the increasing content of PVA. Moreover, XRD tests confirmed that the glycerol would insert into the macromolecular blending structure and destroy the crystalline of blends, and the crosslinkage between glycerol molecules and SPI reduced the interstitial spaces in protein matrix, thus allowing for decreasing diffusion rate of water molecules through the films.


1994 ◽  
Vol 2 (3) ◽  
pp. 189-195 ◽  
Author(s):  
Aristippos Gennadios ◽  
Alice H. Brandenburg ◽  
Jang W. Park ◽  
Curtis L. Weller ◽  
Robert F. Testin

2008 ◽  
Vol 14 (2) ◽  
pp. 119-125 ◽  
Author(s):  
A.N. Mauri ◽  
M.C. Añón

Mechanical, physical, and barrier properties of films obtained from soy protein isolate solutions at different pH were studied and correlated with the structural properties and the microstructure of films. Films obtained at pH 2 and 11, which had denser microstructures and a higher amount of disulfide bonds, showed a higher tensile strength — of about 1.05 MPa — and a higher Young's modulus — of at least 0.15MPa — than the one at pH 8. However, films formed at alkaline pH (8 and 11) exhibited a higher deformation than films at pH 2 — by about 70%. The presence of at least a protein fraction in native state allowed macromolecules to unfold during the mechanical test, reaching greater deformation before breaking. Acidic films exhibited higher water vapor permeability — of about 7 × 10-11 g/m s Pa — and water content — of about 1.5% — and a lower glass transition temperature — of at least 15 °C — than basic ones, due to their higher hydrophilic nature.


Author(s):  
Yuanyuan Liu ◽  
Lina Xu ◽  
Rui Li ◽  
Huangjiang Zhang ◽  
Wenhui Cao ◽  
...  

AbstractAntimicrobial films were prepared by incorporating nano-titanium dioxide (TiO2) modified by silane into soy protein isolate (SPI) films. The effects of different concentrations of modified nano-TiO2 (TiO2-NM) on the physical properties, antimicrobial properties, and microstructure of the SPI-based films were investigated. Attenuated total reflectance Fourier-transform infrared spectroscopy indicated that the interaction between the SPI and TiO2-NM was via hydrogen bonds. Scanning electron microscopy and atomic force microscopy both showed that the microstructure of SPI-based films with TiO2-NM was compact. Moreover, as the content of TiO2-NM increased from 0 to 1.5 g/100 mL, the water vapor permeability and oxygen permeability were decreased from 5.43 to 4.62 g· mm/m2d· kPa and 0.470 to 0.110 g· cm−2· d−1, respectively. An increase from 6.67 MPa to 14.56 MPa in tensile strength and a decrease from 36.53% to 27.62% in elongation at break indicate the optimal mechanical properties of all groups. TiO2-NM films had excellent UV barrier properties, with a whiter surface with increasing TiO2-NM content. In addition, the SPI-based films with TiO2-NM showed antimicrobial activity, as evidenced by an inhibitory zone increasing from 0 to 27.34 mm. Therefore, TiO2-NM can be used as an antimicrobial agent in packaging films.


2012 ◽  
Vol 503-504 ◽  
pp. 446-449 ◽  
Author(s):  
Chun Xia Sui ◽  
Lian Zhou Jiang ◽  
Guo Ping Yu

The objective of this research was to investigate the effect of pH(7.0, 8.0, 9.0, 10.0) on the properties of soy protein isolate (SPI)/guar gum (GG)composite films casted with 0.2 %(w/v)guar gum polysaccharide, 5.0 %(w/v)SPI, 1.5 %(w/v)glycerol plasticizer, and 4:1(v/v) mixture of distilled water and anhydrous alcohol. Composite membranes from different pH conditions were evaluated from following aspects: tensile strength (TS), elongation at break (EB), water vapor permeability (WVP), water solubility (WS) and surface hydrophobicity(SH)


Molecules ◽  
2021 ◽  
Vol 26 (12) ◽  
pp. 3738
Author(s):  
Magdalena Mikus ◽  
Sabina Galus ◽  
Agnieszka Ciurzyńska ◽  
Monika Janowicz

The possibility of using oilseed flours as a waste source for film-forming materials with a combination of soy protein isolate in preparation of edible films was evaluated. Physical, mechanical and barrier properties were determined as a function of the oilseed type: hemp, evening primrose, flax, pumpkin, sesame and sunflower. It was observed that the addition of oilseed flours increased the refraction and thus the opacity of the obtained films from 1.27 to 9.57 A mm−1. Depending on the type of flours used, the edible films took on various colors. Lightness (L*) was lowest for the evening primrose film (L* = 34.91) and highest for the soy protein film (L* = 91.84). Parameter a* was lowest for the sunflower film (a* = −5.13) and highest for the flax film (a* = 13.62). Edible films made of pumpkin seed flour had the highest value of the b* color parameter (b* = 34.40), while films made of evening primrose flour had the lowest value (b* = 1.35). All analyzed films had relatively low mechanical resistance, with tensile strength from 0.60 to 3.09 MPa. Films made of flour containing the highest amount of protein, pumpkin and sesame, had the highest water vapor permeability, 2.41 and 2.70 × 10−9 g·m−1 s−1 Pa−1, respectively. All the edible films obtained had high water swelling values from 131.10 to 362.16%, and the microstructure of the films changed after adding the flour, from homogeneous and smooth to rough. All blended soy protein isolate–oilseed flour films showed lower thermal stability which was better observed at the first and second stages of thermogravimetric analysis when degradation occurred at lower temperatures. The oilseed flours blended with soy protein isolate show the possibility of using them in the development of biodegradable films which can find practical application in the food industry.


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