Rapid Fabrication of ZnS Thin Film and Microsphere by Microwave-Assisted Chemical Solution Method

2012 ◽  
Vol 455-456 ◽  
pp. 711-715
Author(s):  
Jian Min Li ◽  
Long Long Zhang ◽  
Ling Yu Li ◽  
Hai Yan Xu

A rapid preparation route, microwave-assisted chemical solution method, has been developed for the fabrication of zinc sulfide (ZnS) thin film and powder with shape of microsphere. The as-obtained products were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), atomic force microscopy (AFM), and optical measurement. XRD results indicated that the structures of as-obtained products are wurtzite. The SEM and AFM photographs show that uniform ZnS microsphere with size of less than 1 μm and homogeneous thin film could be obtained from solution under adequate conditions with thiourea as sulfide source. The results show that microwave-assisted chemical solution method is really a time saving method to fabricate the ZnS thin film and nanostructured microspheres.

2015 ◽  
Vol 830-831 ◽  
pp. 592-594 ◽  
Author(s):  
Shilpa Thakur ◽  
Hakikat Sharma ◽  
Sarita Sharma ◽  
N.S. Negi

Co0.6Zn0.4Fe2O4(CZFO), Pb0.76Ca0.24TiO3(PCT) thin films and Co0.6Zn0.4Fe2O4– Pb0.76Ca0.24TiO3(CZFO/PCT) composite thin film were prepared by chemical solution method using metello – organic precursor. Structural and microstructural properties were studied by using XRD and Atomic force microscopy (AFM) respectively. XRD patterns confirme cubic spinel structure for CZFO ferrite and perovskite structure for PCT ferroelectric phase without any impurity phase formation. Grain size and roughness were calculated from AFM images. Grain size and roughness of composite thin film are decreased in comparison to individual phases (CZFO,PCT). Magnetic properties were studied using VSM.


2012 ◽  
Vol 520 (6) ◽  
pp. 1734-1739 ◽  
Author(s):  
Y. Romaguera-Barcelay ◽  
J. Agostinho Moreira ◽  
A. Almeida ◽  
J. Pérez de la Cruz

2009 ◽  
Vol 24 (6) ◽  
pp. 1201-1204 ◽  
Author(s):  
Yue ZHAO ◽  
Hong-Li SUO ◽  
Jean-Claude GRIVEL ◽  
Shuai YE ◽  
Min LIU ◽  
...  

2017 ◽  
Vol 29 (5) ◽  
pp. 4075-4079
Author(s):  
Wei Wang ◽  
Lingyun Hao ◽  
Wei Zhang ◽  
Qing Lin ◽  
Xiaojuan Zhang ◽  
...  

2011 ◽  
Vol 14 (8) ◽  
pp. H311 ◽  
Author(s):  
J. Y. Son ◽  
D.-Y. Kim ◽  
H. Kim ◽  
W. J. Maeng ◽  
Y.-S. Shin ◽  
...  

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