Microwave Synthesis and Characterization of Europium Complexes with Cinnamic Acid and 2, 2' –Bipyridine

2013 ◽  
Vol 670 ◽  
pp. 106-109 ◽  
Author(s):  
X.J. Wang ◽  
X.C. Zhou
Keyword(s):  
Electron Microscope ◽  
Cinnamic Acid ◽  
Luminescence Spectroscopy ◽  
Synthesis And Characterization ◽  
Material Synthesis ◽  
Europium Complexes ◽  
Novel Material ◽  
Microwave Process ◽  
Scanning Electron

A novel material synthesis technique, microwave process was investigated for the production of phosphor powders. In this study, we have developed a new method to product phosphor powders, and applied this process into one materials fabrication. EuDL3 where L is cinnamic acid (C6H5CH = CHCOOH, HL), D = 2, 2' – Bipyridine (bipy) phosphor powders were successfully synthesized by microwave process. The process takes only 24 min to obtain phosphor powders. The resultant phosphor powders were investigated by TG – DTA, IR, luminescence spectroscopy, and scanning electron microscope (SEM).

Preparation and Characterization of Europium(III) Complexes with Cinnamic Acid by Microwave Process

2010 ◽  
Vol 663-665 ◽  
pp. 922-925
Author(s):  
Man Hua Wan ◽  
Xiao Hong Liu
Keyword(s):  
Electron Microscope ◽  
Scanning Electron Microscope ◽  
Cinnamic Acid ◽  
New Method ◽  
Luminescence Spectroscopy ◽  
Material Synthesis ◽  
Novel Material ◽  
Microwave Process ◽  
Scanning Electron

A novel material synthesis technique, microwave process was investigated for the production of phosphor powders. In this study, we have developed a new method to product phosphor powders, and applied this process into two materials fabrication. EuDL3 where L is cinnamic acid (C6H5CH = CHCOOH, HL), D = 2, 9-dimethyl-1, 10-phenantroline (dmp), or 2, 2'-bipyridine (bipy) phosphor powders were successfully synthesized by microwave process. The process takes only 24 min to obtain two phosphor powders. The process takes only 24 min to obtain two phosphor powders. The resultant phosphor powders were investigated by TG-DTA, IR, luminescence spectroscopy, and scanning electron microscope (SEM). The results revealed that the two materials is significant different, compared to micrographs of scanning electron microscope (SEM).

Synthesis and Characterization of Y2O3 Nanoflowers

2012 ◽  
Vol 465 ◽  
pp. 76-79 ◽  
Author(s):  
Shuang Zhan ◽  
Xia Li
Keyword(s):  
Fourier Transform ◽  
Phase Composition ◽  
Electron Microscope ◽  
Synthesis And Characterization ◽  
The Novel ◽  
X Ray Diffraction ◽  
Facile Hydrothermal Method ◽  
X Ray ◽  
Scanning Electron

The novel Y2O3 nanoflowers were synthesized through a facile hydrothermal method without using any catalyst or template. The phase composition and the microstructure of as-prepared products were characterized by field emission scanning electron microscope (FE-SEM), X-ray diffraction (XRD) as well as Fourier transform infrared spectrum. The formation mechanism for the Y2O3 flowers has been proposed.

Synthesis and Characterization of Nanostructured Materials Prepared from SiO2 and GeO2 Mixture by Carbon Assisted Method

2008 ◽  
Vol 55-57 ◽  
pp. 637-640 ◽  
Author(s):  
Pattanasuk Chamninok ◽  
P. Kasian ◽  
Pichet Limsuwan ◽  
Udom Tipparach ◽  
S. Samran ◽  
...  
Keyword(s):  
Electron Microscope ◽  
Silicon Dioxide ◽  
Nanostructured Materials ◽  
Thermal Evaporation ◽  
Synthesis And Characterization ◽  
Image Analyzer ◽  
Evaporation Process ◽  
Stereo Microscope ◽  
Scanning Electron

Nanostructured materials were synthesized by thermal evaporation process using silicon dioxide and carbon from coconut shell charcoal or graphite mixed with GeO2 by the ratio of 5:1:1 at temperature 1200 oC in one atmosphere of nitrogen for 3 hours. The nanostructured materials were characterized by the stereo microscope (image analyzer) and scanning electron microscope. The diameters of nanowires vary from 10 nm to 50 nm and length of several 10 micrometers. Length of nanorods was around 15 micrometers and diameters vary from 10 nm to 100 nm.

Synthesis and Characterization of CuO/SnO2 Nanocomposites

2014 ◽  
Vol 575 ◽  
pp. 175-179 ◽  
Author(s):  
Supakorn Pukird ◽  
Dheerachai Polsongkram ◽  
Suttinart Noothongkeaw ◽  
Khanidtha Jantasom ◽  
Ki Seok An
Keyword(s):  
Electron Microscope ◽  
Scanning Electron Microscope ◽  
Synthesis And Characterization ◽  
Photoemission Spectroscopy ◽  
Distilled Water ◽  
X Rays ◽  
X Ray ◽  
Coprecipitation Process ◽  
Scanning Electron

CuO/SnO2 nanocomposites materials were prepared by solution coprecipitation process using CuO nanowires-rods and SnO2 nanowires mixture as a starting materials. The mixture materials were put in beaker glass with distilled water and magnetic stering at 90 oC for 3 h. The mixture materials were filtered and heated at 980 oC for 20 h. The prepared products were investigated by FE scanning electron microscope (FESEM), X-rays photoemission spectroscopy (XPS) and X-ray driffraction technique (XRD). The results showed nanocomposites structures which consisting of CuO and SnO2 phase.

Synthesis and Characterization of a Novel Netlike Nano-TiO2 with Polylactic Acid (PLA) as Template

2011 ◽  
Vol 233-235 ◽  
pp. 623-626 ◽  
Author(s):  
Ling Xin ◽  
Bo Liu ◽  
Jiu Hong Ai ◽  
Jian Cheng Deng
Keyword(s):  
Methylene Blue ◽  
Electron Microscope ◽  
Methyl Orange ◽  
Scanning Electron Microscope ◽  
Synthesis And Characterization ◽  
X Ray Diffraction ◽  
X Ray ◽  
Transmission Electron ◽  
Scanning Electron

Novel netlike nano-TiO2 was successfully prepared using polylatic acid (PLA) as a new template, and in particular, it was recyclable as photocatalyst. The products obtained at various temperatures were characterized by scanning electron microscope (SEM), transmission electron microscope (TEM) and powder X-ray diffraction (XRD). Besides, the products have an excellent photocatalysis to methyl orange (MO) and methylene blue (MB).

Synthesis and Characterization of Tungsten Micro-/Nanoparticles Using Tungstate-Based Inorganic-Organic Hybrid Nanobelts as Precursors

2011 ◽  
Vol 266 ◽  
pp. 204-208 ◽  
Author(s):  
De Liang Chen ◽  
He Jing Wen ◽  
Rui Zhang ◽  
Xin Jian Li
Keyword(s):  
Electron Microscope ◽  
Scanning Electron Microscope ◽  
Lamellar Structure ◽  
Synthesis And Characterization ◽  
X Ray Diffraction ◽  
X Ray ◽  
Organic Hybrid ◽  
Scanning Electron

Tungsten (W) micro-/nanoparticles were synthesized by thermally treating tungstate-based inorganic-organic hybrid nanobelts with a lamellar structure or the mixture of WO3 nanoplates and C6H12O6 in an Ar flow at 1000-1200 oC for 2-6 h. Phase compositions and morphologies of the W particles obtained were characterized by powder X-ray diffraction and scanning electron microscope.

scholarly journals Synthesis and characterization of poly thiophene-2-carbaldehyde by hydrochloric acid as catalyst

2021 ◽  
Vol 48 (3) ◽  
Author(s):  
Ahmad Al-Hamdan ◽  
◽  
Ahmad Al-Falah ◽  
Fawaz Al-Deri ◽  
◽  
...  
Keyword(s):  
Electron Microscope ◽  
Hydrochloric Acid ◽  
Scanning Electron Microscope ◽  
Polymer Structure ◽  
Spherical Particles ◽  
Morphological Properties ◽  
Synthesis And Characterization ◽  
Ft Ir ◽  
Scanning Electron

Usually, thiophene and its derivatives are polymerized by chemical and electrochemical methods. In this paper, thiophene-2-carbaldehyde was polymerized by hydrochloric acid as a catalyst in alcohol as a solvent. The resulting polymer was characterized by (FT/IR, 1H-NMR, EDX, and XPS) to determine the polymer structure. The resulting polymer was scanned by scanning electron microscope (SEM) for its morphological properties. We found the polymer consisting of spherical particles with a rough surface (average diameters of 127 nanometers) that clump together and form clusters.

Synthesis and Characterization of Spherical Aggregations of Organic-ZnS Hybrids

2012 ◽  
Vol 268-270 ◽  
pp. 262-265
Author(s):  
Jun Song Yang
Keyword(s):  
Electron Microscope ◽  
Scanning Electron Microscope ◽  
Photophysical Properties ◽  
Luminescent Properties ◽  
Synthesis And Characterization ◽  
Hybrid Particles ◽  
Spherical Structure ◽  
Scanning Electron ◽  
Large Spherical

By using a novel terpyridine-based dye (4-(4-2-[dimethyl4,4'-(phenylazanediyl) dibenzoate]phenyl)-2,2:6,2-terpyri-dine(L)) as a surface stabilizing agent, novel dye-capped ZnS were obtained. The photophysical properties of these dye-capped ZnS have been investigated experimentally. These hybrid particles (ZnS/L) aggregate a large spherical structure observed by scanning electron microscope (SEM) exhibiting novel luminescent properties, which differ from those of the pure L.

Characterization of Sputtered Films using the Scanning Electron Microscope

1973 ◽  
Vol 31 ◽  
pp. 44-45
Author(s):  
R. F. Schneidmiller ◽  
W. F. Thrower ◽  
C. Ang
Keyword(s):  
Electron Microscope ◽  
Scanning Electron Microscope ◽  
Thin Film Deposition ◽  
Film Deposition ◽  
Sputtered Films ◽  
Plasma Sputtering ◽  
Microelectronic Devices ◽  
Control Film ◽  
Scanning Electron

Solid state materials in the form of thin films have found increasing structural and electronic applications. Among the multitude of thin film deposition techniques, the radio frequency induced plasma sputtering has gained considerable utilization in recent years through advances in equipment design and process improvement, as well as the discovery of the versatility of the process to control film properties. In our laboratory we have used the scanning electron microscope extensively in the direct and indirect characterization of sputtered films for correlation with their physical and electrical properties.Scanning electron microscopy is a powerful tool for the examination of surfaces of solids and for the failure analysis of structural components and microelectronic devices.

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