Mechanical Performance of the Annealed NiTi Shape Memory Alloy Coating onto 316L Stainless Bio-Steel

2010 ◽  
Vol 297-301 ◽  
pp. 365-369 ◽  
Author(s):  
Tuty Asma Abubakar ◽  
M. Rahman ◽  
Denis P. Dowling ◽  
Joseph Stokes ◽  
M.S.J. Hashmi

This paper presents the mechanical performance of the annealed NiTi Shape Memory Alloy (SMA) coating deposited onto 316L stainless steel substrate. The as-deposited SMA coating, Ni55.9 Ti44.1, showed an amorphous behaviour. The crystalline NiTi (SMA) coating was produced by annealing the as-deposited NiTi with a thickness about 2.0 µm, at above its crystallisation temperature in a vacuum ambient. The annealed NiTi coatings were characterised to determine the effect of the annealing parameters on their mechanical behaviour. The NiTi phases and structures were determined by x-ray diffraction (XRD) and scanning electron microscopy (SEM) whereas the mechanical properties were measured using the Rockwell C adhesion test. Three main phases; NiTi B2 parent phase, Ni3Ti and TiO2 were found in the annealed samples and the intensities of each phase were dependent on the annealing temperature and annealing time. Each phase significantly affected the mechanical behaviour of the coatings. Higher intensities of Ni3Ti and TiO2 phases were believed to contribute to the low adhesion of the annealed NiTi coatings due to their brittle properties. The annealing parameters; 600 °C for durations of 30 min was considered as the optimum parameter, yielding no fine cracks at the Rockwell C indentation interface compared to other samples at high magnification under the SEM. Adding a hard top layer of TiN would potentially provide a hard coating with an interlayer capable of absorbing impact which would be very suitable for ball joints used in hip replacement therapy.

Author(s):  
K. P. Mohanchadra ◽  
Michael C. Emmons ◽  
Sunny Karnani ◽  
Gregory P. Carman ◽  
W. Lance Richards

This paper describes the sputter deposition and characterization of nickel titanium (NiTi) shape memory alloy thin film onto the surface of an optical fiber Bragg sensor. The NiTi coating uniformity, crystallinity and transformation temperatures are measured using scanning electron microsocopy, x-ray diffraction and differential scanning calorimetry respectively. The strain in the optical fiber is measured using centroid calculation of wavelength shifts. Results show distinct and abrupt changes in the optical fiber signal with the four related transformation temperatures represented by the austenite-martensite forward and reverse phase transformations. These tests demonstrate a coupling present between optical energy and thermal energy, i.e. a modified multiferroic material.


2018 ◽  
Vol 2018 ◽  
pp. 1-13
Author(s):  
Xian Xu ◽  
Guangming Cheng ◽  
Junhua Zheng

Austenitic shape memory alloy has potential applications in self-centering seismic resistant structural systems due to its superelastic response under cyclic tension. Raw austenitic SMA needs proper pretreatments and pretraining to gain a stable superelastic property. In this paper, tests are carried out to investigate the effects of pretraining, pretreatments, loading rate, and strain amplitude on the mechanical performance on austenitic SMA rods with a given size. The tested rods are to be used in a new concept self-centering steel link beam. Customized pretraining scheme and heat treatment are determined through the tests. The effects of loading rate and strain amplitude are investigated. A simplified stress-strain model for the SMA rods oriented to numerical simulations is obtained based on the test results. An example of using the simplified material model in numerical analysis of a self-centering steel link beam is conducted to validate the applicability of the model.


2017 ◽  
Vol 907 ◽  
pp. 8-13 ◽  
Author(s):  
Lucian Burlacu ◽  
Nicanor Cimpoeşu ◽  
Nicoleta Monica Lohan ◽  
Leandru Gheorghe Bujoreanu

The paper introduces the possibility to replace the “wet alloy”, used for sprinkler-triggering within automatic fire protection systems, with a shape memory alloy (SMA) type. The idea of the present application is based on the thermoelastic reversible martensitic transformation, governing SMA functioning, which has completely reversible character, and enables the occurrence of two-way shape memory effect (TWSME) after the application of a thermomechanical treatment called “training”. For this purpose a commercial NiTi rod, which was martensitic at room temperature, was subjected to thermal analysis tests, performed by differential scanning calorimetry (DSC) and dilatometry. Martensite (M) reversion to parent phase (A), during heating, was emphasized by an endothermic peak on the DSC thermogram and by a length shrinkage, on the dilatogram. The capacity to develop TWSME was revealed by the change in displacement-temperature variation, with increasing the number of training cycles. This stabilized fully reversible behavior recommends NiTi rods as executive elements of a new concept of resettable sprinkler for fire protection.


2018 ◽  
Vol 27 (1-2) ◽  
Author(s):  
Pardeep Sharma

AbstractThe current research work focuses on the mechanical and tribological behavior of an NiTi shape memory alloy (SMA) processed with the help of powder metallurgy. SMAs have found applications in the medical, space and aerospace industries with usage in the manufacturing of microelectromechanicals (MEMS) and as actuators in the electronic industry. The wear behavior of a material greatly affects its performance. The wear behavior of an SMA can be determined with the help of the dry abrasion test. The increase in binder content and rotational speed at a constant load increases the wear rate of SMA alloys. The coefficient of friction decreases with the usage of alloys. A decrease in density has been found, as well as porosity, with the increasing content of binder in the alloy. Density decreases from 6.7 to 5.1 g/cm3 while porosity decreases from 57 to 23% with increased binder content. Scanning electron microscopy (SEM) and X-ray diffraction has been used for the investigation of surface morphology and phases present in the alloy.


1990 ◽  
Vol 31 (11) ◽  
pp. 935-940 ◽  
Author(s):  
Tsugio Tadaki ◽  
Hiroshi Okazaki ◽  
Yoshiyuki Nakata ◽  
Ken’ichi Shimizu

2007 ◽  
Vol 130 ◽  
pp. 151-154 ◽  
Author(s):  
Tomasz Goryczka ◽  
Paweł Pączkowski ◽  
Józef Lelątko ◽  
Tadeusz Wierzchoń ◽  
Henryk Morawiec

In order to increase corrosion resistance, the NiTi shape memory alloy was covered by protection layers using glow discharge method. Samples were nitrided with some oxygen addition at temperatures: 350, 380, 400 and 800°C. Microstructure and sequence of obtained layers were studied applying X-ray diffraction technique as well as electron microscopy. Low temperature process produces a layers which consist of Ti3O5, TiN and Ni2Ti4O. Intermediate Ni3Ti layer was between Ni2Ti4O and NiTi matrix. High temperature process forms TiO2 and TiN with interlayer Ti2Ni. Surface does not contain phase with Ni, which is considered as toxic element.


2013 ◽  
Vol 203-204 ◽  
pp. 90-93 ◽  
Author(s):  
Karolina Dudek ◽  
Barbara Szaraniec ◽  
Józef Lelątko ◽  
Tomasz Goryczka

In order to improve a biocompatibility of a NiTi shape memory alloys used as a long-term implant, surface was covered by protective multi-layers coating. First, alloy was passivated in autoclave, and then hydroxyapatite was deposited using electrophoresis at room temperature. In result of that multi-layer was formed on the top of the surface consisted of titanium oxide and hydroxyapatite. Phase identification done with use of grazing incidence beam X-ray diffraction proved sequence of obtained coatings. Applied procedure for multi-layer deposition allowed avoiding of the B2 parent phase decomposition. Moreover, the martensitic transformation occurs in two-steps.


2015 ◽  
Vol 60 (3) ◽  
pp. 1777-1782 ◽  
Author(s):  
K. Dudek ◽  
T. Goryczka ◽  
T. Wierzchoń ◽  
J. Lelątko

Abstract In order to improve a corrosion resistance and biocompatibility of NiTi shape memory alloys, the surface of the NiTi alloy was covered by protective layers. The paper presents results of the layers composed of titanium nitride and hydroxyapatite (HAp). The TiN layers were deposited using the glow discharge technique and then the bioactive hydroxyapatite layer was formed from simulated body fluids solution. The results of the structure studies and microscopic observations confirmed that on the surface of the NiTi alloy a thin titanium nitride layer 35-50 nm thick (depending on the glow discharge technique parameters) was obtained. The structure of the deposited layers was studied by means of the X-ray diffraction technique. Also, mechanical parameters of obtained layers were characterized using nanoindentation. On the top of the titanium nitride, a layer consisted of hydroxyapatite and NaCl was formed. Applied parameters of deposition process did not lead to decomposition of the NiTi parent phase (B2) to the equilibrium ones.


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