Numerical analysis of WaveOne Gold and 2Shape endodontic files during root canal treatment

This study aims to develop and analyse a finite element model of the endodontic nickel-titanium (NiTi) instrument during the root canal treatment (RCT). The 3D model of the tooth and the endodontic instrument has been created using computer-aided design software. The nonlinear explicit dynamic analysis in the CAE package (ANSYS) has been used to analyse the mechanical behaviour of endodontic instruments such as total deformation, equivalent elastic strain, and equivalent stress during canal preparation. The mechanical behaviour of three commercially available endodontic NiTi alloy instruments such as WaveOne Gold (WOG), 2Shape 1 (TS1) and 2Shape 2 (TS2) endodontic files was evaluated using FEA. Consequently, the effect of deformation, equivalent stress and equivalent elastic strain on endodontic files during cleaning and shaping are investigated and compared. The results show that the total deformation and equivalent elastic strain are maximum in the TS1 endodontic file in comparison to TS2 and WOG files. Graphical abstract [Formula: see text]

Ionic liquid-Functionalized Poly-N-phenylpyrrole coating on NiTi Alloy Substrate for highly efficient Solid-phase Microextraction

A novel ionic liquid (i.e. 1-butyl-3-methylimidazolium hexafluorophosphate, [C4MIM]PF6) doped poly-N-phenylpyrrole (PPPy) composite coating ([C4MIM]PF6@PPPy) was successfully fabricated by direct electrochemical polymerization on the surface of NiTi substrate as solid phase...

Influence of annealing on the functional properties of the NiTi alloy produced by wire arc additive manufacturing

The influence of the annealing temperature on the recoverable strain variation on cooling and heating under a stress of 200 MPa was studied in the NiTi samples produced by wire arc additive manufacturing. The samples including the Ni-rich NiTi layer in the working length were annealed for 10 hours at various temperature from 450 to 600 °C. It is shown that an increase in annealing temperature leads to non-monontonic variation in the recoverable strain. This is caused by an increase in annealing temperature from 450 to 550 °C increases the volume fraction of Ni4Ti3 precipitates. As a result, the volume fraction of the NiTi phase undergoing the martensitic transformation and recoverable strain decrease. An increase in annealing temperature from 550 to 600 °C leads to a dissolving the Ni4Ti3 precipitates and formation of the Ni3Ti2 precipitates that increases the volume fraction of the NiTi phase and the recoverable strain.

Formation tantalum coating on NiTi surface by magnetron sputtering technique

The materials of research the structure and morphology of the tantalum coating on the surface of the NiTi alloy in this work presents. Tantalum was deposited by the DC - magnetron sputtering method. The influence of the energy supplied to the magnetron on the formation of the Ta-coating is shown.Changes in the structure of the coating at different stages of its formation are shown.It was found that with a significant decrease in the energy supplied to the magnetron, tantalum is deposited more uniformly. Besides the gradient of mechanical stresses in the coating is reduced.

The Influence of the Soaking Temperature Rotary Forging and Solution Heat Treatment on the Structural and Mechanical Behavior in Ni-Rich NiTi Alloy

The structural and thermophysical characteristics of an Ni-rich NiTi alloy rod produced on a laboratory scale was studied. The soak temperature of the solution heat-treatment steps above 850 °C taking advantage of the precipitate dissolution to provide a matrix homogenization, but it takes many hours (24 to 48) when used without thermomechanical steps. Therefore, the suitable reheating to apply between the forging process steps is very important, because the product’s structural characteristics are dependent on the thermomechanical processing history, and the time required to expose the material to high temperatures during the processing is reduced. The structural characteristics were investigated after solution heat treatment at 900 °C and 950 °C for 120 min, and these heat treatments were compared with as-forged sample structural characteristics (one hot deformation step after 800 °C for a 30 min reheat stage). The phase-transformation temperatures were analyzed through differential scanning calorimetry (DSC), and the structural characterization was performed through synchrotron radiation-based X-ray diffraction (SR-XRD) at room temperature. It was observed that the solution heat treatment at 950 °C/120 min presents a lower martensitic reversion finish temperature (Af); the matrix was fully austenitic; and it had a hardness of about 226 HV. Thus, this condition is the most suitable for the reheating stages between the hot forging-process steps to be applied to this alloy to produce materials that can display a superelasticity effect, for applications such as crack sensors or orthodontic archwires.

A Critical Appraisal of the Use and Properties of Nickel–Titanium Dental Alloys

Nickel–titanium (NiTi) archwires are used in dentistry for orthodontic treatment. NiTi alloys have favourable mechanical characteristics, such as superelasticity and shape memory, and are also known as a corrosion-resistant alloy. In specific cases, an archwire could be attacked by certain types of corrosion or wear degradation, which can cause the leaching of metal ions and a hypersensitive response due to increased concentrations of Ni in the human body. A systematic search of the literature retrieved 102 relevant studies. The review paper focuses on three main fields: (i) electrochemical properties of NiTi wires and the effect of different environments on the properties of NiTi wires (fluoride and low pH); (ii) tribocorrosion, a combination of chemical and mechanical wear of the material, and (iii) the biocompatibility of NiTi alloy and its subsequent effect on the human body. The review showed that corrosion properties are affected by microstructure, pH of saliva and the presence of fluorides. A high variation in published results should be, therefore, interpreted with care. The release of nickel ions was assessed using the same unit, showing that the vast majority of metal ions were released in the first few days of exposure, then a stable, steady state was reached. In tribocorrosion studies, the increased concentrations of Ni ions were reported.