Early Stages of the Recrystallization Texture Formation in {112} - Oriented Silver Single Crystals

2002 ◽  
Vol 408-412 ◽  
pp. 809-814
Author(s):  
Henryk Paul ◽  
Zdzislaw Jasieński ◽  
Claire Maurice ◽  
Andrzej Piątkowski
1969 ◽  
Vol 19 (161) ◽  
pp. 899-924 ◽  
Author(s):  
S. J. Basinski ◽  
Z. S. Basinski ◽  
A. Howie

2004 ◽  
Vol 467-470 ◽  
pp. 177-182 ◽  
Author(s):  
Henryk Paul ◽  
Julian H. Driver ◽  
Claire Maurice ◽  
Andrzej Piątkowski

The recrystallization mechanisms in high purity Ag crystals with C{112}<111> initial orientation, deformed by channel-die compression, have been studied by local orientation measurements using TEM and SEM/EBSD. The microtexture analysis clearly indicates the importance of a simple relation of 25-40o (<111> or <112>) type, which is frequently observed during the early stages of recrystallization between isolated nuclei of uniform orientation and one of the as-deformed groups of components. As recrystallization proceeds, recrystallization twinning increases radically. In C-oriented silver single crystals this latter mechanism also plays a decisive role in the formation of the cube orientation.


2014 ◽  
Vol 783-786 ◽  
pp. 2585-2590
Author(s):  
M. Miszczyk ◽  
Henryk Paul ◽  
Julian H. Driver ◽  
Claire Maurice

The objective of this paper is to identify the predominant crystallographic relations between deformed state and recrystallized grains during the early stages of recrystallization of fcc metals with medium and low stacking fault energy. The experimental investigations, based on SEM/EBSD measurements, have focused on the transformations which occur in plane strain compressed single crystals with stable orientations. After annealing the disorientation across the recrystallization front 'defines' the final rotation by angles in the ranges of 25-35oand 45-55oaround axes mostly grouped near the <122>, <012>, <112> and <111> directions located around the normals of all four {111} slip planes.


1970 ◽  
Vol 14 ◽  
pp. 214-230 ◽  
Author(s):  
M. Matsuo ◽  
S. Hayami ◽  
S. Nagashima

AbstractThe possibility that primary recrystallization textures are influenced by local inhomogeneities of deformation induced in the regions of grain boundaries has been confirmed by comparing the cold rolling and the annealing textures of polycrystalline pure irons which were different in the grain size prior to cold rolling. Analyses were made for the effects of deformation on crystals, namely storage of lattice strain and orientation spread, with application of X-ray diffraction techniques, in order to elucidate the role of in homogeneities of deformation on recrystallization texture formation. Apparent correspondence was found between the orientation dependence of stored strain energy and the textural change on recrystallization. This is a scribed to oriented nucleation in high energy blocks, in the case of originally large-grain material in which the effects of inhomogeneities of deformation are small. But discrepancies arise on this basis in originally small - grain material in which the effects of inhomogeneities of deformation are thought to be considerable. The discrepancy is inferred to arise as an effect of local inhomogeneities of deformation, from the change in the trend of rotational orientation spreads from, a stable orientation and the extent of development of potential nuclei of recrystallization at high energy blocks in the orientation spreads. The change is considered to give rise to the variation in amount of microstrain distribution, which is expressed in recovery characteristics of lattice strains and in the dependence of microstrains on the column length as analyzed by following the procedure of Warren-Averbach.


2013 ◽  
Vol 753 ◽  
pp. 257-262 ◽  
Author(s):  
Wei Min Mao ◽  
Ping Yang

The effects of net driving force for migration of high angle grain boundaries were emphasized beside many other factors which could influence the process of texture formation during recrystallization annealing of 95% cold rolled pure aluminum sheets. The net driving force consists basically of stored energy. However, it could be reduced by recovery, boundary drag, solute drag and Zener drag in different extents, in which only boundary drag is mis-orientation dependent. It was indicated that both oriented nucleation and oriented growth have obvious influence on recrystallization texture, and how far they influence the texture depends also on the level of net driving force when the grain growth starts during annealing. Oriented growth, which is induced by the differences in boundary drag of differently oriented grains, and the corresponding texture formation, could be observed easily when the recrystallization proceeds under relative higher solute drag and Zener drag in commercial purity aluminum. The oriented nucleation process prevails during recrystallization of sufficiently recovered high purity aluminum with very low solute drag and Zener drag, after which strong cube texture forms. In this case the oriented growth indicates limited effect. Both the oriented growth and oriented nucleation will fail if high purity deformation matrix without clear solute drag and Zener drag has not experienced an obvious recovery before recrystallization grain growth, since extremely high net driving force leads to very small critical nucleus size and multiplicity of growing grains, which results in randomization of recrystallization texture.


2017 ◽  
Vol 56 (39) ◽  
pp. 11885-11890 ◽  
Author(s):  
Yi-Yeoun Kim ◽  
Colin L. Freeman ◽  
Xiuqing Gong ◽  
Mark A. Levenstein ◽  
Yunwei Wang ◽  
...  

1993 ◽  
Vol 20 (1-4) ◽  
pp. 125-140 ◽  
Author(s):  
F. Habiby ◽  
F. J. Humphreys

Single crystals and polycrystals of aluminium containing non-deformable second-phase particles of silicon, have been deformed, and the resultant structures investigated by microscopy and by X-ray and microtexture techniques. The particle size is found to influence the scale of the deformation bands formed, and there is evidence that particles may affect the nucleation of these bands. The deformed materials were recrystallized, and the effect of particle stimulated nucleation on the weakening of the rolling texture is discussed with reference to a computer simulation. In contrast, the recrystallization texture of particle-containing single crystals deformed on only two slip systems is sharp, and it is shown that the texture components are consistent with plasticity theory.


The beam of an electron microscope has been used to decompose single crystals of silver azide into nitrogen and metallic silver. The decomposition was slow enough to allow electrondiffraction photographs and electron micrographs to be taken at various stages of the decomposition. From these observations it is possible to follow very closely the process of nucleation. The diffraction photographs show that two forms of silver result, one highly oriented and the other randomly oriented. The microscope identifies the two forms. The randomly oriented silver appears to separate at the boundaries of a substructure of the crystal. The highly oriented silver exists as discrete nuclei, of dimensions of the order 0.1 x 0.1 x 0.05p, probably formed near the surface of the silver azide crystal. The nuclei consist of normal metallic silver only at the end of the decomposition. There is no evidence for the formation in the early stages of a small speck of metallic silver which then grows. Rather, a nucleus is a region into which silver diffuses to build up a face-centred cubic lattice of parameter greater than that of normal silver, and which uses the silver positions in the silver azide lattice as the basis for this build-up. In the last stage a collapse to normal metallic silver takes place. During decomposition the size of a nucleus does not appear to change, but the density increases.


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