Preparing MIM Feedstocks for Bio-Applications Using an Agar-Based Binder

2008 ◽  
Vol 587-588 ◽  
pp. 385-389 ◽  
Author(s):  
Fatima M. Barreiros ◽  
A.G. Martins ◽  
Mariana Matos ◽  
João M.G. Mascarenhas ◽  
M. Teresa Vieira

The present study aims to prepare feedstocks for MIM (Metal Injection Molding) where the metal powders are 316L stainless steel powders (SS). The master objective is to compare the performance of a biodegradable binder with a commercial one based on polyolefins. Different challenges must be overcome in SS injection molding, as follows: to decrease binder/carbon content in feedstocks; to decrease carbon contamination during debinding and sintering; to avoid the formation of chromium carbide and presence of precipitation-free zones; to avoid the grain growth during sintering and to reduce the feedstock price. The optimization of the feedstocks was performed using a torque rheometry technique. Feedstocks of coated and uncoated SS powders mixed with an agar-based binder were used to produce sound parts. A feedstock constituted by SS powders mixed with a high quality commercial binder was the standard. SS with agar-based on feedstocks can admit solids content similar to those based on the commercial binder (62 vol.%). For similar powder content, the sinters resulting from feedstocks with the agar-based binder shows a lower quantity of solid solution of carbon and chromium carbides, absence of precipitation-free zones than commercial feedstocks and good sinter soundness. Coating powders with nanocrystalline stainless steel contribute to control grain growth during debinding and sintering.

2010 ◽  
Vol 44-47 ◽  
pp. 2872-2876
Author(s):  
Pei Li Haw ◽  
Norhamidi Muhamad ◽  
Hadi Murthadha

The rheological behaviors of the Micro Metal Injection Molding feedstock are important for the stability of the feedstock during micro injection molding process and quality of the final micro-components. Homogeneous feedstocks are preferable for MIM process to ensure the dimensional consistency of molded components and prevent the defects of powder-binder separation or particle segregation. In this work, feedstocks with various formulations of 316L stainless steel and binder system were prepared by using Brabender Plastograph EC Plus mixer. The binder system comprises of palm stearin, polyethelene (PE) and stearic acid. In order to obtain the viscosity, activation energy, flow behavior and mold ability index, the rheological characterization of the feedstocks were investigated in numerous conditions by using Shimadzu 500-D capillary rheometer The study showed that all of the 316L stainless steel feedstocks are homogenous with pseudo-plastic behaviors.


2015 ◽  
Vol 651-653 ◽  
pp. 32-37
Author(s):  
Mohamed Sahli ◽  
Jean Claude Gelin ◽  
Thierry Barrière

The metal injection molding (MIM) process allows the manufacturing of small and very complex metallic components. The metal injection molding processing combines the shaping capability of polymer injection molding with the large material variety of metals and ceramics. This paper discusses in detail the development of a numerical model capable of simulating micro-structural evolution and macroscopic deformation during sintering of complex powder compacts. A sintering model based on elastic–viscoplastic constitutive equations was proposed and the corresponding parameters such as bulk viscosity, shearing viscosity and sintering stress were identified from dilatometer experimental data. The constitutive model was then implemented into finite element software in order to perform the simulation of the sintering process. The numerical simulation methods being compared against results of the sintering experiments. The experimental data were obtained from sintering of 316L stainless steel powders.


2014 ◽  
Vol 879 ◽  
pp. 134-138 ◽  
Author(s):  
Nurazilah Mohd Zainon ◽  
Noorsyakirah Abdullah ◽  
Norazlan Roslani ◽  
Mohd Afian Omar

The tribological properties of sintered 316L stainless steel fabricated via injection molding were investigated. Tests were carried out at room temperature comparing metal injection molded dog bone tensile samples at different sintering temperatures. The parameter used for the pin on disk test is a 10kN load, 500m sliding distance and a chromium steel ball as a sliding partner. The morphologies and compositions of the worn surfaces were analyzed by SEM, Raman and XPS. The results showed that the wear mechanism and friction coefficient of SS316L depended strongly on the microstructure which was influenced by the sintering temperature.


1995 ◽  
Vol 10 (3) ◽  
pp. 425-438 ◽  
Author(s):  
G. Veltl ◽  
Th. Hartwig ◽  
F. Petzoldt ◽  
H.-D. Kunze

2015 ◽  
Vol 60 (2) ◽  
pp. 1281-1285
Author(s):  
Jin Man Jang ◽  
Wonsik Lee ◽  
Se-Hyun Ko ◽  
Chulwoong Han ◽  
Hanshin Choi

Abstract The effects of sintering condition and powder size on the microstructure of MIMed parts were investigated using water-atomized 316L stainless steel powder. The 316L stainless steel feedstock was injected into micro mold with micro features of various shapes and dimensions. The green parts were debound and pre-sintered at 800°C in hydrogen atmosphere and then sintered at 1300°C and 1350°C in argon atmosphere of 5torr and 760torr, respectively. The oxide particles were formed and distributed homogeneously inside the sample except for the outermost region regardless of sintering condition and powder size. The width of layer without oxide particles are increased with decrease of sintering atmosphere pressure and powder size. The fine oxides act as the obstacle on grain growth and the high sintering temperature causes severe grain growth in micro features due to larger amount of heat gain than that in macro ones.


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