Deformation Behavior of Fe-Al Single Crystals Containing Fe2AlTi Precipitates

2018 ◽  
Vol 941 ◽  
pp. 1372-1377
Author(s):  
Hiroyuki Y. Yasuda ◽  
Hiroyuki Yakage ◽  
Yunima Shinohara ◽  
Ken Cho

Fe-20Al-5Ti (at.%) single crystals composed of the bcc Fe-Al matrix and the Fe2AlTi precipitates with the L21 structure was examined. In the single crystals furnace-cooled (FC) from 1373 K to room temperature, coarse Fe2AlTi phase about 300 nm in diameter were precipitated in the bcc matrix. A misfit strain and a dissolution temperature of the L21 precipitates are +0.59% and 1151 K, respectively. The single crystals exhibited high yield stress above 600 MPa up to 973 K while further increase in temperature resulted in a decrease in yield stress due to the dissolution of the precipitates. In the FC crystals, 1/2<111> dislocations in the bcc matrix bypassed the coarse L21 precipitates due to their large misfit strain, resulting in high strength. In contrast, the fine L21 precipitates about 30 nm in diameter were observed in the crystals after solutionization and annealing at 873 K. The crystals with the fine L21 precipitates demonstrated high yield stress above 1100 MPa at and below 773 K. Uncoupled or paired 1/2<111> dislocations cut the fine L21 precipitates, leaving an anti-phase boundary (APB) inside the precipitates. The APB inside the precipitates was considered to be responsible for strong precipitation hardening.

2016 ◽  
Vol 879 ◽  
pp. 2210-2215 ◽  
Author(s):  
Hiroyuki Y. Yasuda ◽  
Ryota Kobayashi

Deformation behavior of Fe-15Al-18Co-3Ti (at.%) single crystals containing the Co2AlTi precipitates was examined. In the single crystals furnace-cooled (FC) from 1373 K to room temperature, coarse Co2AlTi phase with the L21 structure was precipitated in the bcc matrix. The L21 phase showed a cuboidal shape with a misfit strain of 0.59%. It is also noted that large amount of Fe substituted for Co in the Co2AlTi precipitates. The FC single crystals exhibited high yield stress above 600 MPa up to 823 K while further increase in temperature resulted in a decrease in yield stress. In the FC crystals, 1/2<111> dislocations in the bcc matrix bypassed the coarse L21 precipitates due to their large misfit strain, resulting in high strength. In contrast, the fine L21 precipitates about 30 nm in diameter were observed in the crystals after solutionization and annealing at 823 K. The crystals with the fine L21 precipitates demonstrated high yield stress above 1400 MPa at room temperature. Paired 1/2<111> dislocations cut the fine L21 precipitates, which led to high strength. The dependence of the yield stress on the precipitate size was also discussed.


2014 ◽  
Vol 783-786 ◽  
pp. 2869-2874 ◽  
Author(s):  
Hiroyuki Y. Yasuda ◽  
Kentaro Soma ◽  
Yoshiaki Odawara

The effect of the CoAl precipitates on the deformation behavior of Fe-15.0Al-15.0Co (at.%) single crystals was examined. The spherical CoAl phase with the B2 structure was precipitated in the single crystals and was stable below 974 K. The bcc matrix and CoAl phase satisfied the cube-on-cube orientation relationship with a misfit strain of 0.25%. The single crystals showed a high yield stress up to 923 K while the stress dropped at 1023 K due to the dissolution of the CoAl phase into the matrix. Moreover, the activated sip system of the crystals containing the CoAl precipitates depended strongly on loading axis. At <149> orientation, {101} <111> slip favorable for the bcc matrix and the CoAl precipitates were sheared by a pair of 1/2<111> dislocations without forming Orowan loops. The CoAl single phase was known to hardly deform by <111> slip which resulted in high strength at <149> orientation. In contrast, {010} <001> or {hk0} <001> slip favorable for the CoAl precipitates was activated at <011> orientation, although the volume fraction of the CoAl phase was very small. <001> slip was generally impossible to take place in the bcc matrix, leading to the extreme hardening. Therefore, the difference in primary slip system between the bcc matrix and CoAl precipitates was responsible for the significant precipitation hardening.


2002 ◽  
Vol 80 (5) ◽  
pp. 888-890 ◽  
Author(s):  
Yuling Zhang ◽  
Kunquan Lu ◽  
Guanghui Rao ◽  
Yu Tian ◽  
Shaohua Zhang ◽  
...  

1996 ◽  
Vol 460 ◽  
Author(s):  
M. Moriwaki ◽  
K. Ito ◽  
H. Inui ◽  
M. Yamaguchi

ABSTRACTThe deformation behavior of single crystals of Mo(Si,Al)2 with the C40 structure has been studied as a function of crystal orientation and Al content in the temperature range from room temperature to 1500°C in compression. Plastic flow is possible only above 1100°C for orientations where slip along <1120> on (0001) is operative and no other slip systems are observed over whole temperature range investigated. The critical resolved shear stress for basal slip decreases rapidly with increasing temperature and the Schmid law is valid. Basal slip appears to occur through a synchroshear mechanism, in which a-dislocations (b=1/3<1120>) dissociate into two synchro-partial dislocations with the identical Burgers vector(b*1/6<1120>) and each synchro-partial further dissociates into two partials on two adjacent planes.


1988 ◽  
Vol 1 (3) ◽  
pp. 219-243 ◽  
Author(s):  
Susumu Machida ◽  
Hiroshige Kitada ◽  
Hiroshi Yajima ◽  
Akinobu Kawamura

1994 ◽  
Vol 364 ◽  
Author(s):  
S. S. Ezz ◽  
Y. Q. Sun ◽  
P. B. Hirsch

AbstractThe strain rate sensitivity ß of the flow stress τ is associated with workhardening and β=(δτ/δln ε) is proportional to the workhardening increment τh = τ - τy, where τy is the strain rate independent yield stress. The temperature dependence of β/τh reflects changes in the rate controlling mechanism. At intermediate and high temperatures, the hardening correlates with the density of [101] dislocations on (010). The nature of the local obstacles at room temperature is not established.


2020 ◽  
Vol 17 (1) ◽  
pp. 117-128
Author(s):  
N. A. Tanicheva ◽  
◽  
I. V. Fedorov ◽  
I. O. Filippova ◽  
◽  
...  

2014 ◽  
Vol 2014 (0) ◽  
pp. _OS0125-1_-_OS0125-2_
Author(s):  
Shinji ANDO ◽  
Kazuki FUKUSHIMA ◽  
Masayuki TSUSHIDA ◽  
Hiromoto KITAHARA

1944 ◽  
Vol 22 (8) ◽  
pp. 417-424
Author(s):  
C E REYNOLDS ◽  
C V BLUMFIELD ◽  
J CUEREL ◽  
K HAJNAL KONYI

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