scholarly journals Microstructure and texture evolution in polycrystalline ice during hot torsion. Impact of intragranular strain and recrystallization processes

2018 ◽  
Author(s):  
Baptiste Journaux ◽  
Thomas Chauve ◽  
Maurine Montagnat ◽  
Andrea Tommasi ◽  
Fabrice Barou ◽  
...  
Keyword(s):  
High Temperature ◽  
Grain Boundary ◽  
Dynamic Recrystallization ◽  
Grain Boundaries ◽  
Simple Shear ◽  
Texture Evolution ◽  
Boundary Migration ◽  
Shear Plane ◽  
Dislocation Slip ◽  
Polycrystalline Ice

Abstract. Torsion experiments were performed in polycrystalline ice at high temperature (0.97 ⋅ Tm) to reproduce simple shear conditions close to those encountered in ice streams and at the base of fast flowing glaciers. As well documented more than 30 years ago (Hudleston, 1977; Bouchez and Duval, 1982), under simple shear ice develops a two-maxima c-axis texture, which evolves rapidly into a single cluster texture with c-axis perpendicular to the shear plane. This evolution still lacks a physical explanation. Current viscoplastic modeling approaches on ice involving dislocation slip on multiple slip systems (basal pyramidal, and prismatic) fail to reproduce it. Dynamic recrystallization mechanisms that occur in both laboratory conditions and in natural setups are likely candidates to explain the texture evolution observed. In this study, we use Electron BackScattering Diffraction (EBSD) and Automatic Ice Texture Analyzer (AITA) to characterize the mechanisms accommodating deformation, the stress and strain heterogeneities that form under torsion of an initially isotropic polycrystalline ice sample at high temperature, and the role of dynamic recrystallization in accommodating these heterogeneities. These analyses highlight an interlocking microstructure, which results from heterogeneity-driven serrated grain boundary migration, and sub-grain boundaries composed by dislocations with [c]-component Burgers vector, indicating that strong local stress heterogeneity develops, even at high temperature and high finite shear strain. Based on these observations, we propose that that nucleation by bulging, assisted by sub-grain boundary formation, is a very likely candidate to explain the progressive disappearance of the texture cluster at low angle to the shear plane and the stability of the one normal to it. We therefore strongly support the development of new models limiting dislocation slip on non-basal slip system and allowing for efficient polygonization by an association of bulging and formation of sub-grain boundaries with a significant [c]-component.

scholarly journals Recrystallization processes, microstructure and crystallographic preferred orientation evolution in polycrystalline ice during high-temperature simple shear

2019 ◽  
Vol 13 (5) ◽  
pp. 1495-1511 ◽  
Author(s):  
Baptiste Journaux ◽  
Thomas Chauve ◽  
Maurine Montagnat ◽  
Andrea Tommasi ◽  
Fabrice Barou ◽  
...  
Keyword(s):  
High Temperature ◽  
Grain Boundary ◽  
Dynamic Recrystallization ◽  
Grain Boundaries ◽  
Simple Shear ◽  
Shear Plane ◽  
Preferred Orientation ◽  
Dislocation Slip ◽  
Crystallographic Preferred Orientation ◽  
Polycrystalline Ice

Abstract. Torsion experiments were performed in polycrystalline ice at high temperature (0.97 Tm) to reproduce the simple shear kinematics that are believed to dominate in ice streams and at the base of fast-flowing glaciers. As clearly documented more than 30 years ago, under simple shear ice develops a two-maxima c axis crystallographic preferred orientation (CPO), which evolves rapidly into a single cluster CPO with a c axis perpendicular to the shear plane. Dynamic recrystallization mechanisms that occur in both laboratory conditions and naturally deformed ice are likely candidates to explain the observed CPO evolution. In this study, we use electron backscatter diffraction (EBSD) and automatic ice texture analyzer (AITA) to characterize the mechanisms accommodating deformation, the stress and strain heterogeneities that form under torsion of an initially isotropic polycrystalline ice sample at high temperature, and the role of dynamic recrystallization in accommodating these heterogeneities. These analyses highlight an interlocking microstructure, which results from heterogeneity-driven serrated grain boundary migration, and sub-grain boundaries composed of dislocations with a [c]-component Burgers vector, indicating that strong local stress heterogeneity develops, in particular, close to grain boundaries, even at high temperature and high finite shear strain. Based on these observations, we propose that nucleation by bulging, assisted by sub-grain boundary formation and followed by grain growth, is a very likely candidate to explain the progressive disappearance of the c axis CPO cluster at low angle to the shear plane and the stability of the one normal to it. We therefore strongly support the development of new polycrystal plasticity models limiting dislocation slip on non-basal slip systems and allowing for efficient accommodation of strain incompatibilities by an association of bulging and formation of sub-grain boundaries with a significant [c] component.

scholarly journals Microstructural Evidence for Grain Boundary Migration and Dynamic Recrystallization in Experimentally Deformed Forsterite Aggregates

Minerals ◽  
2018 ◽  
Vol 9 (1) ◽  
pp. 17
Author(s):  
Caroline Bollinger ◽  
Billy Nzogang ◽  
Alexandre Mussi ◽  
Jérémie Bouquerel ◽  
Dmitri Molodov ◽  
...  
Keyword(s):  
Grain Boundary ◽  
Dynamic Recrystallization ◽  
Grain Boundaries ◽  
Driving Forces ◽  
Electron Backscatter Diffraction ◽  
Boundary Migration ◽  
Large Strains ◽  
Grain Boundary Migration ◽  
Mapping Techniques ◽  
Von Mises

Plastic deformation of peridotites in the mantle involves large strains. Orthorhombic olivine does not have enough slip systems to satisfy the von Mises criterion, leading to strong hardening when polycrystals are deformed at rather low temperatures (i.e., below 1200 °C). In this study, we focused on the recovery mechanisms involving grain boundaries and recrystallization. We investigated forsterite samples deformed at large strains at 1100 °C. The deformed microstructures were characterized by transmission electron microscopy using orientation mapping techniques (ACOM-TEM). With this technique, we increased the spatial resolution of characterization compared to standard electron backscatter diffraction (EBSD) maps to further decipher the microstructures at nanoscale. After a plastic strain of 25%, we found pervasive evidence for serrated grain and subgrain boundaries. We interpreted these microstructural features as evidence of occurrences of grain boundary migration mechanisms. Evaluating the driving forces for grain/subgrain boundary motion, we found that the surface tension driving forces were often greater than the strain energy driving force. At larger strains (40%), we found pervasive evidence for discontinuous dynamic recrystallization (dDRX), with nucleation of new grains at grain boundaries. The observations reveal that subgrain migration and grain boundary bulging contribute to the nucleation of new grains. These mechanisms are probably critical to allow peridotitic rocks to achieve large strains under a steady-state regime in the lithospheric mantle.

scholarly journals Comparison between experiment and computer modelling of plane-strain simple-shear ice deformation

1994 ◽  
Vol 40 (134) ◽  
pp. 46-55
Author(s):  
C.J. L. Wilson ◽  
Y. Zhang
Keyword(s):  
Grain Size ◽  
Grain Boundary ◽  
Simple Shear ◽  
Computer Modelling ◽  
Boundary Migration ◽  
Stress And Strain ◽  
Grain Boundary Migration ◽  
Lattice Orientation ◽  
Polycrystalline Ice ◽  
Good Agreement

AbstractAn examination of both experiments and computer models of polycrystalline ice undergoing a simple shear suggests that there is good agreement. The model has correctly reproduced the deformational and microstructural features caused by glide on (0001) in the ice aggregates. This success is particularly prominent for those ice grains with a lattice orientation suitable for hard or easy glide or kinking, and where there is a sub-horizontal с axis and a larger grain-size. A limitation may be that the model cannot explicitly simulate recrystallization and grain-boundary migration, which are two other important processes operating jointly with glide in experimentally deformed ice. However, through the use of the models, it is possible to show how kinematic factors can control the processes of recrystallization. The localization of recrystallization in the polycrystalline ice aggregate is determined by the stress and strain variations between neighbouring grains.

scholarly journals Comparison between experiment and computer modelling of plane-strain simple-shear ice deformation

1994 ◽  
Vol 40 (134) ◽  
pp. 46-55 ◽  
Author(s):  
C.J. L. Wilson ◽  
Y. Zhang
Keyword(s):  
Grain Size ◽  
Grain Boundary ◽  
Simple Shear ◽  
Computer Modelling ◽  
Boundary Migration ◽  
Stress And Strain ◽  
Grain Boundary Migration ◽  
Lattice Orientation ◽  
Polycrystalline Ice ◽  
Good Agreement

AbstractAn examination of both experiments and computer models of polycrystalline ice undergoing a simple shear suggests that there is good agreement. The model has correctly reproduced the deformational and microstructural features caused by glide on (0001) in the ice aggregates. This success is particularly prominent for those ice grains with a lattice orientation suitable for hard or easy glide or kinking, and where there is a sub-horizontalсaxis and a larger grain-size. A limitation may be that the model cannot explicitly simulate recrystallization and grain-boundary migration, which are two other important processes operating jointly with glide in experimentally deformed ice. However, through the use of the models, it is possible to show how kinematic factors can control the processes of recrystallization. The localization of recrystallization in the polycrystalline ice aggregate is determined by the stress and strain variations between neighbouring grains.

Analysis of Large Strain Hot Torsion Textures Associated With “Continuous” Dynamic Recrystallization

2008 ◽  
Vol 131 (1) ◽  
Author(s):  
S. M. Lim ◽  
C. Desrayaud ◽  
F. Montheillet
Keyword(s):  
Grain Boundary ◽  
Dynamic Recrystallization ◽  
Large Strain ◽  
Texture Evolution ◽  
Boundary Migration ◽  
Grain Boundary Migration ◽  
Shear Direction ◽  
Continuous Dynamic Recrystallization ◽  
Hot Torsion ◽  
Continuous Dynamic

The development of ideal orientations within the steady-state region of hot torsion flow curves of fcc and bcc metals undergoing “continuous” dynamic recrystallization is analyzed. It is well known that in fcc metals, e.g., Al deformed at 400°C and above, the experimentally observed end texture consists of the twin-symmetric B(112¯)[11¯0]/B¯(1¯1¯2)[1¯10] component, whereby the (hkl)[uvw] indices correspond to the shear plane z and the shear direction θ, respectively. In bcc iron however, only one of the self-symmetric D1(112¯)[111] and D2(1¯1¯2)[111] components dominates (the former in the case of positive shear or clockwise rotation about the r-axis, and the latter during negative shear). The tendency toward a single end orientation imposes certain limitations on grain refinement, as this would ultimately imply the coalescence of subgrains of or close to this orientation, and therefore the disappearance of existing high angle boundaries (≥15 deg). It is believed that the preference of D1 over D2, or vice versa, could be related to phenomena other than glide-induced rotations, e.g., grain boundary migration resulting from differences in work hardening rates. In this paper, the standard Taylor model is first used to predict the texture evolution in simple shear under the full-constraint rate-sensitive scheme. This is then coupled with an approach that takes into account grain boundary migration resulting from differences in dislocation densities within grains of varying orientations. The preliminary results are in agreement with experimental findings, i.e., grains with initial orientations close to D2 grow at the expense of neighboring grains during negative shear and vice versa.

scholarly journals The effect of particles on creep rate and microstructures of granular ice

2008 ◽  
Vol 54 (186) ◽  
pp. 533-537 ◽  
Author(s):  
Min Song ◽  
Ian Baker ◽  
David M. Cole
Keyword(s):  
Creep Rate ◽  
Grain Boundary ◽  
Dynamic Recrystallization ◽  
Grain Boundaries ◽  
Initial Stress ◽  
Nucleation Rate ◽  
Boundary Migration ◽  
Nucleation And Growth ◽  
Grain Boundary Migration ◽  
Before And After

AbstractThe microstructures of particle-free granular freshwater ice and ice containing 1 wt.% of 50 ± 10 mm uniformly distributed particles were investigated before and after compressive creep to ∼10% strain with stresses of 1.45 MPa at −10°C and 0.4 MPa at −5°C. Creep rates of particle-containing ice were always higher than those of particle-free ice. For an initial stress of 1.45 MPa at −10°C, dynamic recrystallization occurred with new grains nucleating and growing along grain boundaries for both sets of specimens, and the ice with particles showed a higher nucleation rate. Under creep with an initial stress of 0.4 MPa at −5°C, dynamic recrystallization also occurred by the nucleation and growth of new grains along the grain boundaries for ice containing particles, but recrystallization in the particle-free ice occurred through grain boundary migration.

Measurement of solute segregation to grain boundaries in the AEM: A review

1988 ◽  
Vol 46 ◽  
pp. 606-607
Author(s):  
D. B. Williams ◽  
A. D. Romig
Keyword(s):  
Grain Boundary ◽  
Grain Boundaries ◽  
Boundary Migration ◽  
Grain Boundary Migration ◽  
Boundary Misorientation ◽  
Collector Plate ◽  
Segregation Process ◽  
Grain Boundary Misorientation ◽  
Structure Boundary ◽  
Equilibrium Segregation

The segregation of solute or imparity elements to grain boundaries can occur by three well-defined processes. The first is Gibbsian segregation in which an element of minimal matrix solubility confines itself to a monolayer at the grain boundary. Classical examples include Bi in Cu and S or P in Fe. The second process involves the depletion of excess matrix solute by volume diffusion to the boundary. In the boundary, the solute atoms diffuse rapidly to precipitates, causing them to grow by the ‘collector-plate mechanism.’ Such grain boundary diffusion is thought to initiate “Diffusion-Induced Grain Boundary Migration,” (DIGM). This process has been proposed as the origin of eutectoid transformations or discontinuous grain boundary reactions. The third segregation process is non-equilibrium segregation which result in a solute build-up around the boundary because of solute-vacancy interactions.All of these segregation phenomena usually occur on a sub-micron scale and are often affected by the nature of the grain boundary (misorientation, defect structure, boundary plane).

Domain coarsening by grain boundary migration in ordered Ni4Mo

1986 ◽  
Vol 44 ◽  
pp. 560-561
Author(s):  
K. Vasudevan ◽  
H. P. Kao ◽  
C. R. Brooks ◽  
E. E. Stansbury
Keyword(s):  
Grain Boundary ◽  
Grain Boundaries ◽  
Short Range ◽  
Boundary Migration ◽  
Grain Boundary Migration ◽  
Rapid Cooling ◽  
Temperature Range ◽  
Fee Structure ◽  
Domain Coarsening ◽  
Boundary Reaction

The Ni4Mo alloy has a short-range ordered fee structure (α) above 868°C, but transforms below this temperature to an ordered bet structure (β) by rearrangement of atoms on the fee lattice. The disordered α, retained by rapid cooling, can be ordered by appropriate aging below 868°C. Initially, very fine β domains in six different but crystallographically related variants form and grow in size on further aging. However, in the temperature range 600-775°C, a coarsening reaction begins at the former α grain boundaries and the alloy also coarsens by this mechanism. The purpose of this paper is to report on TEM observations showing the characteristics of this grain boundary reaction.

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