boundary misorientation
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Metals ◽  
2021 ◽  
Vol 11 (11) ◽  
pp. 1850
Author(s):  
Giancarlo Sanchez Chavez ◽  
Segen Farid Estefen ◽  
Tetyana Gurova ◽  
Anatoli Leontiev ◽  
Lincoln Silva Gomes ◽  
...  

A study of the migration of the grain boundary misorientation and its relationship with the residual stresses through time immediately after the completion of a thermomechanical simulation has been carried out. After physically simulating an intercritically overheated welding heat affected zone, the variation of the misorientation of grain contours was observed with the electron backscatter diffraction (EBSD) technique and likewise the variation of the residual stresses of welding with RAYSTRESS equipment. It was observed that the misorientation of the grain contours in an ASTM DH36 steel was modified after the thermomechanical simulation, which corresponds to the measured residual stress variation along the first week of monitoring, with compressive residual stresses ranging from 195 MPa to 160 MPa. The changes in misorientation indicate that the stress relaxation phenomenon is associated with the evolution of the misorientation in the microstructure caused by the welding procedure. On the first day, there was a fraction of 4% of the kernel average misorientation (KAM) values at 1° misorientation and on the fourth day, there was a fraction of 7% of the KAM values at 1° misorientation.


Crystals ◽  
2021 ◽  
Vol 11 (11) ◽  
pp. 1395
Author(s):  
Hong Li ◽  
Miaoquan Li

The microstructure evolution characteristics and the shear strength of bond and base alloys were investigated during the press bonding of the Ti–5Al–2Sn–2Zr–4Mo–4Cr alloy. The quantitative detection of the interfacial void shows that the interfacial voids shrunk gradually with time and a bond free of voids could be obtained at the time above 10 min. The microstructure of the base alloy shows that the primary α phase tends to be equiaxed because of the increase in plastic deformation and the variation in the volume fraction and grain size of the primary α phase that are complicated with time. The grain boundary misorientation characteristics in bond and base alloys are not consistent. However, they tend to be comparable over time. The shear strength of bond and base alloys at different times was explained and compared. The compared results indicate that the enhanced strength of the bond is mainly due to the increase in the bonded area. However, the strength of the bond decreases slightly because of the slight coarsening of the grain size and the decrease in the volume fraction of the primary α phase at the time more than 20 min. The shear strength of the bond and base alloys tends to be highest and close at 10 min.


Materials ◽  
2021 ◽  
Vol 14 (18) ◽  
pp. 5129
Author(s):  
Abhilash Kiran ◽  
Martina Koukolíková ◽  
Jaroslav Vavřík ◽  
Miroslav Urbánek ◽  
Jan Džugan

The microstructural morphology in additive manufacturing (AM) has a significant influence on the building structure. High-energy concentric heat source scanning leads to rapid heating and cooling during material deposition. This results in a unique microstructure. The size and morphology of the microstructure have a strong directionality, which depends on laser power, scanning rate, melt pool fluid dynamics, and material thermal properties, etc. The grain structure significantly affects its resistance to solidification cracking and mechanical properties. Microstructure control is challenging for AM considering multiple process parameters. A preheating base plate has a significant influence on residual stress, defect-free AM structure, and it also minimizes thermal mismatch during the deposition. In the present work, a simple single track deposition experiment was designed to analyze base plate preheating on microstructure. The microstructural evolution at different preheating temperatures was studied in detail, keeping process parameters constant. The base plate was heated uniformly from an external heating source and set the stable desired temperature on the surface of the base plate before deposition. A single track was deposited on the base plate at room temperature and preheating temperatures of 200 °C, 300 °C, 400 °C, and 500 °C. Subsequently, the resulting microstructural morphologies were analyzed and compared. The microstructure was evaluated using electron backscattered diffraction (EBSD) imaging in the transverse and longitudinal sections. An increase in grain size area fraction was observed as the preheating temperature increased. Base plate preheating did not show influence on grain boundary misorientation. An increase in the deposition depth was noticed for higher base plate preheating temperatures. The results were convincing that grain morphology and columnar grain orientation can be tailored by base plate preheating.


Crystals ◽  
2021 ◽  
Vol 11 (8) ◽  
pp. 923
Author(s):  
Hui Zhou ◽  
Pei Wang ◽  
Shanping Lu

A dislocation density–grain boundary interaction scheme coupled with the dislocation density-based crystalline plasticity finite element method has been established and used to investigate the deformation behavior of bicrystalline pillars with the same grain boundary misorientation angle but different crystal orientations. It is found that the angle between the activated slip systems, which is determined by the crystal orientations, rather than the grain boundary misorientation angle, influences the interactions between the plastic slip and the grain boundary, which further influence the heterogeneous deformation of bicrystalline specimens.


Materials ◽  
2021 ◽  
Vol 14 (12) ◽  
pp. 3426
Author(s):  
Shuwan Cui ◽  
Shuwen Pang ◽  
Dangqing Pang ◽  
Zhiqing Zhang

In this paper, 8.0 mm thickness 2205 duplex stainless steel (DSS) workpieces were welded with a keyhole tungsten inert gas (K-TIG) welding system under different welding speeds. After welding, the morphologies of the welds under different welding speed conditions were compared and analyzed. The microstructure, two-phase ratio of austenite/ferrite, and grain boundary characteristics of the welded joints were studied, and the microhardness and tensile properties of the welded joints were tested. The results show that the welding speed has a significant effect on the weld morphology, the two-phase ratio, grain boundary misorientation angle (GBMA), and mechanical properties of the welded joint. When the welding speed increased from 280 mm/min to 340 mm/min, the austenite content and the two-phase ratio in the weld metal zone (WMZ) decreased. However, the ferrite content in the WMZ increased. The proportion of the Σ3 coincident site lattice grain boundary (CSLGB) decreased as the welding speed increased, which has no significant effect on the tensile strength of welded joints. The microhardness of the WMZ and the tensile strength of the welded joint gradually increased when the welding speed was 280–340 mm/min. The 2205 DSS K-TIG welded joints have good plasticity.


2021 ◽  
Vol 2021 ◽  
pp. 1-11
Author(s):  
Yunqiang Zhao ◽  
Chunlin Dong ◽  
Zhongxue Jia ◽  
Jiaqing You ◽  
Jinhong Tan ◽  
...  

In this study, 2205 duplex stainless steel was friction-stir-welded at different welding speeds. The microstructural characteristics such as grain sizes, grain boundary misorientation angles, and phase contents in the stir zones of the joints were detected. The potentiodynamic polarization and electrochemical impedance spectroscopy were also measured to evaluate the corrosion property of the stir zones. The effects of the microstructures on the corrosion property for friction-stir-welded 2205 duplex stainless steel were analyzed. The results indicated that the FSW process refined the grains and increased the ferrite contents in the stir zones. With increasing the welding speed from 30 mm/min to 50 mm/min, the grain size in the stir zone decreased from 1.64 μm to 0.96 μm, the ferrite content decreased from 59% to 54.4%, and the fractions of low angle grain boundaries for austenite and ferrite phases decreased from 63.9% and 92.6% to 18.0% and 41.1%, respectively. In this study, the effect of grain size on the corrosion resistance was the most significant and it was followed by the phase composition and the grain boundary misorientation angle. The stir zone obtained at 50 mm/min has the highest corrosion resistance, and it is followed by the base material and the stir zone obtained at 30 mm/min.


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