scholarly journals Screening of factors influencing the hydrolysis reaction of chicken leg cartilage with Protamex enzyme as a catalyst

2020 ◽  
Vol 19 (04) ◽  
pp. 73-79
Author(s):  
Cuong V. Bui
Keyword(s):  
Amino Acid ◽  
Reaction Time ◽  
Reaction Temperature ◽  
Hydrolysis Reaction ◽  
Reaction Volume ◽  
Optimal Point ◽  
Acid Yield ◽  
Acid Hydrolysate ◽  
Significant Difference ◽  
Enzyme Ratio

The objective of this research was to use Protamex enzyme as a catalyst to hydrolyze chicken leg cartilage for production of amino acid hydrolysate. The proximate composition of chicken cartilage was analyzed. The results indicated that the major components in the dry matter of chicken leg cartilage were lipid (19.72 ± 0.05%) and protein (13.34 ± 0.08%). The main parameters affecting the hydrolysis reaction of chicken leg cartilage with Protamex enzyme were selected for investigation: reaction temperature (oC), pH, enzyme ratio (%, based on the weight of substrate), reaction time (min), and the ratio of reaction volume (v/v). The significant difference was analyzed by ANOVA One-Way to identify the optimal point of each parameter toward amino acid yield. The results revealed that the hydrolysis degree and amino acid yield reached the maximal values of 22.93 ± 4.01% and 30.25 ± 1.86%, respectively, when the reaction temperature, pH, enzyme ratio, reaction time, and ratio of reaction volume (v/v) were 40oC, 4, 0.52%, 40 min, and 1/18, respectively.

Preparation of A Spherical Cellulose Adsorbent as Amino Acid Sorbent

2011 ◽  
Vol 197-198 ◽  
pp. 899-905 ◽  
Author(s):  
Chun Xiang Lin ◽  
Ming Hua Liu ◽  
Huai Yu Zhan
Keyword(s):  
Amino Acids ◽  
Amino Acid ◽  
Reaction Time ◽  
Acrylic Acid ◽  
Reaction Temperature ◽  
Monomer Concentration ◽  
Initiator Concentration ◽  
Basic Amino Acids ◽  
Cellulose Adsorbent

The spherical cellulose adsorbent was prepared by grafting acrylic acid onto the spherical cellulose beads prepared by NMMO method. The effecting factors, e.g., monomer concentration, initiator concentration, reaction temperature and reaction time were optimized by the orthogonal and signal-factor experiments and the structure of the adsorbent was characterized by FTIR and SEM. The graft mechanism was also discussed. Moreover, the spherical cellulose adsorbents were shown to behave as good sorbents for basic amino acids L-Arg, L-Lys and L-His.

Transesterification of Natural Lecithin Catalyzed by Isopropylamine

2014 ◽  
Vol 884-885 ◽  
pp. 603-606
Author(s):  
Hong Ya Li ◽  
Biao Yan ◽  
Xiao Li Zhang ◽  
Bin Xia Zhao
Keyword(s):  
Reaction Time ◽  
Reaction Temperature ◽  
Boiling Point ◽  
Transesterification Reaction ◽  
Reaction Volume ◽  
Effective Catalyst ◽  
Total Reaction ◽  
Mild Conditions ◽  
Catalyst Content

The isopropylamine with low boiling point was used for preparing GPC from natural lecithin under mild conditions, it was confirmed as an effective catalyst and the recovery can be combined with the recovery of methanol by distillation. The mechanism of the transesterification reaction was proposed and the experiments obtained the better effect under the conditions of: catalyst content was 2.4% of the total reaction volume, lecithin concentration was 0.05-0.10mol L1 , reaction temperature was 60 °C and reaction time was 260 min.

Hydrothermal Conversion of Glucose into Lactic Acid with Nickel as a Catalyst

2011 ◽  
Vol 347-353 ◽  
pp. 3873-3876
Author(s):  
Adama Yousif ◽  
Xu Zeng ◽  
Fang Ming Jin ◽  
Yan Fang
Keyword(s):  
Lactic Acid ◽  
Reaction Time ◽  
Reaction Temperature ◽  
Efficient Method ◽  
Optimum Conditions ◽  
Hydrothermal Conditions ◽  
Hydrothermal Conversion ◽  
Acid Yield

In this paper, an efficient method for producing lactic acid from glucose with nickel as a catalyst under hydrothermal conditions has been developed. The addition of nickel can improve the lactic acid yield efficiently under alkaline hydrothermal conditions. The highest lactic acid yield of 35% was obtained under the optimum conditions, i.e., reaction temperature 300 °C, reaction time 60 s, 0.5 mmol nickel and 2.5 M NaOH.

L-α-Glycerophosphocholine from Natural Lecithin via Transesterification Catalyzed by Propylamine

2014 ◽  
Vol 997 ◽  
pp. 73-76
Author(s):  
Hong Ya Li ◽  
Tian Tian Zhang
Keyword(s):  
Reaction Time ◽  
Reaction Temperature ◽  
Boiling Point ◽  
Reaction Volume ◽  
Total Reaction ◽  
Catalyst Content

The propylamine with low boiling point was confirmed as effective catayst for preparing GPC from natural lecithin via transesterification. The catalyst can be separated combined with the recovery of methanol by distillation. Under the conditions of: the catalyst content was 2.4% of the total reaction volume, lecithin concentration was 0.05-0.10mol L–1 , reaction temperature was 60 °C and reaction time was 4 h, the conversion of phosphatidylcholine could reach over 98%.

Study on the Transesterification of Phosphatidylcholine over Diethylamine

2014 ◽  
Vol 997 ◽  
pp. 93-96
Author(s):  
Biao Yan ◽  
Tian Tian Zhang
Keyword(s):  
Reaction Time ◽  
Reaction Temperature ◽  
Boiling Point ◽  
Reaction Volume ◽  
Total Reaction ◽  
Catalyst Content

The catalyst diethylamine with low boiling point can be separated combined with the recovery of ethanol by distillation in the transesterification of phosphatidylcholine, and it was an effective catayst for preparing GPC from natural lecithin via transesterification. Under the conditions of: the catalyst content was 3.6% of the total reaction volume, lecithin concentration was 100 mmol/L , reaction temperature was 60 °C and reaction time was 260 min, the phosphatidylcholine was reacted completely and the yield of GPC can reach about 80%

Analysis of Task Difficulty under Varying Conditions of Induced Stress

1970 ◽  
Vol 31 (2) ◽  
pp. 343-348 ◽  
Author(s):  
Jerry W. Thornton ◽  
Paul D. Jacobs
Keyword(s):  
Reaction Time ◽  
Choice Reaction Time ◽  
Reaction Time Task ◽  
Simple Reaction Time Task ◽  
Simple Task ◽  
Practical Applications ◽  
Time Task ◽  
Significant Difference ◽  
Task Relatedness ◽  
Related Stress

Two tasks (simple and choice reaction time) were examined while varying three types of stressors (shock, threat of shock, and noise) and the stressor task relationship (i.e., task-related stress, task-unrelated stress, and no-stress). Four specific hypotheses were tested and 3 were supported in the simple reaction-time task. There were no significant differences among stressors for either task, although greater differences were reported in the simple than in the choice reaction-time task. A significant difference between the “task-relatedness” of stress levels in the simple task was interpreted as possibly due to a “coping” or “protective adaptive mechanism” in which increases in performance serve to reduce stress. Practical applications were examined.

Optimization of Magnesium Separation and Extraction from Boron Slurry Using Response Surface Methodology

2011 ◽  
Vol 366 ◽  
pp. 366-369
Author(s):  
Feng Gao ◽  
Rong Fu ◽  
Ming Yang Qian ◽  
Zhu Min Wang ◽  
Xiang Zhang
Keyword(s):  
Response Surface Methodology ◽  
Reaction Time ◽  
Factorial Design ◽  
Response Surface ◽  
Reaction Temperature ◽  
Fractional Factorial Design ◽  
Design Criterion ◽  
Fractional Factorial ◽  
Effective Factors

Response surface methodology was used to optimize the soaking Mg leaching ratio from the boron slurry screened by 25 fractional factorial design. Five effective factors such as H2SO4 concentrations, reaction time, reaction temperature and stir velocity were tested by using 25 fractional factorial design criterion and three effective factors H2SO4 concentrations, reaction time and reaction temperature showed significant effect(P2SO4 concentrations of 0.29mol/l, reaction time of 90 min and reaction temperature of 50°C. Three runs of additional confirmation experiments were conducted. The mixture magnesium leaching value was 58.20%.

Ring-Opening Polymerization of Lactide Using Aluminum Salen-Type Initiators

2014 ◽  
Vol 915-916 ◽  
pp. 713-716
Author(s):  
Qing Zhang ◽  
Jing Tian ◽  
Zhi Qi Cao ◽  
Ru Xia Xu ◽  
Zhen Zhen Sun ◽  
...  
Keyword(s):  
Nuclear Magnetic Resonance ◽  
Infrared Spectroscopy ◽  
Reaction Time ◽  
Magnetic Resonance ◽  
Schiff Bases ◽  
Reaction Temperature ◽  
Ring Opening ◽  
Ring Opening Polymerization ◽  
Resonance Spectroscopy ◽  
Aluminum Complex

In this investigation, Schiff bases aluminum complex was synthesized and used as the initiator in the polymerization of D,L-lactide. The aluminum complex was characterized by infrared spectroscopy (IR), and nuclear magnetic resonance spectroscopy (NMR). The influences of different factors, including reaction time, reaction temperature, and the ratio of D, L-lactide/Al3+ on the synthesis of polylactide were described. The results showed that Schiff bases aluminum complex could be successfully applied in the ring opening polymerization. The optimum condition of the ring opening polymerization of D,L-lactide, which included D,L-lactide/Al3+ (mol/mol) ratio of 250, reaction temperature of 120 °C, and reaction time of 16 hours.

scholarly journals Synthesis of propylene carbonate from urea and 1,2-propylene glycol over metal carbonates

2011 ◽  
Vol 17 (3) ◽  
pp. 323-331 ◽  
Author(s):  
Jiancheng Zhou ◽  
Wu Dongfang ◽  
Birong Zhang ◽  
Yali Guo
Keyword(s):  
Reaction Time ◽  
Propylene Glycol ◽  
Propylene Carbonate ◽  
Reaction Temperature ◽  
Reaction Conditions ◽  
Lead Carbonate ◽  
Synthetic Process ◽  
Metal Carbonates ◽  
Optimal Reaction ◽  
Mixed Carbonate

A series of single-metal carbonates and Pb-Zn mixed-metal carbonates were prepared as catalysts for alcoholysis of urea with 1,2-propylene glycol (PG) for the synthesis of propylene carbonate (PC). The mixed carbonates all show much better catalytic activities than the single carbonates, arising from a strong synergistic effect between the two crystalline phases, hydrozincite and lead carbonate. The mixed carbonate with Pb/Zn=1:2 gives the highest yield of PC, followed by the mixed carbonate with Pb/Zn=1:3. Furthermore, Taguchi method was used to optimize the synthetic process for improving the yield of PC. It is shown that the reaction temperature is the most significant factor affecting the yield of PC, followed by the reaction time, and that the optimal reaction conditions are the reaction time at 5 hours, the reaction temperature at 180 oC and the catalyst amount at 1.8 wt%, resulting in the highest PC yield of 96.3%.

Hydrothermal Sintering under Mild Temperature Conditions: Preparation of Calcium-deficient Hydroxyapatite Compacts

2010 ◽  
Vol 65 (8) ◽  
pp. 1038-1044 ◽  
Author(s):  
Kazumichi Yanagisawa ◽  
Jae-Hyen Kim ◽  
Chisato Sakata ◽  
Ayumu Onda ◽  
Eri Sasabe ◽  
...  
Keyword(s):  
Reaction Time ◽  
Reaction Temperature ◽  
Hot Pressing ◽  
Reaction Parameter ◽  
High Bulk Density ◽  
Temperature And Pressure ◽  
Mild Temperature ◽  
Short Time ◽  
High Bulk ◽  
Dissolution And Precipitation

Calcium-deficient hydroxyapatite (CDHA) prepared by the coprecipitation method was solidified by the hydrothermal hot-pressing technique, and compacts of CDHA with high bulk density beyond 80% were obtained at 200 ℃. Each reaction parameter, viz. reaction temperature, pressure, and time, was systematically changed from the standard conditions to investigate its effects on density, Vickers hardness, and Ca/P ratio of the compacts obtained. The reaction temperature and pressure had a large effect on densification, but not the reaction time because the densification proceeds in a short time. The densification by hydrothermal hot-pressing involved dissolution and precipitation of the starting CDHA powder, so that the Ca/P ratio changed from 1.52 of the starting powders to 1.61 of the compact obtained by hydrothermal hot-pressing at 200 ℃ and 35 MPa for 24 h with the addition of 10 wt.-% water

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