Microshear bond strength of a flowable resin to enamel according to the different adhesive systems

SUMMARY Objectives: The aim of this study was to investigate the effect of different protocols of 17% ethylene diamine tetra-acetic acid (EDTA) conditioning on the etching pattern and immediate bond strength of universal adhesives to enamel and sclerotic dentin. Methods and Materials: Forty bovine teeth with sclerotic dentin and 20 human third molars were randomly divided into eight groups resulting from the combination of the main factors surface treatment (none, two-minute EDTA conditioning manual application, 30-second EDTA manual application, 30-second EDTA sonic application) and adhesives systems (Scotchbond Universal Adhesive [SBU] and Prime & Bond Elect [PBE]). Resin-dentin and enamel-dentin bond specimens were prepared and tested under the microtensile bond strength (μTBS) and microshear bond strength (μSBS) tests, respectively. The etching pattern produced on the unground enamel and the sclerotic dentin surfaces under the different protocols and adhesive systems was evaluated under scanning electron microscopy. Results: For enamel, only the main factor adhesive was significant (p<0.0001), with SBU showing the highest μSBS. In sclerotic dentin, the lowest mean was observed for the group without EDTA application and the highest mean in the group with EDTA application with the sonic device for 30 seconds. Regardless of the EDTA protocol, the highest means of μTBS were observed for SBU (p<0.05). Conclusions: EDTA conditioning improves the bonding performance of universal adhesives in the self-etch mode on sclerotic dentin, mainly when applied for 30 seconds with the aid of a sonic device. EDTA pretreatment also improves the retentive etching pattern of enamel, but it does not result in higher enamel bond strength.

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Microshear Bond Strength of Different Adhesive Systems to Dentin

Frontiers in Dentistry ◽

10.18502/fid.v16i4.2085 ◽

2019 ◽

Author(s):

Sara Valizadeh ◽

Aida Moradi ◽

Mansooreh Mirazei ◽

Hooman Amiri ◽

Mohammad Javad Kharazifard

Keyword(s):

Bond Strength ◽

Testing Machine ◽

Single Bond ◽

Adhesive Systems ◽

Etch And Rinse ◽

Significant Difference ◽

Microshear Bond Strength ◽

Self Etch ◽

Composite Cylinders

Objectives: The aim of this study was to compare the microshear bond strength (µSBS) of various adhesive systems to dentin. Materials and Methods: In this in vitro experimental study, 60 sound human third molars were divided into four groups. Dentin discs were prepared of middle-third dentin measuring 4 mm in diameter and 2 mm in thickness. Dentin surfaces were bonded with one of the four types of adhesives: (A) Single Bond (3M ESPE), Scotchbond Universal (3M ESPE) in etch and rinse (B) and self-etch (C) modes and (D) Clearfil SE Bond (Kuraray Noritake Dental). After the application of adhesive systems according to the manufacturers’ instructions, composite cylinders (Vit-l-escence) were bonded to dentin surfaces. The μSBS test was performed using a universal testing machine at a crosshead speed of 1 mm/min. Data were analyzed with one-way ANOVA and Tukey’s test (α=0.05). Results: The µSBS was the highest in self-etch Scotchbond Universal (15.8±6.08 MPa) followed by Clearfil SE Bond (15.24±4.6 MPa), etch and rinse Scotchbond Universal (11.68±4.07MPa) and Single Bond (11.24±3.74 MPa). A significant difference was only found between Single Bond and etch and rinse Scotchbond Universal groups (P=0.04). Conclusion: Based on the results of this study, application of Scotchbond Universal in self-etch mode provides a reliable bond to dentin.

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Microshear Bond Strength of Different Adhesive Systems to Dentin

Frontiers in Dentistry ◽

10.18502/fid.v14i4.2085 ◽

2019 ◽

Author(s):

Sara Valizadeh ◽

Aida Moradi ◽

Mansooreh Mirazei ◽

Hooman Amiri ◽

Mohammad Javad Kharazifard

Keyword(s):

Bond Strength ◽

Testing Machine ◽

Single Bond ◽

Adhesive Systems ◽

Etch And Rinse ◽

Significant Difference ◽

Microshear Bond Strength ◽

Self Etch ◽

Composite Cylinders

Objectives: The aim of this study was to compare the microshear bond strength (µSBS) of various adhesive systems to dentin. Materials and Methods: In this in vitro experimental study, 60 sound human third molars were divided into four groups. Dentin discs were prepared of middle-third dentin measuring 4 mm in diameter and 2 mm in thickness. Dentin surfaces were bonded with one of the four types of adhesives: (A) Single Bond (3M ESPE), Scotchbond Universal (3M ESPE) in etch and rinse (B) and self-etch (C) modes and (D) Clearfil SE Bond (Kuraray Noritake Dental). After the application of adhesive systems according to the manufacturers’ instructions, composite cylinders (Vit-l-escence) were bonded to dentin surfaces. The μSBS test was performed using a universal testing machine at a crosshead speed of 1 mm/min. Data were analyzed with one-way ANOVA and Tukey’s test (α=0.05). Results: The µSBS was the highest in self-etch Scotchbond Universal (15.8±6.08 MPa) followed by Clearfil SE Bond (15.24±4.6 MPa), etch and rinse Scotchbond Universal (11.68±4.07MPa) and Single Bond (11.24±3.74 MPa). A significant difference was only found between Single Bond and etch and rinse Scotchbond Universal groups (P=0.04). Conclusion: Based on the results of this study, application of Scotchbond Universal in self-etch mode provides a reliable bond to dentin.

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Comparative study of adhesive systems applied to different regions of dental substrate

Revista Odonto Ciência ◽

10.15448/1980-6523.2016.4.22482 ◽

2017 ◽

Vol 31 (4) ◽

pp. 158

Author(s):

Veridiana Camilotti ◽

Virgínia Bosquiroli ◽

Máx Dobrovolski ◽

Mario Alexandre Coelho Sinhoretic ◽

Priscilla Busatoa Do Monte Ribeiro ◽

...

Keyword(s):

Bond Strength ◽

Composite Resin ◽

Resin Composite ◽

Adhesive System ◽

Cervical Region ◽

Test Machine ◽

Adhesive Failure ◽

Adhesive Systems ◽

Type Analysis ◽

Microshear Bond Strength

OBJECTIVE: The aim of this study was to evaluate the bond strength (BS) of different self-etching adhesive systems to bovine dentin.METHODS: For this purpose, 50 teeth were flattened with silicon carbide abrasive papers and randomly divided into 5 groups: SB – Single Bond Plus; Group AEO – Adper Easy One; Group ADH – AdheSE; Group ASE – Adper SE Plus and Group Clear – Clear Fill. After adhesive system application, 5 Tygon cylinders (1.8 mm×2 mm) were placed on the vestibular surface of each tooth, filled with resin composite (Filtek Z350) and light activated. Three composite resin cylinders were fabricated for each bovine crown, one being located in the incisal region, one in the middle third and one in the cervical region, totaling 30 composite resin test specimens (TS) for each group. The TS were submitted to the microshear bond strength test in a Universal Test Machine Kratos), at a cross-head speed of 0.5 mm/min.RESULTS: The BS was calculated and analyzed by ANOVA (one-way) and Tukey’s test (p<0.05). The highest BS values were obtained in Group SB and there were no significant differences between the adhesive systems tested in the middle and cervical thirds. In the fracture type analysis it was found that adhesive failure was dominant for all groups.CONCLUSION: The conventional two-step adhesive system SB presented the highest bond strength mean to bovine dentin for all the regions.

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Effect of Chlorhexidine on Dentin Bond Strength of Two Adhesive Systems after Storage in Different Media

Brazilian Dental Journal ◽

10.1590/0103-6440201300159 ◽

2015 ◽

Vol 26 (6) ◽

pp. 642-647 ◽

Cited By ~ 4

Author(s):

Enio Marcos da Silva ◽

Daniel Hatschbach Glir ◽

Allana Walesca Martins Castanho Gill ◽

Allan Fernando Giovanini ◽

Adilson Yoshio Furuse ◽

...

Keyword(s):

Bond Strength ◽

Resin Composite ◽

Adhesive System ◽

Mineral Oil ◽

Time Interval ◽

Distilled Water ◽

Single Bond ◽

Storage Medium ◽

Adhesive Systems ◽

Microshear Bond Strength

The aim of this study was to evaluate the effect of 2% chlorhexidine (CHX) application during the bonding protocol on microshear bond strength of two adhesive systems, after storage in different media. Seventy-two human molars had their crowns cut in half and embedded in PVC cylinders with acrylic resin. The specimens were randomly divided into experimental groups (n=12) according to the adhesive system (Ambar and Single Bond 2), use of CHX in the bonding protocol, and time interval (24 h and 15 days) in the storage media (distilled water, mineral oil and 1% sodium hypochlorite - NaOCl). Adhesive systems were applied in accordance to manufacturers' recommendations, with or without the use of CHX, and resin composite (Z350 XT) cylinders were placed on the hybridized dentin. After photoactivation, the specimens were stored in distilled water, mineral oil and 1% NaOCl for 24 h and 15 days. Microshear bond strength was determined at a crosshead speed of 0.5 mm/min until fracture. The bond strength data were analyzed statistically by 4-way ANOVA and Tukey's test (α=5%). Use of CHX in the bonding protocol did not cause loss of bond strength in any of the evaluated situations, irrespective of time and storage medium. The storage medium had no influence on bond strength values after 15 days when the bond protocol without CHX application was used. However, the use of CHX in the protocol influenced negatively the bond strength values for Single Bond 2 after 15 days storage in distilled water and 1% NaOCl.

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CPP–ACP pretreatment effect on microshear bond strength of simplified etch-and-rinse adhesive systems plus a flowable composite to enamel

Journal of Adhesion Science and Technology ◽

10.1080/01694243.2014.976498 ◽

2014 ◽

Vol 29 (2) ◽

pp. 109-115

Author(s):

Diana Ferreira Gadelha de Araújo ◽

Boniek Castillo Dutra Borges ◽

Ariza Magalhães Mendes ◽

Eduardo José Souza-Junior ◽

Isauremi Vieira de Assunção ◽

...

Keyword(s):

Bond Strength ◽

Adhesive Systems ◽

Flowable Composite ◽

Pretreatment Effect ◽

Etch And Rinse ◽

Microshear Bond Strength

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Effect of Cigarette Smoke on Resin Composite Bond Strength to Enamel and Dentin Using Different Adhesive Systems

Operative Dentistry ◽

10.2341/15-056-l ◽

2016 ◽

Vol 41 (3) ◽

pp. E57-E63 ◽

Cited By ~ 3

Author(s):

JD Theobaldo ◽

A Catelan ◽

U Rodrigues-Filho ◽

GM Marchi ◽

DANL Lima ◽

...

Keyword(s):

Bond Strength ◽

Cigarette Smoke ◽

Resin Composite ◽

Single Bond ◽

Adhesive Systems ◽

Tooth Structure ◽

Composite Resin Restorations ◽

Microshear Bond Strength ◽

Intermediate Value ◽

Composite Restoration

SUMMARY Objective: To evaluate the microshear bond strength of composite resin restorations in dental blocks with or without exposure to cigarette smoke. Method: Eighty bovine dental blocks were divided into eight groups (n=10) according to the type of adhesive (Scotchbond Multi-Purpose, 3M ESPE, St Paul, MN, USA [SBMP]; Single Bond 2, 3M ESPE [SB]; Clearfil SE Bond, Kuraray Medical Inc, Okayama, Japan [CSEB]; Single Bond Universal, 3M ESPE [SBU]) and exposure to smoke (no exposure; exposure for five days/20 cigarettes per day). The adhesive systems were applied to the tooth structure, and the blocks received a composite restoration made using a matrix of perforated pasta. Data were statistically analyzed using analysis of variance and Tukey test (α<0.05). Results: For enamel, there was no difference between the presence or absence of cigarette smoke (p=0.1397); however, there were differences among the adhesive systems (p<0.001). CSEB showed higher values and did not differ from SBU, but both were statistically different from SB. The SBMP showed intermediate values, while SB demonstrated lower values. For dentin, specimens subjected to cigarette smoke presented bond strength values that were lower when compared with those not exposed to smoke (p<0.001). For the groups without exposure to cigarette smoke, CSEB showed higher values, differing from SBMP. SB and SBU showed intermediary values. For the groups with exposure to cigarette smoke, SBU showed values that were higher and statistically different from SB and CSEB, which presented lower values of bond strength. SBMP demonstrated an intermediate value of bond strength. Conclusion: The exposure of dentin to cigarette smoke influenced the bonding strength of adhesives, but no differences were noted in enamel.

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Effect of cpp-acp on the bond strength of silorane and methacrylate based restorative systems

Journal of Research in Dentistry ◽

10.19177/jrd.v1e1201364-71 ◽

2013 ◽

Vol 1 (1) ◽

pp. 64

Author(s):

Bruno de Castro Ferreira Barreto ◽

Anderson Catelan ◽

Marina Baptista Aleixo ◽

Gisele Rodrigues Silva ◽

Tathy Aparecida Xavier ◽

...

Keyword(s):

Bond Strength ◽

Hybrid Composites ◽

Resin Composite ◽

Testing Machine ◽

Adhesive Systems ◽

Universal Testing ◽

Significant Difference ◽

S Matrix ◽

Casein Phosphopeptide ◽

Microshear Bond Strength

This study evaluated the influence of the previous application of casein phosphopeptide amorphous calcium phosphate (CPP-ACP) on the bond strength of two restorative systems to dentin. Self-etching adhesive systems Clearfil SE Bond (Kuraray) and FiltekTM LS System Adhesive (3M ESPE) were used in combination with two micro-hybrid composites FiltekTM Z250 (3M ESPE) and FiltekTM LS (3M ESPE), respectively. Twenty-eight sound human third molars had the occlusal surface worn until the total exposure of dentin and were randomly divided into 4 groups (n = 7): G1 (Clearfil + Z250), G2 (CPP-ACP + Clearfil + Z250), G3 (LS system) and G4 (CPP-ACP + LS system). The application of the paste containing CPP-ACP was held in the dentin of G2 and G4 prior to adhesive protocol, which followed the manufacturer's recommendations. Two cylinders of a single increment of resin composite were built on each dentin surface using tygon`s matrix with 1.26 mm of diameter x 1 mm high and light-cured with LED Bluephase 16i (Vivadent) apparatus. Microshear bond strength test was conducted in a universal testing machine (EZ Test, Shimadzu) with a speed of 0.5 mm/min. The data were subjected to two-way ANOVA test with a significance of 5%. There was no significant difference on bond strength between restorative systems with or without the previous use of a CPP-ACP paste. It was concluded that the application of CPP-ACP in the dentin prior to adhesive protocol did not influence the bond strength of the restorative systems tested.

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Effect of water storage on microshear bond strength of four dental adhesive systems to dentin

Journal of Research in Dentistry ◽

10.19177/jrd.v3e22015626-635 ◽

2015 ◽

Vol 3 (2) ◽

pp. 626

Author(s):

Robinson Viegas Montenegro ◽

Hugo Lemes Carlo ◽

André Ulisses Dantas Batista ◽

Sheyla Christinne Lira Montenegro ◽

Ohana Rodrigues Farias

Keyword(s):

Bond Strength ◽

Water Storage ◽

Bivariate Analysis ◽

Single Bond ◽

Adhesive Systems ◽

Storage Material ◽

Dental Adhesive ◽

Tukey Test ◽

Microshear Bond Strength ◽

Storage Times

AIM: To evaluate the microshear bond strength of 4 dental adhesive systems after 1 year-water storage. MATERIAL AND METHODS: The sample consisted of 120 cylinders of composite, obtained from 24 bovine incisors, which were divided into four experimental groups: G1-Scotchbond Multi-Purpose, G2-Single Bond 2, G3-Clearfil SE Bond, G4-Adper Easy One and two storage times in distilled water: T0 - 24h and T1 - 1 year. A bivariate analysis was performed using the ANOVA and Tukey test (α=0.05). Results were evaluated inter-and intra-group in both times. RESULTS: After 24 hours, G1T0 (39.68A ± 11.55) showed higher bond strength (MPa) followed by G2T0 (22.71B ± 4.07), G3T0 (18.94BC ± 7.29) and G4T0 (13.30C ± 3.94). After 1 year of storage only G1T1 (33.95A ± 6.35) and G3T1 (13.59BC ± 2.63) maintained the bond strength values (p ≥ 0.05), while G2T1 (10.62C ± 4.32) and G4T1 (4.49D ± 2.49) presented a decrease in this values. CONCLUSION: The hydrophobic two-step adhesive systems maintained the bond strength after 1-year water storage.

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