Fiber Push-Out Nanoindentation Study of BN Interface in SIC/SIC Composites Exposed to High Temperatures

Author(s):  
Eric Jones ◽  
Sergey Yarmolenko ◽  
Jag Sankar
1997 ◽  
Vol 3 (S2) ◽  
pp. 733-734
Author(s):  
Mani Gopal

Silicon carbide (SiC) composites are receiving much attention for structural use at high temperatures. One class of composites are those reinforced with SiC fibers. The SiC fibers are coated with boron nitride (BN) which is weakly bonded to the fiber. During fracture, the coating deflects cracks causing pull-out of the fibers (Fig. 1). This process of fiber pull-out consumes energy and increases the toughness of the composite. Although much work has been done on characterizing these materials by SEM, not much has been done using TEM due to difficulties in specimen preparation. The purpose of this study is to characterize these fibers and composites using conventional and analytical TEM.In this study, TEM specimens were prepared by dimpling and ion milling. Careful control of the preparation was needed to ensure the integrity of the SiC-BN interface. Figure 2a is a TEM image of the fiber showing delamination at the SiC-BN interface.


2018 ◽  
Vol 9 (2) ◽  
pp. 147-160 ◽  
Author(s):  
Peter Schaumann ◽  
Inka Kleibömer

Purpose This paper deals with experimental and numerical investigations of the composite behaviour within concrete-filled tubular columns with embedded massive steel core (CFTES columns). As the inner profile provides the main load-bearing capacity, the load introduction and transfer is of particular interest for the structural detailing of CFTES columns. Currently, no specific design regulations are available – neither for room temperature nor fire design. The presented investigations provide a basis for design recommendations and numerical approaches on reliable shear stresses. Design/methodology/approach Three series of push-out tests at room temperature and high temperatures are analysed in terms of ultimate shear strength, bond strength and shear strength-displacement-curve shape. The test parameters involve the steel core diameter and concrete cover, applying normal strength steel and concrete. Furthermore, a three-dimensional finite element model of the push-out tests is set up in Abaqus. The model implies temperature-dependent contact properties derived from the experimental tests using the cohesive behaviour method. Findings The test data reveal a distinctive reduction in both ultimate shear and bond strength for high temperatures. For high temperatures, the thermal expansion coefficients dominate the composite behaviour. Using the 3D numerical model and applying a temperature-dependent joint stiffness, maximum shear stress criterion and damage evolution, the observed composite behaviour can be described in a realistic manner. Originality/value The presented experimental investigations are unique, both concerning the investigated column type and performing push-out tests at high temperatures. For the first time, a temperature-dependent reduction of capable shear stresses is identified, which is crucial for the design of structural components.


1996 ◽  
Vol 79 (12) ◽  
pp. 3065-3077 ◽  
Author(s):  
Mineo Mizuno ◽  
Shijie Zhu ◽  
Yasuo Nagano ◽  
Yoshihisa Sakaida ◽  
Yutaka Kagawa ◽  
...  

Author(s):  
Robin M. G. De Meyere ◽  
Kay Song ◽  
Louise Gale ◽  
Stephen Harris ◽  
Ian M. Edmonds ◽  
...  

AbstractTraditional fibre push-outs for the evaluation of interfacial properties in long fibre ceramic matrix composites present their limitations—solutions for which are addressed in this work by introducing the novel trench push-out test. The trench push-out makes use of a FIB milling system and an SEM in-situ nanoindenter to probe a fibre pushed into a trench underneath, allowing in-situ observations to be directly correlated with micromechanical events. SiCf/BN/SiC composites—candidate material for turbine engines—were used as model materials in this work. Different fibre types (Hi-Nicalon and Tyranno type SA3) were coated with BN interphases, presenting mean interfacial shear stresses of 14 ± 7 MPa and 20 ± 2 MPa, respectively, during fibre sliding. The micromechanical technique enabled visualisation of how defects in the interphase (voids, inclusions & milled notches) or in the fibre (surface asperities, non-uniform coatings) affected the variability of interfacial property measurement. Graphic abstract


2005 ◽  
Vol 75-79 ◽  
pp. 789-793 ◽  
Author(s):  
J.B.J. Hegeman ◽  
J.G. van der Laan ◽  
M. van Kranenburg ◽  
M. Jong ◽  
D. d’Hulst ◽  
...  

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