Consolidation of Aluminum Magnesium Boride (AlMgB14) by Pulsed Electric Current Sintering (PECS) Technique

Author(s):  
Nesredin Kedir ◽  
Gary Gilde ◽  
Kyu Cho
Crystals ◽  
2020 ◽  
Vol 10 (9) ◽  
pp. 823
Author(s):  
Alexander M. Grishin

We report optical and mechanical properties of hard aluminum magnesium boride films magnetron sputtered from a stoichiometric AlMgB14 ceramic target onto Corning® 1737 Glass and Si (100) wafers. High target sputtering rf-power and sufficiently short target-to-substrate distance appeared to be critical processing conditions. Amorphous AlMgB14 films demonstrate very strong indentation size effect (ISE): exceptionally high nanohardness H = 88 GPa and elastic Young’s modulus E* = 517 GPa at 26 nm of the diamond probe penetration depth and almost constant values, respectively, of about 35 GPa and 275 GPa starting at depths of about 2–3% of films’ thickness. For comparative analysis of elastic strain to failure index  H/E*, resistance to plastic deformation ratio H3/E*2 and elastic recovery ratio We were obtained in nanoindentation tests performed in a wide range of loading forces from 0.5 to 40 mN. High authentic numerical values of H = 50 GPa and E* = 340 GPa correlate with as low as only 10% of total energy dissipating through the plastic deformations.


2018 ◽  
Vol 43 (13) ◽  
pp. 3065 ◽  
Author(s):  
Hiroaki Furuse ◽  
Yuki Koike ◽  
Ryo Yasuhara

2016 ◽  
Vol 721 ◽  
pp. 419-424
Author(s):  
M. Erkin Cura ◽  
Vivek Kumar Singh ◽  
Panu Viitaharju ◽  
Joonas Lehtonen ◽  
Simo Pekka Hannula

Chromium oxide is a promising material for applications where excellent corrosion resistance, high hardness, and high wear resistance are needed. However, its use is limited because of low fracture toughness. Improvement of fracture toughness of chromium oxide while maintaining its afore mentioned key properties is therefore of high interest. In this communication we study the possibility of increasing the toughness of pulsed electric current sintered (PECS) chromium oxide by the addition of graphene oxide (GO). The indentation fracture toughness was improved markedly with the addition of graphene oxide. Materials prepared by direct chemical homogenization had better fracture toughness. In composites with 10 vol.% GO piling of thin graphene oxide layers resulted in the formation of graphite layers between Cr2O3 and in carbide formation, which were observed to be the main reasons for the degradation of the mechanical properties. The distribution of graphene oxide was more homogeneous, when the GO amount was 0.1 vol.% and the formation of graphitic layers were avoided due to lesser amount of GO as well as ultrasonic treatment following the ball milling.


2011 ◽  
Vol 509 (20) ◽  
pp. 5981-5987 ◽  
Author(s):  
Outi Söderberg ◽  
David Brown ◽  
Ilkka Aaltio ◽  
Jussi Oksanen ◽  
Jesse Syrén ◽  
...  

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