Atomic site correspondence and surface relief in the formation of plate-shaped transformation products

1994 ◽  
Vol 25 (9) ◽  
pp. 1917-1922 ◽  
Author(s):  
James M. Howe
Keyword(s):  
Surface Relief ◽  
Transformation Products ◽  
Atomic Site

Changes in the Structure of Steel during Quenching in a Magnetic Field

2020 ◽  
Vol 989 ◽  
pp. 79-84 ◽  
Author(s):  
Viktor N. Pustovoit ◽  
Yuri V. Dolgachev ◽  
L.P. Aref'eva
Keyword(s):  
Magnetic Field ◽  
Experimental Data ◽  
Martensitic Transformation ◽  
Specific Surface ◽  
Surface Area ◽  
Constant Magnetic Field ◽  
Surface Relief ◽  
Volumetric Strain ◽  
Transformation Products ◽  
Electron Microscopes

The structure of martensite obtained by quenching steel under the action of a constant magnetic field was studied. The kinetic changes of the martensitic transformation, caused by the action of a magnetic field, are expressed in the structure by an increase in the dispersity of the transformation products. Samples of steels C45, 100CrMn6 and 30HGSA were investigated. Dispersity was evaluated statistically in images obtained on light and electron microscopes. The specific surface area was measured and the parameters of the surface relief caused by martensitic transformation were studied. Experimental data show that after quenching in a magnetic field, a decrease in the volumetric strain of the transformation, an increase in the dispersity of packets of martensitic crystals and components of the packets are observed. It is concluded that an increase in dispersion and a fragmentation of the structure of martensite are mainly the result of multiplicative nucleation.

Granular bainite or granular ferrite? A preliminary TEM investigation of an HSLA-100 steel

1991 ◽  
Vol 49 ◽  
pp. 584-585
Author(s):  
R. Varughese ◽  
S. W. Thompson ◽  
P. R. Howell
Keyword(s):  
Room Temperature ◽  
Transformation Products ◽  
Accurate Description ◽  
Granular Bainite ◽  
Preliminary Results ◽  
The Past ◽  
Light Micrograph ◽  
Multiphase Reaction ◽  
Detailed Nature

Ever since Habraken and Economopoulos first employed the term granular bainite to classify certain unconventional transformation products in continuously cooled steels, the term has been widely accepted and used, despite the lack of a clear consensus as to the detailed nature of the transformation products which constitute granular bainite. This paper presents the preliminary results of a TEM investigation of an 0.04 wt% C, copper-containing steel (designated HSLA-100). It is suggested that the term granular ferrite rather than granular bainite is a more accurate description of this multiphase reaction product.Figure 1 is a light micrograph of a sample which had been air-cooled from 900°C to room temperature. The microstructure is typical of that which has been termed granular bainite in the past and appears to consist of equiaxed ferritic grains together with other minor transformation products. In order to examine these structures in more detail, both continuously cooled and isothermally transformed and quenched materials have been examined with TEM. Granular bainite has been found in virtually all samples.

X-ray Gabor holography

1995 ◽  
Vol 53 ◽  
pp. 612-613
Author(s):  
Steve Lindaas ◽  
Chris Jacobsen ◽  
Alex Kalinovsky ◽  
Malcolm Howells
Keyword(s):  
Surface Relief ◽  
Biological Imaging ◽  
Specimen Preparation ◽  
X Rays ◽  
X Ray ◽  
Water Window ◽  
Biological Objects ◽  
Transmission Imaging ◽  
Atomic Force ◽  
Electron Microscopes

Soft x-ray microscopy offers an approach to transmission imaging of wet, micron-thick biological objects at a resolution superior to that of optical microscopes and with less specimen preparation/manipulation than electron microscopes. Gabor holography has unique characteristics which make it particularly well suited for certain investigations: it requires no prefocussing, it is compatible with flash x-ray sources, and it is able to use the whole footprint of multimode sources. Our method serves to refine this technique in anticipation of the development of suitable flash sources (such as x-ray lasers) and to develop cryo capabilities with which to reduce specimen damage. Our primary emphasis has been on biological imaging so we use x-rays in the water window (between the Oxygen-K and Carbon-K absorption edges) with which we record holograms in vacuum or in air.The hologram is recorded on a high resolution recording medium; our work employs the photoresist poly(methylmethacrylate) (PMMA). Following resist “development” (solvent etching), a surface relief pattern is produced which an atomic force microscope is aptly suited to image.

Features of rolled billets milling and methods for its improvement

2020 ◽  
pp. 67-71
Author(s):  
M.Z. Pevzner ◽  
S.A. Smertin
Keyword(s):  
Surface Relief ◽  
Regression Dependence ◽  
Processing Mode ◽  
Hot Rolled

A model of the formation of the surface relief hiring milling of rolled billets and a method for selecting the milling mode based determining the regression dependence of the resulting relief on the processing mode are proposed. It is shown that the regulation of the processing mode as the tool wears out allows to increase the milling resource and productivity. Keywords hot rolled strips, milling, rolling, relic resistance, mill. [email protected]

scholarly journals Degradation Products of Polychlorinated Biphenyls and Their In Vitro Transformation by Ligninolytic Fungi

Toxics ◽  
2021 ◽  
Vol 9 (4) ◽  
pp. 81
Author(s):  
Kamila Šrédlová ◽  
Kateřina Šírová ◽  
Tatiana Stella ◽  
Tomáš Cajthaml
Keyword(s):  
Polychlorinated Biphenyls ◽  
Extracellular Enzymes ◽  
Degradation Products ◽  
Transformation Products ◽  
Irpex Lacteus ◽  
Chlorobenzoic Acid ◽  
Ligninolytic Fungi ◽  
Wide Range ◽  
Pcb Metabolites

Metabolites of polychlorinated biphenyls (PCBs)—hydroxylated PCBs (OH‑PCBs), chlorobenzyl alcohols (CB‑OHs), and chlorobenzaldehydes (CB‑CHOs)—were incubated in vitro with the extracellular liquid of Pleurotus ostreatus, which contains mainly laccase and low manganese-dependent peroxidase (MnP) activity. The enzymes were able to decrease the amount of most of the tested OH‑PCBs by > 80% within 1 h; the removal of more recalcitrant OH‑PCBs was greatly enhanced by the addition of the laccase mediator syringaldehyde. Conversely, glutathione substantially hindered the reaction, suggesting that it acted as a laccase inhibitor. Hydroxylated dibenzofuran and chlorobenzoic acid were identified as transformation products of OH‑PCBs. The extracellular enzymes also oxidized the CB‑OHs to the corresponding CB‑CHOs on the order of hours to days; however, the mediated and nonmediated setups exhibited only slight differences, and the participating enzymes could not be determined. When CB‑CHOs were used as the substrates, only partial transformation was observed. In an additional experiment, the extracellular liquid of Irpex lacteus, which contains predominantly MnP, was able to efficiently transform CB‑CHOs with the aid of glutathione; mono‑ and di-chloroacetophenones were detected as transformation products. These results demonstrate that extracellular enzymes of ligninolytic fungi can act on a wide range of PCB metabolites, emphasizing their potential for bioremediation.

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