Phase evolution studies of sol–gel derived lead zirconate titanate (PZT) nanopowder using X-ray diffraction and X-ray photoelectron spectroscopy

2011 ◽  
Vol 104 (1) ◽  
pp. 103-108 ◽  
Author(s):  
Anupama Sachdeva ◽  
Mahesh Kumar ◽  
Vandna Luthra ◽  
R. P. Tandon
Keyword(s):  
Lead Zirconate Titanate ◽  
Photoelectron Spectroscopy ◽  
Sol Gel ◽  
Phase Evolution ◽  
Lead Zirconate ◽  
X Ray Diffraction ◽  
X Ray ◽  
Zirconate Titanate

A Study on the Microstructure of Preferred Orientation of Lead Zirconate Titanate (PZT) Thin Films

1997 ◽  
Vol 12 (4) ◽  
pp. 1043-1047 ◽  
Author(s):  
Chang Jung Kim ◽  
Dae Sung Yoon ◽  
Joon Sung Lee ◽  
Chaun Gi Choi ◽  
Kwangsoo No
Keyword(s):  
Electron Microscopy ◽  
Thin Films ◽  
Lead Zirconate Titanate ◽  
Sol Gel ◽  
Lead Zirconate ◽  
Preferred Orientation ◽  
X Ray Diffraction ◽  
Pzt Thin Films ◽  
X Ray ◽  
Zirconate Titanate

The lead zirconate titanate (PZT) thin films were fabricated using sol-gel spin coating onto Pt/Ti/glass substrates. Effects of the holding time for pyrolysis and the coating cycle on the preferred orientation of the PZT thin films were studied. The films were fabricated with different coating cycles (3, 5, 7, 9, 11), dried at 330 °C for different holding times (5, 30, 60 min), and then annealed at the same temperature of 650 °C using rapid thermal annealing (RTA). The preferred orientations of the films were investigated using x-ray diffraction and glancing angle x-ray diffraction. The microstructure and the selected area diffraction pattern of the PZT thin films were also investigated using scanning electron microscopy (SEM) and transmission electron microscopy (TEM), respectively.

Contribution from Ferroelastic Domain Switching Detected Using X-ray Diffraction toR-Curves in Lead Zirconate Titanate Ceramics

2001 ◽  
Vol 84 (12) ◽  
pp. 2921-2929 ◽  
Author(s):  
Alexandre E. Glazounov ◽  
Hans Kungl ◽  
Jan-Thorsten Reszat ◽  
Michael J. Hoffmann ◽  
Arnd Kolleck ◽  
...  
Keyword(s):  
Lead Zirconate Titanate ◽  
Domain Switching ◽  
Lead Zirconate ◽  
X Ray Diffraction ◽  
X Ray ◽  
Zirconate Titanate ◽  
Titanate Ceramics

Time-resolved small angle X-ray scattering study of sol–gel precursor solutions of lead zirconate titanate and zirconia

2012 ◽  
Vol 369 (1) ◽  
pp. 184-192 ◽  
Author(s):  
Tomasz M. Stawski ◽  
Rogier Besselink ◽  
Sjoerd A. Veldhuis ◽  
Hessel L. Castricum ◽  
Dave H.A. Blank ◽  
...  
Keyword(s):  
Lead Zirconate Titanate ◽  
Small Angle ◽  
Sol Gel ◽  
Lead Zirconate ◽  
Time Resolved ◽  
X Ray ◽  
X Ray Scattering ◽  
Zirconate Titanate ◽  
Scattering Study ◽  
Ray Scattering

Direct observation of 90° domain switching in lead zirconate titanate thick films using x-ray diffraction

2007 ◽  
Vol 90 (26) ◽  
pp. 262905 ◽  
Author(s):  
Satoko Osone ◽  
Yoshiro Shimojo ◽  
Kyle Brinkman ◽  
Takashi Iijima ◽  
Keisuke Saito
Keyword(s):  
Direct Observation ◽  
Lead Zirconate Titanate ◽  
Domain Switching ◽  
Thick Films ◽  
Lead Zirconate ◽  
X Ray Diffraction ◽  
X Ray ◽  
Zirconate Titanate

Effects of Calcination Parameters on the Microstructure and Morphology of PZT Nanoparticles Prepared by Modified Sol–Gel Method

2012 ◽  
Vol 576 ◽  
pp. 326-329 ◽  
Author(s):  
Amid Shakeri ◽  
Hossein Abdizadeh ◽  
Mohammad Reza Golobostanfard
Keyword(s):  
Lead Zirconate Titanate ◽  
Sol Gel ◽  
Lead Zirconate ◽  
X Ray Diffraction ◽  
Gel Method ◽  
X Ray ◽  
Sol Gel Method ◽  
Treatment Conditions ◽  
Perovskite Type ◽  
Perovskite Type Structure

Lead zirconate titanate nanopowder Pb(Zr0.53Ti0.47)O3 (PZT) was prepared by modified sol-gel method with 1-propanol as solvent and acetylacetone as stabilizer. The microstructure and particle size measurements at different heat treatment conditions were characterized by field emission scanning electron microscopy and x-ray diffraction analysis. It was found that the PZT nanoparticles calcinated at 600 °C showed mean diameter of 75-125 nm with high crystallinity of perovskite-type structure.

Characterization of Lead Zirconate Titanate Powders Prepared by a Hydrothermal Method

2005 ◽  
Vol 902 ◽  
Author(s):  
Lingjuan Che ◽  
Yongping Ding ◽  
Jinrong Cheng ◽  
Chao Chen ◽  
Zhongyan Meng
Keyword(s):  
Electron Microscopy ◽  
Hydrothermal Method ◽  
Lead Zirconate Titanate ◽  
Fourier Transformation ◽  
Lead Zirconate ◽  
X Ray Diffraction ◽  
X Ray ◽  
Zirconate Titanate ◽  
Scanning Electron

AbstractLead Zirconate Titanate (PZT) powders have been synthesized by a hydrothermal method at the processing temperatures of 120-220 °C for 1.5-50 hours, based on the reaction of Pb(CH3COOH)2·3H2O, ZrOCl2·8H2O, Ti(C4H9O)4 and KOH. Hydrothermally treated PZT powders were characterized using X-ray diffraction (XRD), scanning electron microscopy (SEM), and Fourier transformation infrared (FTIR) techniques respectively. The influences of hydrothermal synthesize conditions on the crystalline structure and the morphology of PZT particles were investigated. Crystallized PZT powders could be synthesized at the KOH concentration of >2.5 mol/l.

Structural, Morphological and Thermal Decomposition Studies of Calcium and Hafnium Modified BaTiO3 Electro Ceramics

2021 ◽  
Author(s):  
Jude Fernandez ◽  
B Bindhu ◽  
M. Prabu ◽  
KY Sandhya
Keyword(s):  
Lead Zirconate Titanate ◽  
Sol Gel ◽  
Lead Zirconate ◽  
Ferroelectric Material ◽  
Tetragonal Symmetry ◽  
X Ray Diffraction ◽  
X Ray ◽  
Gel Combustion ◽  
Combustion Technique ◽  
P4mm Space Group

Abstract Calcium and hafnium co-doped barium titanate could be used as a replacement for lead zirconate titanate, which is a lead-based ferroelectric material. Solid state reaction accompanied by the usual sintering technique is the classical ceramic-processing method, which demands a lot of time and effort. The present work aims to make the process a lot easier and quicker by employing a modified sol-gel combustion technique to synthesize polycrystalline Ba0.85Ca0.15Ti(1-x)HfxO3 (x=0.00, 0.05, 0.10, 0.15) electro ceramics . The molar ration is fixed at 1:1 for metal and citric acid at pH ~ 1. It was found that Ba0.85Ca0.15Ti(1-x)HfxO3 (where x=0.00, 0.05, 0.10, 0.15) crystallizes completely at around 1000 °C which is much lower than traditional methods. The structure supposedly displays a tetragonal symmetry with the P4mm space group as confirmed through x-ray diffraction (XRD) and Raman spectroscopy.

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