Fatigue Crack Growth under High Pressure of Gaseous Hydrogen in a 15-5PH Martensitic Stainless Steel: Influence of Pressure and Loading Frequency

2012 ◽  
Vol 44 (3) ◽  
pp. 1320-1330 ◽  
Author(s):  
Z. Sun ◽  
C. Moriconi ◽  
G. Benoit ◽  
D. Halm ◽  
G. Henaff
Author(s):  
Giovambattista Bilotta ◽  
Mandana Arzaghi ◽  
Gilbert Hénaff ◽  
Guillaume Benoit ◽  
Clara Moriconi ◽  
...  

In this study, the effect of gaseous hydrogen on the fatigue crack growth behavior in a precipitation-hardened martensitic stainless steel is investigated. It is known that the degradation in fatigue crack growth behavior derives from a complex interaction between the fatigue damage and the amount of hydrogen enriching the crack tip, which is dependent on the hydrogen pressure, loading frequency, and stress intensity factor amplitude. Therefore, fatigue crack growth tests were performed in a range of 0.09 to 40 MPa under gaseous hydrogen at a frequency of 20 and 0.2 Hz. The fatigue data as well as fracture morphologies obtained so far indicate a sharp increase in crack growth rates in a narrow range of stress intensity factor amplitudes. Also, it is shown that by decreasing the loading frequency to 0.2 Hz at a given pressure of hydrogen the transition occurs at lower values of stress intensity factor amplitudes accompanied by a change in fracture mode. Scanning electron microscope (SEM) observations of the fracture surfaces are used to support the explanations proposed to account for the observed phenomena.


2018 ◽  
Vol 165 ◽  
pp. 03008
Author(s):  
Ashok Saxena ◽  
Kevin Nibur

The design of safe and low-cost, high-pressure hydrogen storage systems are a critical need for harnessing clean power but must consider the propensity of hydrogen to accelerate fatigue crack growth rates in the construction materials. Design of safe pressure vessels needs robust models for predicting crack growth rates and how they are affected by variables such as loading frequency, load ratios, hydrogen pressure, gaseous impurities, temperature, and material variability. In this study, fatigue crack growth rates were measured in the liner material in 10 MPa gaseous hydrogen at various load ratios, R, in the range -1 ≤ R ≤ 0.2. The effects of varying loading frequency were investigated, and the results were pooled with those from literature for similar alloys tested in 103 MPa gaseous hydrogen pressure. The differences in crack growth rates between H2 pressures of 10 to 103 MPa as well as the effects of frequency on the environment assisted crack growth rates were assessed. Loading frequency effects tend to saturate at frequencies of 1 Hz and less. H2 pressure effects appear to saturate at pressures of 45MPa, while load ratio effects are not significant for –1 ≤ R ≤ 0.2 but become important for R ≥ 0.2.


Author(s):  
Chris San Marchi ◽  
Joseph Ronevich ◽  
Paolo Bortot ◽  
Yoru Wada ◽  
John Felbaum ◽  
...  

Abstract The design of pressure vessels for high-pressure gaseous hydrogen service per ASME Boiler and Pressure Vessel Code Section VIII Division 3 requires measurement of fatigue crack growth rates in situ in gaseous hydrogen at the design pressure. These measurements are challenging and only a few laboratories in the world are equipped to make these measurements, especially in gaseous hydrogen at pressure in excess of 100 MPa. However, sufficient data is now available to show that common pressure vessel steels (e.g., SA-372 and SA-723) show similar fatigue crack growth rates when the maximum applied stress intensity factor is significantly less than the elastic-plastic fracture toughness. Indeed, the measured rates are sufficiently consistent that a master curve for fatigue crack growth in gaseous hydrogen can be established for steels with tensile strength less than 915 MPa. In this overview, published reports of fatigue crack growth rate data in gaseous hydrogen are reviewed. These data are used to formulate a two-part master curve for fatigue crack growth in high-pressure (106 MPa) gaseous hydrogen, following the classic power-law formulation for fatigue crack growth and a term that accounts for the loading ratio (R). The bounds on applicability of the master curve are discussed, including the relationship between hydrogen-assisted fracture and tensile strength of these steels. These data have been used in developing ASME VIII-3 Code Case 2938. Additionally, a phenomenological term for pressure can be added to the master curve and it is shown that the same master curve formulation captures the behavior of pressure vessel and pipeline steels at significantly lower pressure.


Author(s):  
Yoru Wada ◽  
Yusuke Yanagisawa

Autofrettage is used to known as an effective method to prevent fatigue crack propagation of thick-walled cylinder vessels operating under high pressure. Since low-alloy steel shows an enhanced crack growth rate in high-pressure gaseous hydrogen, this paper aims to validate the effect of autofrettage on crack growth behavior in high-pressure gaseous hydrogen utilizing 4%NiCrMoV steel (SA723 Gr3 Class2). An autofrettaged cylindrical specimen with a 70mm inside diameter and 111mm outside diameter was prepared with an axial EDM (depth of 1mm) notched on the inside surface. The measured residual stress profile coincides well with the calculated results. The fatigue crack growth test was conducted by pressurizing the cylinder and varying the external water pressure. Crack propagation from the EDM notch was observed in the non-autofrettaged cylindrical specimen while no crack propagation was observed when the initial EDM notch size was within the compressive residual stress field. When the initial EDM notch size was increased, the fatigue crack growth showed a narrow, groove-like fracture surface for the autofrettaged specimen. In order to qualitatively analyze those results, fatigue crack growth rates were examined under various load ratios including a negative load ratio using a fracture mechanics specimen. From the information obtained, crack growth analysis of an autofrettaged cylinder in a high-pressure hydrogen environment was successfully demonstrated with a fracture mechanics approach.


Author(s):  
Kazuhisa Matsumoto ◽  
Shinichi Ohmiya ◽  
Hideki Fujii ◽  
Masaharu Hatano

To confirm a compatibility of a newly developed high strength stainless steel “NSSC STH®2” for hydrogen related applications, tensile and fatigue crack growth properties were evaluated in high pressure hydrogen gas up to 90MPa. At temperatures between −40 and 85°C, no conspicuous deterioration of tensile properties including ductility was observed even in 90 MPa hydrogen gas at −40°C while strength of STH®2 was higher than SUS316L. Although a slight drop of reduction of area was recognized in one specimen tested in 90 MPa hydrogen gas at −40°C, caused by the segregation of Mn, Ni and Cu in the laboratory manufactured 15mm-thick plate, it was considerably improved in the large mill products having less segregation. Fatigue crack growth rates of STH®2 in high pressure hydrogen gas were almost the same as that of SUS316L in air. Although fatigue crack growth rate in air was considerably decelerated and lower than that in hydrogen gas at lower ΔK region, this was probably caused by crack closure brought by oxide debris formed on the fracture surfaces near the crack tip by the strong contact of the fracture surfaces after the fatigue crack was propagated. By taking the obtained results into account, it is concluded that NSSC STH®2 has excellent properties in high pressure hydrogen gas in addition to high strength compared with standard JIS SUS316L.


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