Re-refining of used lubricant oil by solvent extraction using central composite design method

2017 ◽  
Vol 34 (9) ◽  
pp. 2435-2444 ◽  
Author(s):  
Ghassan Rokan Daham ◽  
Adnan AbdulJabbar AbdulRazak ◽  
Adel Sharif Hamadi ◽  
Ayad Ahmed Mohammed
2021 ◽  
Vol 11 (1) ◽  
Author(s):  
Faraz Soltani ◽  
Hossna Darabi ◽  
Reza Aram ◽  
Mahdi Ghadiri

AbstractAn integrated hydrometallurgical process was used for the zinc leaching and purification from a zinc ore containing 9.75 wt% zinc. The zinc minerals in the ore were hemimorphite, willemite, and calcophanite. Main gangue minerals were quartz, goethite, hematite, and calcite. Central composite design (CCD) method was used to design leaching experiments and the optimum conditions were found as follows: 30% of solid fraction, 22.05% sulphuric acid concentration, and the leaching temperature of 45 °C. The PLS containing 35.07 g/L zinc, 3.16 g/L iron, and 4.58 g/L manganese impurities was produced. A special purification process including Fe precipitation and Zn solvent extraction was implemented. The results showed that after precipitation of iron, Zn extraction of 88.5% was obtained with the 2 stages extraction system composed of 30 vol% D2EHPA as extractant. The overall Zn recovery from the ore was 71.44%. Therefore, an appropriate solution containing 16.6 g/L Zn, 0.05 g/L Fe, and 0.11 g/L Mn was prepared for the electro-winning unit without using the roasting and calcination steps (conventional method), which result in environmental pollution.


2015 ◽  
Vol 9 (11) ◽  
pp. 68
Author(s):  
Widayat Widayat ◽  
Hadiyanto Hadiyanto ◽  
Bambang Cahyono ◽  
Ngadiwiyana Ngadiwiyana

The objective of this research was to obtain optimum condition of eugenol production from clove oil using a central composite design method. The main process occured in the eugenol production was saphonification and neutralization processes. In order to optimize these processes, the ratio of NaOH/clove oil and temperature were studied as design variables i.e. ratio of NaOH/clove oil=1:2.5-1:3.5 while temperature was varied between 40 and 60oC. The yield of eugenol was considered as the main response in of this experiment. The result showed that the optimum condition was achieved when the temperature and the ratio of NaOH/clove oil were 50oC and 2.75:1, respectively and the yield was 39.17%.<br />


2016 ◽  
Vol 17 (1) ◽  
pp. 36-43 ◽  
Author(s):  
Khaled Faidi ◽  
Noureddine Baaka ◽  
Saoussen Hammami ◽  
Ridha El Mokni ◽  
Zine Mighri ◽  
...  

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