Microfluidic-enabled ambient-temperature synthesis of ultrasmall bimetallic nanoparticles

Nano Research ◽  
2021 ◽  
Author(s):  
Huayi Shi ◽  
Bin Song ◽  
Runzhi Chen ◽  
Qiang Zhang ◽  
Guyue Hu ◽  
...  
Molbank ◽  
10.3390/m1250 ◽  
2021 ◽  
Vol 2021 (3) ◽  
pp. M1250
Author(s):  
Diana Becerra ◽  
Justo Cobo ◽  
Juan-Carlos Castillo

We report the ambient-temperature synthesis of novel (E)-N-(3-(tert-butyl)-1-methyl-1H-pyrazol-5-yl)-1-(pyridin-2-yl)methanamine 3 in 81% yield by a condensation reaction between 3-(tert-butyl)-1-methyl-1H-pyrazol-5-amine 1 and 2-pyridinecarboxaldehyde 2 in methanol using magnesium sulfate as a drying agent. The N-pyrazolyl imine 3 was full characterized by IR, 1D, and 2D NMR spectroscopy, mass spectrometry, and elemental analysis.


ACS Catalysis ◽  
2020 ◽  
Vol 10 (14) ◽  
pp. 7763-7772 ◽  
Author(s):  
Chao Xie ◽  
Jinliang Song ◽  
Manli Hua ◽  
Yue Hu ◽  
Xin Huang ◽  
...  

1999 ◽  
Vol 42 (1) ◽  
pp. 41-46 ◽  
Author(s):  
Fabio Zuluaga ◽  
Nora E. Valderruten ◽  
K. B. Wagener

2014 ◽  
Vol 43 (44) ◽  
pp. 16580-16583 ◽  
Author(s):  
P. Veeraraghavan Ramachandran ◽  
Hitesh Mistry ◽  
Ameya S. Kulkarni ◽  
Pravin D. Gagare

The presence of NH3 allows a high concentration, ambient temperature synthesis of ammonia borane from sodium borohydride in air using reagent-grade THF.


2013 ◽  
Vol 1 (3) ◽  
pp. 294-305 ◽  
Author(s):  
Sisini Sasidharan ◽  
Aswathy Jayasree ◽  
Sajid Fazal ◽  
Manzoor Koyakutty ◽  
Shantikumar V. Nair ◽  
...  

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