Synthesis and characterization of nanophase face-centered-cubic titanium

The stability constant Kf for the complexation of Ag(Ⅰ) metal ion with Midodrine hydrochloride were determinedby spectrophotometric method at room temperature .The colored complexes were measured at 300 nm. The stability constant of the complexes were found to be 5.47 by mole ratio method. The stoichiometry of the complexes formed between the Midodrine drug and Ag (Ⅰ) metal ion are 1:1 M/L ratio. Silver conjugated Midodrine hydrochloride Nano synthesized and characterized by UV/Visible spectroscopy, SEM, XRD and FT-IR. The UV/Visible spectra of Midodrine –Ag nanoparticle in the range of 322 nm. XRD conformThe crystallite size of Midodrine - Ag (Ⅰ) nanoparticles are found to be 64.5 nmfrom Debye Scherer formula.Thecrystallinity of nanoparticles is Face centered cubic structure. SEM conform of particle size and surface morphology, FTIR analyzed involvement of -NH2 group in Midodrine is the stabilized of silver nanoparticle. This research is focuses on complexation, Nano synthesis and characterization of Drug-silver nanoparticle for antihypotention therapy.

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Synthesis and Characterization of Silver Nanowires

Advanced Materials Research ◽

10.4028/www.scientific.net/amr.678.212 ◽

2013 ◽

Vol 678 ◽

pp. 212-216

Author(s):

Subbaiyan Sugapriya ◽

Rangarajalu Sriram ◽

Sriram Lakshmi

Keyword(s):

Silver Nanowires ◽

Synthesis And Characterization ◽

Face Centered Cubic ◽

Capping Agent ◽

X Ray Diffraction ◽

X Ray ◽

Transmission Electron ◽

Face Centered ◽

Fcc Structure

ABSTRACT Silver nanowires have been synthesized by polyol process with ethylene glycol as solvent and PVP as capping agent. The silver nanowires have been characterized by X-ray diffraction (XRD), Scanning electron microscopy (SEM), Energy-dispersive X-ray spectroscopy (EDX), and Transmission electron microscope (TEM) techniques. The prepared silver nanowires were found to exhibit face-centered cubic (fcc) structure. The diameter of the prepared silver nanowires have been found to lie in the range of 60 - 80 nm and the length of the wires have been observed to be in the range of 10-20 µm. The I-V characteristics have been carried out to study the conducting behavior of the prepared silver nanowires.

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Synthesis and Characterization of Ru Cubic Nanocages with a Face-Centered Cubic Structure by Templating with Pd Nanocubes

Nano Letters ◽

10.1021/acs.nanolett.6b02795 ◽

2016 ◽

Vol 16 (8) ◽

pp. 5310-5317 ◽

Cited By ~ 67

Author(s):

Ming Zhao ◽

Legna Figueroa-Cosme ◽

Ahmed O. Elnabawy ◽

Madeline Vara ◽

Xuan Yang ◽

...

Keyword(s):

Synthesis And Characterization ◽

Face Centered Cubic ◽

Cubic Structure ◽

Face Centered

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Synthesis and Characterization of Novel High Entropy Alloys

Materials Science Forum ◽

10.4028/www.scientific.net/msf.978.167 ◽

2020 ◽

Vol 978 ◽

pp. 167-173

Author(s):

Anil Kumar ◽

B. Vinith ◽

Aditya Kumar Choudhary ◽

Manoj Kumar Chopkar

Keyword(s):

Mechanical Alloying ◽

Synthesis And Characterization ◽

Mixing Enthalpy ◽

Valence Electron Concentration ◽

High Entropy Alloys ◽

Face Centered Cubic ◽

High Entropy ◽

Cubic Structure ◽

Face Centered

High entropy alloys (HEAs) generally exhibit either high resistance to deformation or high toughness due to the presence of body-centered or face-centered cubic structure, respectively. To overcome these limitations, new high entropy alloys have been developed in the present study. This investigation aims to synthesis and characterization of novel CoCrFeNi3Si, CoCrFe2Ni2Si, and Co2CrFeNi2Si high entropy alloys. The mechanical alloying route is used to synthesize these alloys. Grinding was carried out to 20h and X-ray diffraction (XRD) analysis was done at different time intervals of grinding. The face-centered cubic structure along with the intermetallic compound of Ni-Si was observed after 20h of grinding. Furthermore, a pseudo binary strategy based on the valence electron concentration and mixing enthalpy is also employed to design the high entropy alloys considered in the present study. Carefully analysis of the XRD pattern indicates that from 5 to 20h of mechanical alloying there is a decrement in the initial peaks of elements observed.

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Icosahedral Face-Centered Cubic Fe Nanoparticles: Facile Synthesis and Characterization with Aberration-Corrected TEM

Nano Letters ◽

10.1021/nl8037294 ◽

2009 ◽

Vol 9 (4) ◽

pp. 1572-1576 ◽

Cited By ~ 72

Author(s):

Tao Ling ◽

Lin Xie ◽

Jing Zhu ◽

Huimin Yu ◽

Hengqiang Ye ◽

...

Keyword(s):

Synthesis And Characterization ◽

Face Centered Cubic ◽

Facile Synthesis ◽

Fe Nanoparticles ◽

Face Centered ◽

Aberration Corrected

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Characterization of Cobalt Sulfide Thin Films Synthesized from Acidic Chemical Baths

Advances in Materials Science and Engineering ◽

10.1155/2020/2628706 ◽

2020 ◽

Vol 2020 ◽

pp. 1-9

Author(s):

Tizazu Abza ◽

Dereje Gelanu Dadi ◽

Fekadu Gashaw Hone ◽

Tesfaye Chebelew Meharu ◽

Gebremeskel Tekle ◽

...

Keyword(s):

Thin Films ◽

Crystallite Size ◽

Deposition Time ◽

Average Crystallite Size ◽

Cobalt Sulfide ◽

Face Centered Cubic ◽

X Ray Diffraction ◽

Electron Microscopic ◽

Face Centered

Cobalt sulfide thin films were synthesized from acidic chemical baths by varying the deposition time. The powder X-ray diffraction studies indicated that there are hexagonal CoS, face-centered cubic Co3S4, and cubic Co9S8 phases of cobalt sulfide. The crystallite size of the hexagonal CoS phase decreased from 52.8 nm to 22.5 nm and that of the cubic Co9S8 phase increased from 11 nm to 60 nm as the deposition time increased from 2 hrs to 3.5 hrs. The scanning electron microscopic images revealed crack and pinhole free thin films with uniform and smooth background and few large polygonal grains on the surface. The band gap of the cobalt sulfide thin films decreased from 1.75 eV to 1.3 eV as the deposition time increased from 2 hrs to 3.5 hrs. The photoluminescence (PL) spectra of the films confirmed the emission of ultraviolet, violet, and blue lights. The intense PL emission of violet light at 384 nm had red shifted with increasing deposition time that could be resulted from the increase in the average crystallite size. The FTIR spectra of the films indicated the presence of OH, C-O-H, C-O, double sulfide, and Co-S groups. As the deposition time increased, the electrical resistivity of the cobalt sulfide thin films decreased due to the increase in both the crystallite size and the films’ thickness.

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Photocatalytic Analysis and Characterization of Zn2SnO4 Nanoparticles Synthesized via Hydrothermal Method with Na2CO3 Mineralizer

Advanced Materials Research ◽

10.4028/www.scientific.net/amr.97-101.19 ◽

2010 ◽

Vol 97-101 ◽

pp. 19-22 ◽

Cited By ~ 2

Author(s):

Yu Shiang Wu ◽

Wen Ku Chang ◽

Min Jou

Keyword(s):

Photocatalytic Activity ◽

Hydrothermal Process ◽

Face Centered Cubic ◽

X Ray Diffraction ◽

Visible Absorption ◽

Transmission Electron ◽

Excellent Photocatalytic Activity ◽

Face Centered ◽

Xrd Patterns

Zinc stannate Zn2SnO4 (ZTO) nanoparticles were synthesized via a hydrothermal process utilizing sodium carbonate (Na2CO3) as a weak basic mineralizer. The samples were hydrothermally treated at 150, 200, and 250oC for 48 h. The X-ray diffraction (XRD) patterns show that the highly-crystalline ZTO nanostructure could be formed in a well-dispersed manner for the 250°C sample at a particle size of less than 50 nm. As determined from transmission electron microscopy (TEM) results, ZTO nanoparticles are face-centered cubic single crystals agglomerated together. The Raman spectra results showed that the ZTO nanocrystals have a spinel structure. Furthermore, photocatalytic activity was tested with methylene blue (MB) by UV irradiation. The ZTO synthesized by the 2 M Na2CO3 mineralizer at 250oC demonstrated excellent photocatalytic activity. The ZTO treated three different ways had three distinct UV-Visible absorption curves, which directly influences their corresponding photocatalytic activity.

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Synthesis and Characterization of Cobalt-Nickel Nanowires Formed under External Magnetic Field

Applied Mechanics and Materials ◽

10.4028/www.scientific.net/amm.799-800.120 ◽

2015 ◽

Vol 799-800 ◽

pp. 120-124 ◽

Cited By ~ 1

Author(s):

Mary Donnabelle L. Balela ◽

Lalaine M. Dulin ◽

Erica A. Garcia ◽

M. Janelle H. Tica

Keyword(s):

Magnetic Field ◽

External Magnetic Field ◽

Face Centered Cubic ◽

X Ray Diffraction ◽

X Ray ◽

Hexagonal Close Packed ◽

Cobalt Nickel ◽

Nickel Nanowires ◽

Face Centered

Cobalt-nickel (Co-Ni) nanowires were formed by electroless deposition in ethylene glycol under external magnetic field. The effects of initial Co (II) and Ni (II) concentration on the surface and morphology of the synthesized nanowires were investigated by x-ray diffraction (XRD) and scanning electron microscope (SEM) respectively. An increase in the Co (II) concentration resulted in increase in diameter of the nanowires. However, the length of nanowires was observed to decrease. Higher Co (II) concentration resulted in a mixture of hexagonal close-packed and face-centered cubic Co-Ni nanowires. X-ray diffraction revealed that crystal growth occurred when the nanowires are annealed at 653 K for 10h.

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Buerger precession camera and overall characterization of thin films and flat-plate crystals

Journal of Applied Crystallography ◽

10.1107/s0021889887086813 ◽

1987 ◽

Vol 20 (3) ◽

pp. 210-221 ◽

Cited By ~ 4

Author(s):

J.-L. Staudenmann ◽

R. D. Horning ◽

R. D. Knox

Keyword(s):

Flat Plate ◽

Structural Information ◽

Face Centered Cubic ◽

Si Substrates ◽

Bulk Growth ◽

Face Centered ◽

Non Destructive ◽

Growth Methods ◽

Stacking Disorder

A fast simple and non-destructive method is described to provide qualitative structural information for flat-plate crystals and epitaxically grown films. The technique, based upon the Buerger precession camera, produces an easy-to-interpret photograph of the reciprocal space of all the components at once: substrate, film or buffer layer, and/or superlattice. A wide variety of technologically important examples are used to illustrate the technique: a mixture of CdTe phases on (001) Si, an aluminium layer on a (001) Si substrate, (001) Ge epitaxic layers on (001) Si substrates, three combinations of possible orientations of CdTe epitaxic layers on various substrate types, CdTe/ZnTe and other II–VI superlattices on GaAs substrates. In addition, the precession pictures readily reveal the common [111] face-centered cubic twin fault, or stacking disorder, seen in bulk growth methods. This finding may have severe consequences for the electronic mobility and the feasibility of devices fabricated from these composite systems.

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