Determination of total safranal by in situ acid hydrolysis in supercritical fluid media: Application to the quality control of commercial saffron

2006 ◽  
Vol 578 (2) ◽  
pp. 117-121 ◽  
Author(s):  
Mohammed Zougagh ◽  
Angel Ríos ◽  
Miguel Valcárcel
2019 ◽  
Vol 219 ◽  
pp. 08003
Author(s):  
Maja Verstraeten

The SoLid Collaboration is currently operating a 1.6 ton neutrino detector near the Belgian BR2 reactor. Its main goal is the observation of the oscillation of electron antineutrinos to previously undetected flavour states. The highly segmented SoLid detector employs a compound scintillation technology based on PVT scintillator in combination with LiF-ZnS(Ag) screens containing the 6Li isotope. The experiment has demonstrated a channel-to-channel response that can be controlled to the level of a few percent, an energy resolution of better than 14% at 1 MeV, and a determination of the interaction vertex with a precision of 5 cm. This contribution highlights the major outcomes of the R&D program, the quality control during component manufacture and integration, the current performance and stability of the full-scale system, as well as the in-situ calibration of the detector with various radioactive sources.


Author(s):  
Evelio Teijón-López-Zuazo ◽  
Ángel Vega-Zamanillo ◽  
Miguel Ángel Calzada-Pérez ◽  
Luis Juli-Gándara

The construction of random fillings from the excavation of medium hardness rocks, with high particle sizes, presents limitations in compaction control. This research applies new control techniques with revised test procedures in the construction of the random fillings core, which constitutes the main part of the embankment, with the bigger volume and provides the geotechnical stability to the infrastructure. The maximum layer thickness researched was 800mm. As there are many types of rocks, this research is applied to metamorphic slates. Quality control has been carried out by applying new research associated with the revision of wheel impression test, topographic settlements and plate bearing test (PBT). A statistical analysis of the core of 16 slate random fillings has been carried out, with a total of 2250 in situ determination of density and moisture content, 75 wheel impression tests, 75 topographic settlement control and 75 PBT. The strong associations found between different tests have allowed to simplify the quality control.


Author(s):  
Bashar Alramahi ◽  
Dante Fratta ◽  
Khalid A. Alshibli

Soil density and moisture content are two essential properties in the quality control and quality assurance of projects that involve soil compaction. However, current field practices either are destructive and time-consuming (i.e., sand cone or water balloon for soil density and oven drying for moisture content) or include hazardous substances that require special handling and operating procedures (i.e., nuclear density gauge). Therefore, new robust, reliable, and nonnuclear techniques for the determination of in situ density and moisture content would assist in quality control and quality assurance processes and would allow more measurements to be performed in a shorter time. A methodology for the in situ determination of density and moisture content by using the propagation of elastic and electromagnetic waves through soils was evaluated. It is based on a semiempirical model that relates elastic wave velocity through soils to the water content, porosity, and degree of saturation. An experimental program was used to verify the model and examine its range of applicability. It was also used to examine the accuracy and limitations of the suggested methodology. An analysis was made of the experimental assessment, along with a detailed numerical study of the inversion procedure used to calculate the density and moisture content. Although the parametric and experimental study shows that the methodology can provide an estimate of density and water content rapidly and non-destructively, there are inherent accuracy and precision limitations that need to be solved. These results also show that combined elastic and electromagnetic wave propagation measurements can help in the development of a methodology that may assist in solving inconsistencies in stiffness measurements.


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