scholarly journals Feasibility of in situ controlled heat treatment (ISHT) of Inconel 718 during electron beam melting additive manufacturing

2017 ◽  
Vol 13 ◽  
pp. 156-165 ◽  
Author(s):  
W.J. Sames ◽  
K.A. Unocic ◽  
G.W. Helmreich ◽  
M.M. Kirka ◽  
F. Medina ◽  
...  
Author(s):  
A. Förner ◽  
J. Vollhüter ◽  
D. Hausmann ◽  
C. Arnold ◽  
P. Felfer ◽  
...  

AbstractMaterials processed by additive manufacturing often exhibit a very fine-scaled microstructures due to high cooling rates in the process. In this study, single-layer surface electron beam melting is used to create very high cooling rates similar to additive manufacturing processes to investigate the resulting microstructure. In the case of Nb-Si-Cr in-situ composites, a nano-scaled eutectic microstructure is beneficial for improving the mechanical and oxidational properties. Fast solidification results in the formation of supersaturated phases of Nbss and Cr2Nb with phase diameters down to 10 nm as well as in the stabilization of the metastable Nb9(Cr,Si)5 phase at room temperature. After processing with different solidification rates, the decomposition of the Nb9(Cr,Si)5 phase has been studied in detail with atom probe microscopy. The stabilization of mixed silicide phases by electron beam melting shows a new pathway for improving hardness and enhancing oxidation resistance of nanostructured eutectic in-situ composites, by which the inherent weaknesses of Nb-Si-Cr can be overcome without further alloying elements. Graphical Abstract


2016 ◽  
Vol 94 ◽  
pp. 17-27 ◽  
Author(s):  
Alejandro Hinojos ◽  
Jorge Mireles ◽  
Ashley Reichardt ◽  
Pedro Frigola ◽  
Peter Hosemann ◽  
...  

Materials ◽  
2021 ◽  
Vol 14 (13) ◽  
pp. 3603
Author(s):  
Tim Pasang ◽  
Benny Tavlovich ◽  
Omry Yannay ◽  
Ben Jakson ◽  
Mike Fry ◽  
...  

An investigation of mechanical properties of Ti6Al4V produced by additive manufacturing (AM) in the as-printed condition have been conducted and compared with wrought alloys. The AM samples were built by Selective Laser Melting (SLM) and Electron Beam Melting (EBM) in 0°, 45° and 90°—relative to horizontal direction. Similarly, the wrought samples were also cut and tested in the same directions relative to the plate rolling direction. The microstructures of the samples were significantly different on all samples. α′ martensite was observed on the SLM, acicular α on EBM and combination of both on the wrought alloy. EBM samples had higher surface roughness (Ra) compared with both SLM and wrought alloy. SLM samples were comparatively harder than wrought alloy and EBM. Tensile strength of the wrought alloy was higher in all directions except for 45°, where SLM samples showed higher strength than both EBM and wrought alloy on that direction. The ductility of the wrought alloy was consistently higher than both SLM and EBM indicated by clear necking feature on the wrought alloy samples. Dimples were observed on all fracture surfaces.


Metals ◽  
2021 ◽  
Vol 11 (2) ◽  
pp. 266
Author(s):  
Wakshum M. Tucho ◽  
Vidar Hansen

The widely adopted temperature for solid solution heat treatment (ST) for the conventionally fabricated Inconel 718 is 1100 °C for a hold time of 1 h or less. This ST scheme is, however, not enough to dissolve Laves and annihilate dislocations completely in samples fabricated with Laser metal powder bed fusion (L-PBF) additive manufacturing (AM)-Inconel 718. Despite this, the highest hardness obtained after aging for ST temperatures (970–1250 °C) is at 1100 °C/1 as we have ascertained in our previous studies. The unreleased residual stresses in the retained lattice defects potentially affect other properties of the material. Hence, this work aims to investigate if a longer hold time of ST at 1100 °C will lead to complete recrystallization while maintaining the hardness after aging or not. For this study, L-PBF-Inconel 718 samples were ST at 1100 °C at various hold times (1, 3, 6, 9, 16, or 24 h) and aged to study the effects on microstructure and hardness. In addition, a sample was directly aged to study the effects of bypassing ST. The samples (ST and aged) gain hardness by 43–49%. The high density of annealing twins evolved during 3 h of ST and only slightly varies for longer ST.


Materials ◽  
2021 ◽  
Vol 14 (15) ◽  
pp. 4317
Author(s):  
Thywill Cephas Dzogbewu ◽  
Willie Bouwer du Preez

TiAl-based intermetallic alloys have come to the fore as the preferred alloys for high-temperature applications. Conventional methods (casting, forging, sheet forming, extrusion, etc.) have been applied to produce TiAl intermetallic alloys. However, the inherent limitations of conventional methods do not permit the production of the TiAl alloys with intricate geometries. Additive manufacturing technologies such as electron beam melting (EBM) and laser powder bed fusion (LPBF), were used to produce TiAl alloys with complex geometries. EBM technology can produce crack-free TiAl components but lacks geometrical accuracy. LPBF technology has great geometrical precision that could be used to produce TiAl alloys with tailored complex geometries, but cannot produce crack-free TiAl components. To satisfy the current industrial requirement of producing crack-free TiAl alloys with tailored geometries, the paper proposes a new heating model for the LPBF manufacturing process. The model could maintain even temperature between the solidified and subsequent layers, reducing temperature gradients (residual stress), which could eliminate crack formation. The new conceptualized model also opens a window for in situ heat treatment of the built samples to obtain the desired TiAl (γ-phase) and Ti3Al (α2-phase) intermetallic phases for high-temperature operations. In situ heat treatment would also improve the homogeneity of the microstructure of LPBF manufactured samples.


Author(s):  
E.G. Astafurova ◽  
◽  
K.A. Reunova ◽  
S.V. Astafurov ◽  
M.Yu. Panchenko ◽  
...  

We investigated the phase composition, plastic deformation and fracture micromechanisms of Fe-(25-26)Cr-(5-12)Mn-0.15C-0.55N (wt. %) high-nitrogen chromium-manganese steel. Obtained by the method of electron-beam 3D-printing (additive manufacturing) and subjected to a heat treatment (at a temperature of 1150°C following by quenching). To establish the effect of the electron-beam 3D-printing process on the phase composition, microstructure and mechanical properties of high-nitrogen steel, a comparison was made with the data for Fe-21Cr-22Mn-0.15C-0.53N austenitic steel (wt. %) obtained by traditional methods (casting and heat treatment) and used as a raw material for additive manufacturing. It was experimentally established that in the specimens obtained by additive manufacturing method, depletion of the steel composition by manganese in the electron-beam 3D-printing and post-built heat treatment contributes to the formation of a macroscopically and microscopically inhomogeneous two-phase structure. In the steel specimens, macroscopic regions of irregular shape with large ferrite grains or a two-phase austenite-ferrite structure (microscopic inhomogeneity) were observed. Despite the change in the concentration of the basic elements (chromium and manganese) in additive manufacturing, a high concentration of interstitial atoms (nitrogen and carbon) remains in steel. This contributes to the macroscopically heterogeneous distribution of interstitial atoms in the specimens - the formation of a supersaturated interstitial solid solution in the austenitic regions due to the low solubility of nitrogen and carbon in the ferrite regions. This inhomogeneous heterophase (ferrite-austenite) structure has high strength properties, good ductility and work hardening, which are close to those of the specimens of the initial high-nitrogen austenitic steel used as the raw material for additive manufacturing.


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