scholarly journals TiO2 nanocrystals grafted on macroporous silica: A novel hybrid organic–inorganic sol–gel approach for the synthesis of highly photoactive composite material

2011 ◽  
Vol 104 (3-4) ◽  
pp. 282-290 ◽  
Author(s):  
Maurizio Crippa ◽  
Emanuela Callone ◽  
Massimiliano D’Arienzo ◽  
Klaus Müller ◽  
Stefano Polizzi ◽  
...  
2020 ◽  
Vol 854 ◽  
pp. 45-50
Author(s):  
Ekaterina N. Gubareva ◽  
Valeria V. Strokova ◽  
Yulia N. Ogurtsova ◽  
Pavel S. Baskakov ◽  
Lok Pratap Singh

The paper presents the process of sol-gel synthesis of titanium dioxide nanoparticles, the peculiarities of the influence of component composition (titanium precursor content, solvent and stabilizer − surfactant) on the properties of sol and powder obtained on its basis. As a result of the study, the nature of the influence of the type and content of the surfactant in the solution of tetrabutoxytitanium in ethanol on the size of the synthesized particles of titanium dioxide was revealed. The optimal composition of the reaction mixture of TiO–R sol was obtained and the optimal ratio of tetrabutoxytitanium and ethyl alcohol was revealed using which a material with a high content of nanosized titanium dioxide was obtained.


2015 ◽  
Vol 2015 ◽  
pp. 1-8 ◽  
Author(s):  
Magdalena Streckova ◽  
Radovan Bures ◽  
Maria Faberova ◽  
Pavel Kurek ◽  
Pavla Roupcova ◽  
...  

A design of the novel microcomposite material composed of spherical FeSi particles and Mn0.8Zn0.2Fe2O4ferrite is reported together with a characterization of basic mechanical and electrical properties. The sol-gel autocombustion method was used for a preparation of Mn0.8Zn0.2Fe2O4ferrite, which has a spinel-type crystal structure as verified by XRD and TEM analysis. The final microcomposite samples were prepared by a combination of the traditional PM compaction technique supplemented with unconventional microwave sintering process of the prepared green compacts. The composition and distribution of the secondary phase formed by the spinel ferrite were examined by SEM. It is demonstrated that the prepared composite material has a tight arrangement without any significant porosity, which manifests itself through superior mechanical properties (high mechanical hardness, Young modulus, and transverse rupture strength) and specific electric resistivity compared to the related composite materials including resin as the organic binder.


1994 ◽  
Vol 29 (15) ◽  
pp. 4075-4080 ◽  
Author(s):  
S. M. Jones ◽  
S. E. Friberg ◽  
J. Sjöblom

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