Adjusted blank correction method for UV–vis spectroscopic analysis of PTIO-coated filters used in nitrogen oxide passive samplers

2009 ◽  
Vol 43 (10) ◽  
pp. 1823-1826 ◽  
Author(s):  
Cindy DeForest Hauser ◽  
Paul Battle ◽  
Nina Mace
Keyword(s):  
Nitrogen Oxide ◽  
Spectroscopic Analysis ◽  
Correction Method ◽  
Passive Samplers ◽  
Blank Correction

scholarly journals A NEW RAMPED PYROXIDATION/COMBUSTION FACILITY AT 14CHRONO, BELFAST: SETUP DESCRIPTION AND INITIAL RESULTS

Radiocarbon ◽  
2021 ◽  
pp. 1-14
Author(s):  
Evelyn M Keaveney ◽  
Gerard T Barrett ◽  
Kerry Allen ◽  
Paula J Reimer
Keyword(s):  
Bulk Material ◽  
Correction Method ◽  
Source Attribution ◽  
Radiocarbon Age ◽  
Targeted Analysis ◽  
Consensus Values ◽  
Background Material ◽  
Initial Results ◽  
Blank Correction ◽  
Good Agreement

ABSTRACT The Belfast Ramped Pyroxidation/Combustion (RPO/RC) facility was established at the 14CHRONO Centre (Queen’s University Belfast). The facility was created to provide targeted analysis of bulk material for refined chronological analysis and carbon source attribution for a range of sample types. Here we report initial RPO results, principally on background material, but also including secondary standards that are routinely analyzed at 14CHRONO. A description of our setup, methodology, and background (blank) correction method for the system are provided. The backgrounds (anthracite, spar calcite, Pargas marble) reported by the system are in excess of 35,000 14C years BP with a mean age of 39,345 14C years BP (1σ = 36,497–43,800 years BP, N=44) with F14C = 0.0075 ± 0.0032. Initial results for standards are also in good agreement with consensus values: TIRI-B pine radiocarbon age = 4482 ± 47 years BP (N=13, consensus = 4508 years BP); IAEA-C6 ANU Sucrose F14C= 1.5036 ± 0.0034 (N=10, consensus F14C = 1.503). These initial tests have allowed problematic issues to be identified and improvements made for future analyses.

scholarly journals A Dynamic Data Correction Method for Enhancing Resolving Power of Integrated Spectra in Spectroscopic Analysis

2020 ◽  
Vol 92 (19) ◽  
pp. 12763-12768
Author(s):  
Chih-Hao Hsiao ◽  
Yin-Hung Lai ◽  
Shu-Yun Kuo ◽  
Yi-Hong Cai ◽  
Cheng-Huang Lin ◽  
...  
Keyword(s):  
Spectroscopic Analysis ◽  
Correction Method ◽  
Resolving Power ◽  
Dynamic Data ◽  
Data Correction

Characterization of Chemical Impurities in Glutaraldehyde

1975 ◽  
Vol 33 ◽  
pp. 620-621
Author(s):  
B. J. Grenon ◽  
A. J. Tousimis
Keyword(s):  
Glutaric Acid ◽  
Spectroscopic Analysis ◽  
Aldol Condensation ◽  
Condensation Product ◽  
Amorphous Solid ◽  
Water Soluble ◽  
Impurity Component ◽  
Chemical Impurities ◽  
Soluble Liquid

Ever since the introduction of glutaraldehyde as a fixative in electron microscopy of biological specimens, the identification of impurities and consequently their effects on biologic ultrastructure have been under investigation. Several reports postulate that the impurities of glutaraldehyde, used as a fixative, are glutaric acid, glutaraldehyde polymer, acrolein and glutaraldoxime.Analysis of commercially available biological or technical grade glutaraldehyde revealed two major impurity components, none of which has been reported. The first compound is a colorless, water-soluble liquid with a boiling point of 42°C at 16 mm. Utilizing Nuclear Magnetic Resonance (NMR) spectroscopic analysis, this compound has been identified to be — dihydro-2-ethoxy 2H-pyran. This impurity component of the glutaraldehyde biological or technical grades has an UV absorption peak at 235nm. The second compound is a white amorphous solid which is insoluble in water and has a melting point of 80-82°C. Initial chemical analysis indicates that this compound is an aldol condensation product(s) of glutaraldehyde.

Elemental analysis of human erythrocytes

1989 ◽  
Vol 47 ◽  
pp. 242-243
Author(s):  
S. A. Livesey ◽  
A. A. del Campo ◽  
E. S. Griffey ◽  
D. Ohlmer ◽  
T. Schifani ◽  
...  
Keyword(s):  
Sample Preparation ◽  
Elemental Analysis ◽  
Human Erythrocyte ◽  
Spectroscopic Analysis ◽  
Model System ◽  
Human Erythrocytes ◽  
List Type ◽  
Chemical Fixation ◽  
Ethanol Dehydration ◽  
Lowicryl K4m

The aim of this study is to compare methods of sample preparation for elemental analysis. The model system which is used is the human erythrocyte. Energy dispersive spectroscopic analysis has been previously reported for cryofixed and cryosectioned erythrocytes. Such work represents the reference point for this study. The use of plastic embedded samples for elemental analysis has also been documented. The work which is presented here is based on human erythrocytes which have been either chemically fixed and embedded or cryofixed and subsequently processed by a variety of techniques which culminated in plastic embedded samples.Heparinized and washed erythrocytes were prepared by the following methods for this study :(1). Chemical fixation in 4% paraformaldehyde/0.25% glutaraldehyde/0.2 M sucrose in 0.1 M Na cacodylate, pH 7.3 for 30 min, followed by ethanol dehydration, infiltration and embedding in Lowicryl K4M at -20° C.

Ortho-k lenses fitting in patients with “non-typical” corneas

The Eye ◽  
2020 ◽  
Vol 22 (129) ◽  
pp. 22-29
Author(s):  
Svetlana Kravchuk ◽  
Olga Zhabina
Keyword(s):  
Correction Method ◽  
Diameter Ratio ◽  
Corneal Curvature ◽  
Individual Approach ◽  
Fitting In ◽  
Corneal Diameter ◽  
Clinical Cases

We described two clinical cases of ortho-k lenses fitting in patients with “non-typical” corneal curvature/diameter ratio. The main goal was to acknowledge effective and safe use of this myopia correction method in patients with corneal diameter greater than 11 mm. Individual approach to each patient is the key to a successful and safe ortho-k lenses fitting.

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