The influence of heat treatment on fracture surface morphology of the CuAlNi shape memory alloy

2017 ◽  
Vol 77 ◽  
pp. 85-92 ◽  
Author(s):  
Ivana Ivanić ◽  
Stjepan Kožuh ◽  
Franc Kosel ◽  
Borut Kosec ◽  
Ivan Anžel ◽  
...  
2020 ◽  
Vol 405 ◽  
pp. 100-106
Author(s):  
Ivana Ivanić ◽  
Mirko Gojić ◽  
Stjepan Kožuh ◽  
Borut Kosec

The paper presents comparison of microstructure and fracture surface morphology of the CuAlNi shape memory alloy (SMA) after different heat treatment procedures. The investigation was performed on samples in as-cast state and heat treated states (solution annealing at temperatures of 850 °C / 60’ / H2O and 920 °C / 60’ / H2O along with tempering at two different temperature 150 °C / 60’ / H2O and 300 °C / 60’ / H2O). The microstructure of the samples was examined by optical (OM) and scanning electron microscope (SEM) equipped with device for EDS analysis. The obtained fracture surfaces were examined by SEM. Optical and scanning electron microscopy showed martensitic microstructure in all investigated samples. However, the fractographic analysis of samples after tensile testing reveals significant changes in fracture mechanism. In both solution annealed states the results shows transgranular type of fracture, but after tempering at two different temperatures the difference is obvious. After tempering at 150 °C, along with transgranular type of fracture appear some areas with intergranular type of fracture. After tempering at 300 °C, fracture surface reveals completely intergranular type of fracture.


2021 ◽  
Vol 39 (2A) ◽  
pp. 196-205
Author(s):  
Zainab M. Abdul Monem ◽  
Jawad K. Oleiwi ◽  
Qahtan A. Hamad

In the current Research , the heat cured   matrix material powder of PMMA was reinforced with peanut and walnut shells (natural powders) which are chemically treated with 5% (w/v) (NaOH) to improve the matrix bonding (PMMA) before being used as a reinforcing powder and adding to exactly similar averages particle sizes ≤ (53µm), with different weight fractions of (4, 8, and 12 wt.%). The ASTM D638 is used for composite specimens of the tensile test. The results indicated that the Elastic modulus values reached its maximum value at (8 wt.%.) when reinforced with peanut shells particles (1.053Gpa) , while ,the values of tensile strength, elongation percentage at break, decrease as the weight fraction of peanut and walnut shells powder increase and the lowest values is obtained by reinforcing with peanut shells particles to reach their minimum values at (12 wt.%.) where the lowest values of them are (29 MPa, 2.758% ) respectively. The fracture surface morphology of pure PMMA seemed to be homogenous morphology in (SEM) test, whereas the fracture surface morphology of PMMA composite reinforced by (peanut and walnut shells) powders and shows a roughness fracture surface morphology this refer to semi ductile to ductile materials.


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