Mechanical properties, structural and texture evolution of biocompatible Ti–45Nb alloy processed by severe plastic deformation

Author(s):  
Ajit Panigrahi ◽  
Bartosz Sulkowski ◽  
Thomas Waitz ◽  
Kadir Ozaltin ◽  
Witold Chrominski ◽  
...  
Materials ◽  
2019 ◽  
Vol 12 (6) ◽  
pp. 1001 ◽  
Author(s):  
Xi Zhao ◽  
Shuchang Li ◽  
Yong Xue ◽  
Zhimin Zhang

Annular channel angular extrusion has been recently developed as a new single-pass severe plastic deformation method suitable for producing large size cup-shaped parts from cylindrical billets. In this study, the novel technology was successfully applied to commercial AZ80 Mg alloy at 300 °C, and microstructure, texture evolution, and mechanical properties were investigated. Due to severe shear deformation, the initial microstructure, including the coarse grains and large eutectic β-phases, was greatly refined. The strong basal texture formed during the initial deformation stage was modified into a weak tilted dynamic texture. During the deformation process, fine β-particles separated from eutectic phases effectively hindered the grain boundary migration and rotation, enhancing the grain refinement and texture weakening. More than 63% of the microhardness increase was achieved in this extruded part. Also, tensile tests showed the yield strength and elongation in both directions (transverse and longitudinal) of extruded part were improved more than 2.5 times, and the ultimate tensile strength was improved more than 2 times, compared to the initial material state. The improved material properties were mainly attributed to microstructure (grain and phase) refinement and texture weakening. It was demonstrated that the annular channel angular extrusion process can be considered as a novel and effective single-pass severe plastic deformation method.


2018 ◽  
Vol 1 (1) ◽  
pp. 77-90
Author(s):  
Walaa Abdelaziem ◽  
Atef Hamada ◽  
Mohsen A. Hassan

Severe plastic deformation is an effective method for improving the mechanical properties of metallic alloys through promoting the grain structure. In the present work, simple cyclic extrusion compression technique (SCEC) has been developed for producing a fine structure of cast Al-1 wt. % Cu alloy and consequently enhancing the mechanical properties of the studied alloy. It was found that the grain structure was significantly reduced from 1500 µm to 100 µm after two passes of cyclic extrusion. The ultimate tensile strength and elongation to failure of the as-cast alloy were 110 MPa and 12 %, respectively. However, the corresponding mechanical properties of the two pass CEC deformed alloy are 275 MPa and 35%, respectively. These findings ensure that a significant improvement in the grain structure has been achieved. Also, cyclic extrusion deformation increased the surface hardness of the alloy by 49 % after two passes. FE-simulation model was adopted to simulate the deformation behavior of the material during the cyclic extrusion process using DEFORMTM-3D Ver11.0. The FE-results revealed that SCEC technique was able to impose severe plastic strains with the number of passes. The model was able to predict the damage, punch load, back pressure, and deformation behavior.


Materials ◽  
2021 ◽  
Vol 14 (13) ◽  
pp. 3467
Author(s):  
Anna Nocivin ◽  
Doina Raducanu ◽  
Bogdan Vasile ◽  
Corneliu Trisca-Rusu ◽  
Elisabeta Mirela Cojocaru ◽  
...  

The present paper analyzed the microstructural characteristics and the mechanical properties of a Ti–Nb–Zr–Fe–O alloy of β-Ti type obtained by combining severe plastic deformation (SPD), for which the total reduction was of etot = 90%, with two variants of super-transus solution treatment (ST). The objective was to obtain a low Young’s modulus with sufficient high strength in purpose to use the alloy as a biomaterial for orthopedic implants. The microstructure analysis was conducted through X-ray diffraction (XRD), scanning electron microscopy (SEM), and high-resolution transmission electron microscopy (HRTEM) investigations. The analyzed mechanical properties reveal promising values for yield strength (YS) and ultimate tensile strength (UTS) of about 770 and 1100 MPa, respectively, with a low value of Young’s modulus of about 48–49 GPa. The conclusion is that satisfactory mechanical properties for this type of alloy can be obtained if considering a proper combination of SPD + ST parameters and a suitable content of β-stabilizing alloying elements, especially the Zr/Nb ratio.


Materials ◽  
2020 ◽  
Vol 13 (24) ◽  
pp. 5834
Author(s):  
Chi Zhang ◽  
Laszlo S. Toth

During severe plastic deformation (SPD), there is usually extended grain fragmentation, associated with the formation of a crystallographic texture. The effect of texture evolution is, however, coarsening in grain size, as neighbor grains might coalesce into one grain by approaching the same ideal orientation. This work investigates the texture-induced grain coarsening effect in face-centered cubic polycrystals during simple shear, in 3D topology. The 3D polycrystal aggregate was constructed using a cellular automaton model with periodic boundary conditions. The grains constituting the polycrystal were assigned to orientations, which were updated using the Taylor polycrystal plasticity approach. At the end of plastic straining, a grain detection procedure (similar to the one in electron backscatter diffraction, but in 3D) was applied to detect if the orientation difference between neighboring grains decreased below a small critical value (5°). Three types of initial textures were considered in the simulations: shear texture, random texture, and cube-type texture. The most affected case was the further shearing of an initially already shear texture: nearly 40% of the initial volume was concerned by the coalescence effect at a shear strain of 4. The coarsening was less in the initial random texture (~30%) and the smallest in the cube-type texture (~20%). The number of neighboring grains coalescing into one grain went up to 12. It is concluded that the texture-induced coarsening effect in SPD processing cannot be ignored and should be taken into account in the grain fragmentation process.


2010 ◽  
Vol 667-669 ◽  
pp. 253-258
Author(s):  
Wei Ping Hu ◽  
Si Yuan Zhang ◽  
Xiao Yu He ◽  
Zhen Yang Liu ◽  
Rolf Berghammer ◽  
...  

An aged Al-5Zn-1.6Mg alloy with fine η' precipitates was grain refined to ~100 nm grain size by severe plastic deformation (SPD). Microstructure evolution during SPD and mechanical behaviour after SPD of the alloy were characterized by electron microscopy and tensile, compression as well as nanoindentation tests. The influence of η' precipitates on microstructure and mechanical properties of ultrafine grained Al-Zn-Mg alloy is discussed with respect to their effect on dislocation configurations and deformation mechanisms during processing of the alloy.


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