Tailoring the microstructure and the mechanical properties of ultrafine grained high strength ferritic steels by powder metallurgy

2015 ◽  
Vol 465 ◽  
pp. 54-62 ◽  
Author(s):  
B. Mouawad ◽  
X. Boulnat ◽  
D. Fabrègue ◽  
M. Perez ◽  
Y. de Carlan
2014 ◽  
Vol 794-796 ◽  
pp. 851-856
Author(s):  
Tadashiege Nagae ◽  
Nobuhiro Tsuji ◽  
Daisuke Terada

Accumulative roll-bonding (ARB) process is one of the severe plastic deformation processes for fabricating ultrafine grained materials that exhibit high strength. In aluminum alloys, aging heat treatment has been an important process for hardening materials. In order to achieve good mechanical properties through the combination of grain refinement hardening and precipitation hardening, an Al-4.2wt%Ag binary alloy was used in the present study. After a solution treatment at 550°C for 1.5hr, the alloy was severely deformed by the ARB process at room temperature (RT) up to 6 cycles (equivalent strain of 4.8). The specimens ARB-processed by various cycles (various strains) were subsequently aged at 100, 150, 200, 250°C, and RT. The hardness of the solution treated (ST) specimen increased by aging. On the other hand, hardness of the ARB processed specimen decreased after aging at high temperatures such as 250°C. This was probably due to coarsening of precipitates or/and matrix grains. The specimen aged at lower temperature showed higher hardness. The maximum harnesses achieved by aging for the ST specimen, the specimens ARB processed by 2 cycles, 4 cycles and 6 cycles were 55HV, 71HV, 69HV and 65HV, respectively. By tensile tests it was shown that the strength increased by the ARB process though the elongation decreased significantly. However, it was found that the tensile elongation of the ARB processed specimens was improved by aging without sacrificing the strength. The results suggest that the Al-Ag alloy having large elongation as well as high strength can be realized by the combination of the ARB process for grain refinement and the subsequent aging for precipitation hardening.


1998 ◽  
Vol 553 ◽  
Author(s):  
A. Inoue ◽  
H. M. Kimura

AbstractBy the control of composition, clustered atomic configuration and stability of the supercooled liquid in the rapid solidification and powder metallurgy processes, high-strength Al-based bulk alloys containing nanoscale nonperiodic phases were produced in AI-Ln-LTM, AI-ETM-LTM and Al-(V, Cr, Mn)-LTM (Ln=lanthanide metal, LTM=VII and VIII group metals, ETM=IV to VI group metals) alloys containing high Al contents of 92 to 95 at%. The nonperiodic phases are composed of amorphous or icosahedral (I) phase. In particular, the Al-based bulk alloys consisting of nanoscale I particles surrounded by Al phase exhibit much better mechanical properties as compared with commercial Al base alloys. The success of producing the Al-based alloys with good engineering properties by use of I phase is important for future development of I-based alloys as practical materials.


2016 ◽  
Vol 879 ◽  
pp. 145-150
Author(s):  
Kei Ameyama ◽  
Sanjay Kumar Vajpai ◽  
Mie Ota

This paper presents the novel microstructure design, called Harmonic Structure, which gives structural metallic materials outstanding mechanical properties through an innovative powder metallurgy process. Homogeneous and ultra-fine grain (UFG) structure enables the materials high strength. However, such a “Homo-“ and “UFG” microstructure does not, usually, satisfy the need to be both strong and ductile, due to the plastic instability in the early stage of the deformation. As opposed to such a “Homo-and UFG“ microstructure, “Harmonic Structure” has a heterogeneous microstructure consisting of bimodal grain size together with a controlled and specific topological distribution of fine and coarse grains. In other words, the harmonic structure is heterogeneous on micro-but homogeneous on macro-scales. In the present work, the harmonic structure design has been applied to pure metals and alloys via a powder metallurgy route consisting of controlled severe plastic deformation of the corresponding powders by mechanical milling or high pressure gas milling, and subsequent consolidation by SPS. At a macro-scale, the harmonic structure materials exhibited superior combination of strength and ductility as compared to their homogeneous microstructure counterparts. This behavior was essentially related to the ability of the harmonic structure to promote the uniform distribution of strain during plastic deformation, leading to improved mechanical properties by avoiding or delaying localized plastic instability.


2016 ◽  
Vol 879 ◽  
pp. 1317-1322 ◽  
Author(s):  
Anna Mogucheva ◽  
Diana Yuzbekova ◽  
Tatiana Lebedkina ◽  
Mikhail Lebyodkin ◽  
Rustam Kaibyshev

The paper reports on the effect of severe plastic deformation on mechanical properties of an Al-4.57Mg-0.35Mn-0.2Sc-0.09Zr (in wt. pct.) alloy processed by equal channel angular pressing followed by cold rolling (CR). The sheets of the 5024 alloy with coarse grained (CG) structure exhibited a yield stress (YS) near 410 MPa and an ultimate tensile strength (UTS) of 480 MPa, while the YS and UTS of this material with ultrafine-grained (UFG) structure increased to 530 and 560 MPa, respectively. On the other hand, the elongation to failure decreased by a factor of 2 and 4 after CR and CR following ECAP, respectively. It was shown that dislocation strengthening attributed to extensive CR plays a major role in achieving high strength of this alloy. Besides these macroscopic characteristics, jerky flow caused by the Portevin-Le Chatelier (PLC) instability of plastic deformation was examined. The formation of UFG structure results in a transition from mixed type A+B to pure type B PLC serrations. No such effect on the serrations type was observed after CR.


2019 ◽  
Vol 16 (2) ◽  
pp. 183-188
Author(s):  
Shailendra Joshi

Stainless steel has an excellent mechanical property as well as high corrosion resistance. Stainless steel foams, therefore, seemed like an attractive material for impact energy absorption applications where damping capability is required such as in vehicles and buildings. Also when stainless steel foam is produced as stainless steel foam, the material density will be reduced thus the resulting foam will be a combination of light weight and high strength that can also be used in high strength applications. In our analysis, we tried to produce stainless steel foam through powder metallurgy in order to control mechanical properties in a better manner compared to the casting method. Also, we try to compare the pore morphology in foams on changing the space holder from accicular urea to crushed urea using FE-SEM. The properties of stainless steel foam, to a large extent, are found to depend on the arrangement of the pores which is decided by the space holder utilized during its synthesis using powder metallurgy route. The stainless steel obtained using acicular carbamide as space holder is found to possess acicular or irregular pores whereas those produced with crushed urea as space holder possesses nearly circular holes. Also, the previous foams are found to have better mechanical properties contributing towards more useful metallic foam.


2009 ◽  
Vol 24 (6) ◽  
pp. 2118-2122 ◽  
Author(s):  
Y.Y. Li ◽  
C. Yang ◽  
W.P. Chen ◽  
X.Q. Li ◽  
S.G. Qu

We report on the formation of ultrafine-grained Ti66Nb13Cu8Ni6.8Al6.2 composites with in situ precipitated micrometer-sized β-Ti(Nb) phase by spark plasma sintering with crystallization. Microstructure analysis indicated that all alloys consisted of soft (Cu, Ni)Ti2 regions surrounded by hard β-Ti(Nb) regions but displayed different microstructures. The alloys exhibited high fracture strength of more than 2200 MPa and remarkable plasticity of ∼25%. The results provided a promising method for fabricating large-sized bulk composites with excellent mechanical properties by powder metallurgy.


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