Effect of the scanning strategy on microstructure and mechanical anisotropy of Hastelloy X superalloy produced by Laser Powder Bed Fusion

2021 ◽  
Vol 173 ◽  
pp. 110951
Author(s):  
Xuan Zhang ◽  
Hao Xu ◽  
Zhongjie Li ◽  
Anping Dong ◽  
Dafan Du ◽  
...  
2020 ◽  
Vol 10 (1) ◽  
Author(s):  
Itziar Serrano-Munoz ◽  
Tatiana Mishurova ◽  
Tobias Thiede ◽  
Maximilian Sprengel ◽  
Arne Kromm ◽  
...  

Author(s):  
Felix Schmeiser ◽  
Erwin Krohmer ◽  
Christian Wagner ◽  
Norbert Schell ◽  
Eckart Uhlmann ◽  
...  

AbstractLaser powder bed fusion is an additive manufacturing process that employs highly focused laser radiation for selective melting of a metal powder bed. This process entails a complex heat flow and thermal management that results in characteristic, often highly textured microstructures, which lead to mechanical anisotropy. In this study, high-energy X-ray diffraction experiments were carried out to illuminate the formation and evolution of microstructural features during LPBF. The nickel-base alloy Inconel 625 was used for in situ experiments using a custom LPBF system designed for these investigations. The diffraction patterns yielded results regarding texture, lattice defects, recrystallization, and chemical segregation. A combination of high laser power and scanning speed results in a strong preferred crystallographic orientation, while low laser power and scanning speed showed no clear texture. The observation of a constant gauge volume revealed solid-state texture changes without remelting. They were related to in situ recrystallization processes caused by the repeated laser scanning. After recrystallization, the formation and growth of segregations were deduced from an increasing diffraction peak asymmetry and confirmed by ex situ scanning transmission electron microscopy. Graphical Abstract


2020 ◽  
Author(s):  
Bo Qian ◽  
Hongri Fan ◽  
Tengfei Li ◽  
Jianrui Zhang ◽  
Jiangtao Xi ◽  
...  

Abstract Aiming at laser powder bed fusion of GH3536 nickel base alloy, the effects of different scanning strategies on microstructure, porosity and mechanical properties were explored. In the aspect of microstructure and micro hardness of the sample, three scanning strategies had little difference; in the aspect of macro mechanical properties of the sample, the slope subarea scanning was better than the helix and island scanning. On this basis, the slope subarea scanning was selected as the optimal scanning strategy to form the G-surface structure, and the compression performance of G-surface was studied. The results showed that: (1) the compression performance of G-surface structure was smaller than that of solid structure; while G-surface structure had a smooth compression curve, which indicated the good energy absorption characteristics; (2) with the increase of wall thickness, the mechanical performance of G-surface structure was also enhanced, while the energy absorption capacity was constantly reduced; (3) with the same wall thickness, the compression performance of sample in building direction (BD) is higher than that in horizontal direction (HD).


Crystals ◽  
2021 ◽  
Vol 11 (9) ◽  
pp. 1064
Author(s):  
Shinya Hibino ◽  
Tsubasa Todo ◽  
Takuya Ishimoto ◽  
Ozkan Gokcekaya ◽  
Yuichiro Koizumi ◽  
...  

The influence of various laser powder bed fusion (LPBF) process parameters on the crystallographic textures and mechanical properties of a typical Ni-based solid-solution strengthened alloy, Hastelloy-X, was examined. Samples were classified into four groups based on the type of crystallographic texture: single crystalline-like microstructure with <100>//build direction (BD) (<100>-SCM), single crystalline-like microstructure with <110>//BD (<110>-SCM), crystallographic lamellar microstructure (CLM), or polycrystalline microstructure (PCM). These four crystallographic textures were realized in Hastelloy-X for the first time here to the best of our knowledge. The mechanical properties of the samples varied depending on their texture. The tensile properties were affected not only by the Schmid factor but also by the grain size and the presence of lamellar boundaries (grain boundaries). The lamellar boundaries at the interface between the <110>//BD oriented main layers and the <100>//BD-oriented sub-layers of CLM contributed to the resistance to slip transmission and the increased proof stress. It was possible to control a wide range of crystallographic microstructures via the LPBF process parameters, which determines the melt pool morphology and solidification behavior.


Materials ◽  
2021 ◽  
Vol 14 (15) ◽  
pp. 4305
Author(s):  
Shuzhe Zhang ◽  
Yunpei Lei ◽  
Zhen Chen ◽  
Pei Wei ◽  
Wenjie Liu ◽  
...  

It is of great importance to study the microstructure and textural evolution of laser powder bed fusion (LPBF) formed Hastelloy-X alloys, in order to establish a close relationship between the process, microstructure, and properties through the regulation of the Hastelloy-X formation process parameters. In this paper, components of a Hastelloy-X alloy were formed with different laser energy densities (also known as the volume energy density VED). The densification mechanism of Hastelloy-X was studied, and the causes of defects, such as pores and cracks, were analyzed. The influence of different energy densities on grain size, texture, and orientation was investigated using an electron backscatter diffraction technique. The results show that the average grain size, primary dendrite arm spacing, and number of low angle grain boundaries increased with the increase of energy density. At the same time, the VED can strengthen the texture. The textural intensity increases with the increase of energy density. The best mechanical properties were obtained at the VED of 96 J·mm−3.


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