Characterization of silicon carbide ceramics obtained from porous carbon structure achieved by plant carbonization

2020 ◽  
Vol 245 ◽  
pp. 122768 ◽  
Author(s):  
Vladimir Dodevski ◽  
Maja C. Pagnacco ◽  
Ivana Radović ◽  
Milena Rosić ◽  
Bojan Janković ◽  
...  
2009 ◽  
Vol 1181 ◽  
Author(s):  
Malek Amir Abunaemeh ◽  
Ibidapo Ojo ◽  
Mohamed Seif ◽  
Claudiu Muntele ◽  
Daryush Ila

AbstractThe TRISO fuel that is intended to be used for the generation IV nuclear reactor design consists of a fuel kernel of Uranium Oxide (UOx) coated in several layers of materials with different functions. One consideration for some of these layers is Silicon Carbide (SiC) [1]. The design, manufacture and fabrication of SiC are done at the Center for Irradiation of Materials (CIM). This light weight material can maintain dimensional and chemical stability in adverse environments and very high temperatures. The characterization of the elemental makeup of the SiC material used is done using X-ray photoelectron spectroscopy (XPS). Nano-indentation is used to determine the hardness, stiffness and Young's Modulus of the material. Raman Spectroscopy is used to characterize the chemical bonding for different sample preparation temperatures.


2010 ◽  
Vol 434-435 ◽  
pp. 162-164
Author(s):  
Dong Lin Zhao ◽  
Lei Zhang ◽  
Zeng Min Shen

Nano silicon carbide ceramics were prepared via precursor pyrolysis. Polycarbosilane (PCS) and divinylbenzene (DVB) were selected as a precursor to silicon carbide ceramics and a cross-linking reagent for PCS, respectively. The cross-linking properties and pyrolysis of PCS and DVB were investigated by changing the mass ratios of PCS/DVB. The mass ratio of PCS/DVB has a great effect on silicon carbide ceramic yield. The cured PCS/DVB with a mass ratio of 1:0.5 has the highest SiC ceramic yield (63.1%) at the temperature up to 1500 °C and its pyrolyzates consiste of nano silicon carbide with a diameter of 10-40 nm. The microstructures of the nano silicon carbide ceramics were characterized by SEM and XRD. The pyrolysis behavior of the cured PCS/DVB was characterized by thermogravimetry in nitrogen atmosphere.


2012 ◽  
Vol 27 (9) ◽  
pp. 965-969
Author(s):  
Xiao YANG ◽  
Xue-Jian LIU ◽  
Zheng-Ren HUANG ◽  
Gui-Ling LIU ◽  
Xiu-Min YAO

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