scholarly journals Preliminary study of composite fibers polyvinylpyrrolidone/cellulose acetate loaded by garlic extract by means of electrospinning method

2021 ◽  
Author(s):  
Dhewa Edikresnha ◽  
Tri Suciati ◽  
Khairurrijal Khairurrijal
Keyword(s):  
Cellulose Acetate ◽  
Garlic Extract ◽  
Composite Fibers ◽  
Electrospinning Method ◽  
Preliminary Study

scholarly journals Green Synthesis and Incorporation of Sericin Silver Nanoclusters into Electrospun Ultrafine Cellulose Acetate Fibers for Anti-Bacterial Applications

Polymers ◽  
2021 ◽  
Vol 13 (9) ◽  
pp. 1411
Author(s):  
Mujahid Mehdi ◽  
Huihui Qiu ◽  
Bing Dai ◽  
Raja Fahad Qureshi ◽  
Sadam Hussain ◽  
...  
Keyword(s):  
Electron Microscopy ◽  
Green Synthesis ◽  
Cellulose Acetate ◽  
Antibacterial Properties ◽  
Vital Role ◽  
Silver Nanoclusters ◽  
Composite Fibers ◽  
E Coli ◽  
Antibacterial Performance ◽  
Field Emission Electron Microscopy

Fiber based antibacterial materials have gained an enormous attraction for the researchers in these days. In this study, a novel Sericin Encapsulated Silver Nanoclusters (sericin-AgNCs) were synthesized through single pot and green synthesis route. Subsequently these sericin-AgNCs were incorporated into ultrafine electrospun cellulose acetate (CA) fibers for assessing the antibacterial performance. The physicochemical properties of sericin-AgNCs/CA composite fibers were investigated by transmission electron microscopy (TEM), field emission electron microscopy (FE-SEM), Fourier transform infrared spectroscopy (FTIR) and wide X-ray diffraction (XRD). The antibacterial properties of sericin-AgNCs/CA composite fibers against Escherichia coli (E. coli) and Staphylococcus aureus (S. aureus) were systematically evaluated. The results showed that sericin-AgNCs incorporated in ultrafine CA fibers have played a vital role for antibacterial activity. An amount of 0.17 mg/mL sericin-AgNCs to CA fibers showed more than 90% results and elevated upto >99.9% with 1.7 mg/mL of sericin-AgNCs against E. coli. The study indicated that sericin-AgNCs/CA composite confirms an enhanced antibacterial efficiency, which could be used as a promising antibacterial product.

ELECTROSPINNING OF CONTINUOUS CARBON NAONOFIBER-FILLED COMPOSITE FIBERS

2012 ◽  
Vol 05 ◽  
pp. 545-550
Author(s):  
Seyed Hamed Aboutalebi ◽  
Zahra Gholamvand ◽  
Mansoor Keyanpour-Rad
Keyword(s):  
Carbon Nanofibers ◽  
Polymer Fibers ◽  
Composite Fibers ◽  
Force Microscopy ◽  
Atomic Force ◽  
Macro Scale ◽  
Electrospinning Method ◽  
Scale Structures ◽  
Filled Composite ◽  
Pan Fibers

In order to translate the superior properties of carbon nanofibers (CNFs) to macro-scale structures, an electrospinning route capable of placing CNFs into a continuous nano-scale composite fibril is introduced. In this work, composite fibers were produced by electrospinning solution of polyacrylonitrile ( PAN ) with carbon nanofibers dispersed in dimethylformamide ( DMF ), which is an effective solvent for carbon nanofibers. Atomic force microscopy (AFM) and scanning electron microscopy (SEM) demonstrated rough and globular surfaces on the CNF containing fibers. Raman spectra confirmed the presence of CNFs in the polymer fibers prepared employing the electrospinning method. Raman observation served as the direct evidence of successful filling of PAN fibers with CNFs and complemented the results obtained by SEM and AFM studies.

Preparation of Cellulose Acetate Ultra-Fine Fibers Containing Quasi-Spherical Gold Nanoparticles by Electrospinning Method

2011 ◽  
Vol 391-392 ◽  
pp. 400-403
Author(s):  
Dong Mei Zhao ◽  
Li Guo Sun ◽  
Li Li Lv ◽  
Jian Li
Keyword(s):  
Electron Microscopy ◽  
Gold Nanoparticles ◽  
Cellulose Acetate ◽  
Trisodium Citrate ◽  
X Ray Diffraction ◽  
Au Nps ◽  
Transmission Electron ◽  
Electrospinning Method ◽  
Before And After ◽  
Spherical Gold Nanoparticles

Quasi-spherical gold nanoparticles(Au NPs) prepared by trisodium citrate reduction of HAuCl4were dispersed into cellulose acetate(CA) ultra-fine fibers by electrospinning. The optical properties of Au NPs before and after electrospinning were measured by UV-vis spectrometer. The morphology and distribution of Au NPs in CA ultra-fine fibers were observed by transmission electron microscopy (TEM). The morphology and diameter of Au NPs/CA fibers were studied by scanning electron microscopy (SEM). The crystallinity change of CA fiber before and after adding Au NPs was characterized by X-ray diffraction (XRD).

Morphology Studies of Electrospun Lithium Iron Phosphate (LiFePO4)/Cellulose Acetate (CA) Fibers

2016 ◽  
Vol 694 ◽  
pp. 101-105
Author(s):  
M. Mohamad ◽  
M.F.Z. Abidin ◽  
Haslan Fadli Ahmad Marzuki ◽  
Abdullah Ahmad Nizam ◽  
Muhamad Hazri Othman ◽  
...  
Keyword(s):  
Cellulose Acetate ◽  
Lithium Iron Phosphate ◽  
Mixed Solvent ◽  
Iron Phosphate ◽  
Solution Concentration ◽  
Electrospinning Process ◽  
Solution Viscosity ◽  
Pump Rate ◽  
Preliminary Study ◽  
Needle Diameter

This work was carried out as a preliminary study of electrospun LiFePO4/CA fibers. Cellulose acetate (CA) and LiFePO4 solutions were prepared separately using mixed solvent of acetone and water, prior to the electrospinning process. Then, electrospinning parameters including solution concentration, distance tip to collector, pump rate, and needle diameter size were optimized. Brunauer Emmett Teller (BET) was used to determine the surface area of CA fibers. Viscosity of CA solution was obtained by viscometer. LiFePO4/CA fibers were stabilized and carbonized at different temperature. The surface morphology and microstructure of the obtained LiFePO4/ CA fibers were then characterized using scanning electron microscope (SEM). In this work, it is shown that different electrospinning parameter, solution concentration and solution viscosity gives different fibers diameter and distribution. Moreover, the stabilization and carbonization temperature of LiFePO4/CA fibers may also affect the fibers microstructure.

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