Geometrically necessary dislocation density evolution as a function of microstructure and strain rate

Author(s):  
Daniel L. Foley ◽  
Marat I. Latypov ◽  
Xingyuan Zhao ◽  
Jonathan Hestroffer ◽  
Irene J. Beyerlein ◽  
...  
Author(s):  
C. W. Price

Little evidence exists on the interaction of individual dislocations with recrystallized grain boundaries, primarily because of the severely overlapping contrast of the high dislocation density usually present during recrystallization. Interesting evidence of such interaction, Fig. 1, was discovered during examination of some old work on the hot deformation of Al-4.64 Cu. The specimen was deformed in a programmable thermomechanical instrument at 527 C and a strain rate of 25 cm/cm/s to a strain of 0.7. Static recrystallization occurred during a post anneal of 23 s also at 527 C. The figure shows evidence of dissociation of a subboundary at an intersection with a recrystallized high-angle grain boundary. At least one set of dislocations appears to be out of contrast in Fig. 1, and a grainboundary precipitate also is visible. Unfortunately, only subgrain sizes were of interest at the time the micrograph was recorded, and no attempt was made to analyze the dislocation structure.


2017 ◽  
Vol 6 (2) ◽  
pp. 20 ◽  
Author(s):  
Manabu Tamura

Ninety-two sets of observed dislocation densities for crept specimens of 21 types of ferritic/martensitic and austenitic steels, Al, W, Mo, and Mg alloys, Cu, and Ti including germanium single crystals were collected to verify an equation for evaluating the dislocation density during steady-state creep proposed by Tamura and Abe (2015). The activation energy, Qex, activation volume, Vex, and Larson–Miller constant, Cex, were calculated from the creep data. Using these parameter constants, the strain rate, and the temperature dependence of the shear modulus, a correction term, Gamma, was back-calculated from the observed dislocation density for each material. Gamma is defined in the present paper as a function of the temperature dependences of both the shear modulus and pre-exponential factor of the strain rate. The values of Gamma range from −394 to 233  and average 2.1 KJmol-1, which is a value considerably lower than the average value of Qex (410.4 KJmol-1), and values of Gamma are mainly within the range from 0 to 50 KJmol-1. The change in Gibbs free energy, Delta G, for creep deformation is obtained using the calculated value of , and the empirical relation Delta G~Delta GD is found, where Delta GD is the change in Gibbs free energy for self-diffusion of the main componential element of each material. Experimental data confirm the validity of the evaluation equation for the dislocation density.


2016 ◽  
Vol 838-839 ◽  
pp. 404-409
Author(s):  
Roman Mishnev ◽  
Iaroslava Shakhova ◽  
Andrey Belyakov ◽  
Rustam Kaibyshev

A Cu-0.87%Cr-0.06%Zr alloy was subjected to equal channel angular pressing (ECAP) at a temperature of 400 °C up to a total strain of ~ 12. This processing produced ultra-fine grained (UFG) structure with an average grain size of 0.6 μm and an average dislocation density of ~4×1014 m-2. Tensile tests were carried out in the temperature interval 450 – 650 °C at strain rates ranging from 2.8´10-4 to 0.55 s-1. The alloy exhibits superplastic behavior in the temperature interval 550 – 600 °C at strain rate over 5.5´10-3 s-1. The highest elongation-to-failure of ~300% was obtained at a temperature of 575 °C and a strain rate of 2.8´10-3 s-1 with the corresponding strain rate sensitivity of 0.32. It was shown the superplastic flow at the optimum conditions leads to limited grain growth in the gauge section. The grain size increases from 0.6 μm to 0.87 μm after testing, while dislocation density decreases insignificantly to ~1014 m-2.


1996 ◽  
Vol 118 (4) ◽  
pp. 441-447 ◽  
Author(s):  
Y. Estrin ◽  
H. Braasch ◽  
Y. Brechet

A new constitutive model describing material response to cyclic loading is presented. The model includes dislocation densities as internal variables characterizing the microstructural state of the material. In the formulation of the constitutive equations, the dislocation density evolution resulting from interactions between dislocations in channel-like dislocation patterns is considered. The capabilities of the model are demonstrated for INCONEL 738 LC and Alloy 800H.


2021 ◽  
Vol 315 ◽  
pp. 84-89
Author(s):  
Chang Feng Wan ◽  
Dong Feng Li ◽  
Hai Long Qin ◽  
Ji Zhang ◽  
Zhong Nan Bi

In this paper, a micromechanical finite element (FE) model has been proposed to investigate the effect of the nanoscale precipitates on the development of microplasticity for Inconel 718 (IN718) superalloy. A strain gradient crystal plasticity formulation has been developed with the considerations of the evolution of statistically stored dislocation density and geometrically necessary dislocation density. The mesh convergence has been examined, showing that sufficiently fine mesh is required in the FE model. The results show that the model with strain gradient effect incorporated shows less peak plastic strain and higher value of dislocation density than the model with no strain gradient effect. The present study indicates that the strain hardening process at the scale of strengthening precipitate is mainly governed by the evolution of geometrically necessary dislocation densities.


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