Microstructure, mechanical properties and superelasticity of biomedical porous NiTi alloy prepared by microwave sintering

2015 ◽  
Vol 46 ◽  
pp. 387-393 ◽  
Author(s):  
J.L. Xu ◽  
L.Z. Bao ◽  
A.H. Liu ◽  
X.J. Jin ◽  
Y.X. Tong ◽  
...  
2012 ◽  
Vol 70 ◽  
pp. 142-145 ◽  
Author(s):  
Muhammad Hussain Ismail ◽  
Russell Goodall ◽  
Hywel A. Davies ◽  
Iain Todd

Author(s):  
Bahram Raad ◽  
Narges Shayesteh Moghaddam ◽  
Mohammad Elahinia

The aim of this article is to investigate the effect of two different fixation hardware materials on bone remodeling after a mandibular reconstruction surgery and to restore the mandible’s function, healthy appearance, mastication, swallowing, breathing, and speech. The hypothesis is that using fixation hardware with stiffness close to that of the surrounding bone will result in a more successful healing process in the mandible bone. The finite element model includes the material properties and forces of the cancellous bone, cortical bone, ligaments, muscles, and teeth. The reconstruction surgery is modeled by including the fixation hardware and the grafted bone. In the sectioned mandible, to best mimic the geometry of the mandible, two single barrel grafts are placed at the top of each other to form a double barrel graft set. Two different materials were used as the mandibular fixation parts, stiff Ti-6Al-4V, and porous superelastic Nickel-Titanium (NiTi) alloys. A comparison of these two alloys demonstrates that using porous NiTi alloy as the fixation part results in a faster healing pace. Furthermore, the density distribution in the mandibular bone after the healing process is more similar to the normal mandible density distribution. The simulations results indicate that the porous superelastic NiTi fixation hardware transfers and distributes the existing forces on the mandible bone more favorably. The probability of stress shielding and/or stress concentration decrease. This type of fixation hardware, therefore, is more appropriate for mandible bone reconstruction surgery.


Author(s):  
Dayanidhi Krishana Pathak ◽  
Pulak Mohan Pandey

Biodegradable zinc (Zn) has shown great potential in the area of biomedical applications. Though, the mechanical properties are decisive for the use of Zn for orthopedic and cardiovascular applications. Consequently, one needs to focus on improving the mechanical properties of Zn for its suitability in biomedical applications. Alloying of essential elements of the human body resulted in enhancement of Zn’s mechanical properties in recent years. The corrosion rate of pure Zn is ideal; however, the addition of other elements has resulted in a loss of its ideal corrosion rate. The inclusion of hydroxyapatite (HA) and iron (Fe) in Zn has also been reported in improving the mechanical properties. Hence, a need is raised for the development of a model which can predict the corrosion rate after adding HA along with Fe in Zn. In this research work, empirical based modeling is proposed to predict the corrosion rate, which incorporates the outcome of addition of Fe and HA in Zn. The Zn based materials were fabricated with the help of microwave sintering for developing the empirical model. The corrosion properties of the materials were assessed through a potentiodynamic polarization test in a simulated body fluid solution. The enhanced corrosion rate was attained with the rise in HA (wt%) and Fe (wt%) in Zn. An empirical correlation was established between the influencing controlling parameters (i.e., corrosion current, equivalent weight, and material density) of corrosion rate. Confirmation experiments were conducted to validate the developed model, and the highest error of 6.12% was obtained between the experimental and predicted values exhibiting the efficaciousness of the proposed model.


2020 ◽  
Vol 62 (7) ◽  
pp. 678-688
Author(s):  
X. Jiang ◽  
J. Chen ◽  
H. Sun ◽  
Z. Shao

Abstract High-entropy alloy composites were fabricated by ball milling, cold isostatic pressing and microwave sintering to which were added varied contents of Al2O3 whiskers, La-Ce, and carbon nanotubes-graphene, respectively. The structure and mechanical properties of the composites were investigated by X-ray diffraction, scanning electron microscopy and a microhardness tester. The high-entropy alloy and composites show amorphous phases and some crystalline phases. Accordingly, the addition of the reinforcement phase can refine the grain size. The formation mechanism of the phase is mainly related to the factors of mixing entropy, enthalpy, differences in atomic size, and the structure and property of the elements. The hardness of the composites is higher than that of the alloy (437.5 HV), and those composites reinforced by 0.5 wt.-% nanotubes- 0.5 wt.-% graphene are the highest (593.99 HV). The fracture morphology of the Al2O3 whisker reinforced composite shows a river pattern, indicating brittle cleavage. According to the research results, it can be concluded that the strengthening mechanism of the high entropy alloy composites mainly reflects fine grain strengthening and load transfer, and the toughening mechanism mainly crack bridging and a pulling out of the reinforcing phase.


2013 ◽  
Vol 594-595 ◽  
pp. 832-836
Author(s):  
M. Marina ◽  
M.Z.M. Zamzuri ◽  
Mohd Nazree Derman ◽  
Mohd Asri Selamat ◽  
Z. Nooraizedfiza

This research is focused on studying the density and mechanical properties of iron-chromium composites consolidated by innovative rapid microwave sintering technology against conventionally sintered counterparts using slow heating crucible furnace. Another aim of this study is to assess the viability of yttria (Y2O3) ceramic particulates as reinforcement to the iron-chromium composites. Fabrication of iron-chromium-yttria composites consolidated in microwave furnace and conventional crucible furnace was successfully accomplished. Improvement of density is evident in microwave sintered composites. The Y2O3 addition significantly increases the hardness of the composite (118 Hv for microwave specimens as opposed to 110Hv for conventional specimens). The study also successfully established the viability of microwave sintering technique for consolidating iron based powder metallurgy composites by up to 80% reduction of sintering time.


2002 ◽  
Vol 57 (2) ◽  
pp. 448-451 ◽  
Author(s):  
Yong-Hua Li ◽  
Guang-Bin Rao ◽  
Li-Jian Rong ◽  
Yi-Yi Li

2007 ◽  
Vol 336-338 ◽  
pp. 1072-1075 ◽  
Author(s):  
Kaleem Ahmad ◽  
Wei Pan ◽  
Wen Jie Si

Densification behavior, microstructural developments and mechanical properties of 5 wt% SiC nano particulate toughened Al2O3 composites were prepared by using microwave sintering at different sintering temperatures. Densities of up to 97.5% of the theoretical value were achieved at temperature as low as 1380°C. Improvements in fracture toughness and bending strengths are of the order of 99% theoretical dense conventionally sintered composites. Surface heating was observed at the final stages of densification. No thermal runaway was observed in the nanocomposites due to presence of SiC spheroids.


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