Automated sugaring-out liquid-liquid extraction based on flow system coupled with HPLC-UV for the determination of procainamide in urine

Talanta ◽  
2017 ◽  
Vol 167 ◽  
pp. 709-713 ◽  
Author(s):  
Lawrence Nugbienyo ◽  
Yulia Malinina ◽  
Sergei Garmonov ◽  
Mikhail Kamencev ◽  
Ilgiz Salahov ◽  
...  
1991 ◽  
Vol 56 (6) ◽  
pp. 1228-1237 ◽  
Author(s):  
Vlastimil Kubáň

The behaviour of a thin film of an organic solvent on the walls of the extraction coil in a continuous liquid-liquid extraction flow system was studied using a computer-controlled fast-recording on-tube photometric detection system (approx. 3 ms time resolution). A single-loop injector was employed to introduce precise, reproducible volumes (Sr < 2%) of one phase into the continuous stream of the other as a segmented volume standard. The film thickness Df, ranging from 1 to 20 μm for a 0.7 mm teflon tube, was calculated from the segment lengthening at a different chloroform flow rates and was found to obey a polynominal dependence on the linear flow rate, df = f(uα), where α < 1.


2021 ◽  
Vol 162 ◽  
pp. 105833
Author(s):  
Svetlana V. Smirnova ◽  
Kristina A. Lyskovtseva ◽  
Igor V. Pletnev

2019 ◽  
Vol 55 (1) ◽  
pp. 248-258 ◽  
Author(s):  
Karen C. A. Francisco ◽  
Pedro F. Brandão ◽  
Rui Miguel Ramos ◽  
Luís Moreira Gonçalves ◽  
Arnaldo A. Cardoso ◽  
...  

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