Quantitation of environmental contaminants by fused-silica capillary column gas chromatography—mass spectrometry with multiple internal standards and on-column injection

1983 ◽  
Vol 279 ◽  
pp. 209-218 ◽  
Author(s):  
D.E. Wells ◽  
A.A. Cowan
1988 ◽  
Vol 71 (2) ◽  
pp. 440-442 ◽  
Author(s):  
Stephen C Slahck

Abstract The analysis of trichlorfon by direct gas chromatography is discussed. A procedure is described for the determination of impurities in trichlorfon by using a fused silica capillary column and cold on-column injection. Attempts at quantitating trichlorfon using this system were unsuccessful due to problems with irreproducibility of the peak area. Although no derivatization was performed, there was no decomposition of the analyte as confirmed by mass spectrometry


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