Optical particle sizers for on-line applications in industrial plants

2003 ◽  
Vol 39 (2) ◽  
pp. 141-154 ◽  
Author(s):  
Iva Gianinoni ◽  
Elena Golinelli ◽  
Gianfranco Melzi ◽  
Sergio Musazzi ◽  
Umberto Perini ◽  
...  
Keyword(s):  
2003 ◽  
Vol 47 (5) ◽  
pp. 45-49 ◽  
Author(s):  
A. Mollica ◽  
P. Cristiani

The innovative electrochemical monitoring probe (BIOX) recently developed to improve the antifouling treatments of cooling systems in industrial plants is presented. On the basis of the good results obtained from applications on marine sites, some research has been started to validate this technique in biofilm growth and prevention of microbial corrosion in fresh and drinking waters.


2020 ◽  
Author(s):  
Lieven Clarisse ◽  
Martin Van Damme ◽  
Bruno Franco ◽  
Simon Whitburn ◽  
Juliette Hadji-Lazaro ◽  
...  

<p>IASI satellite ammonia (NH<sub>3</sub>) measurements are used to identify, categorise and quantify world's NH<sub>3</sub> emission hotspots. In particular, applying spatial oversampling and supersampling techniques on more than 10 years of IASI measurements, we are able to track-down more than 500 localized point sources of agricultural, industrial (fertilizer, coking, soda ash, geothermal and explosives industries), urban and natural origin. We present an on-line global NH<sub>3</sub> point sources catalogue, consisting of an interactive global map, visualizing the distribution, type and time evolution of the different point sources (http://www.ulb.ac.be/cpm/NH3-IASI.html). Calculated satellite-based emissions of NH<sub>3</sub> suggest a drastic underestimation of point sources in bottom-up inventories, especially those of industrial emitters. Temporal analysis revealed rapid shifts in anthropogenic activities, such as the opening or closure of industrial plants. These results demonstrate that using NH<sub>3</sub> satellite data will be hugely beneficial for improving bottom-up emission inventories.</p><p>A recently obtained homogeneous data record of NH<sub>3</sub> total columns from IASI (ANNI-NH<sub>3</sub>-v3R) is also used to derive trends over the last decade. We apply a bootstrap resampling method to determine the trends and to assess whether the calculated values are significant or not. We obtain the first global distribution (0.5°×0.5°) of atmospheric NH<sub>3</sub> trends based on 11 years (2008-2018) of IASI/Metop-A observations. Distinct temporal patterns are extracted and are analysed in light of anthropogenic activities and biomass burning events. National absolute and relative trends are also calculated and discussed.</p>


1995 ◽  
Author(s):  
Elena Golinelli ◽  
Paolo Martinelli ◽  
Sergio Musazzi ◽  
Umberto U. Perini ◽  
Franco Trespidi ◽  
...  

Author(s):  
William Krakow

In the past few years on-line digital television frame store devices coupled to computers have been employed to attempt to measure the microscope parameters of defocus and astigmatism. The ultimate goal of such tasks is to fully adjust the operating parameters of the microscope and obtain an optimum image for viewing in terms of its information content. The initial approach to this problem, for high resolution TEM imaging, was to obtain the power spectrum from the Fourier transform of an image, find the contrast transfer function oscillation maxima, and subsequently correct the image. This technique requires a fast computer, a direct memory access device and even an array processor to accomplish these tasks on limited size arrays in a few seconds per image. It is not clear that the power spectrum could be used for more than defocus correction since the correction of astigmatism is a formidable problem of pattern recognition.


Author(s):  
A.M.H. Schepman ◽  
J.A.P. van der Voort ◽  
J.E. Mellema

A Scanning Transmission Electron Microscope (STEM) was coupled to a small computer. The system (see Fig. 1) has been built using a Philips EM400, equipped with a scanning attachment and a DEC PDP11/34 computer with 34K memory. The gun (Fig. 2) consists of a continuously renewed tip of radius 0.2 to 0.4 μm of a tungsten wire heated just below its melting point by a focussed laser beam (1). On-line operation procedures were developped aiming at the reduction of the amount of radiation of the specimen area of interest, while selecting the various imaging parameters and upon registration of the information content. Whereas the theoretical limiting spot size is 0.75 nm (2), routine resolution checks showed minimum distances in the order 1.2 to 1.5 nm between corresponding intensity maxima in successive scans. This value is sufficient for structural studies of regular biological material to test the performance of STEM over high resolution CTEM.


Author(s):  
Neil Rowlands ◽  
Jeff Price ◽  
Michael Kersker ◽  
Seichi Suzuki ◽  
Steve Young ◽  
...  

Three-dimensional (3D) microstructure visualization on the electron microscope requires that the sample be tilted to different positions to collect a series of projections. This tilting should be performed rapidly for on-line stereo viewing and precisely for off-line tomographic reconstruction. Usually a projection series is collected using mechanical stage tilt alone. The stereo pairs must be viewed off-line and the 60 to 120 tomographic projections must be aligned with fiduciary markers or digital correlation methods. The delay in viewing stereo pairs and the alignment problems in tomographic reconstruction could be eliminated or improved by tilting the beam if such tilt could be accomplished without image translation.A microscope capable of beam tilt with simultaneous image shift to eliminate tilt-induced translation has been investigated for 3D imaging of thick (1 μm) biologic specimens. By tilting the beam above and through the specimen and bringing it back below the specimen, a brightfield image with a projection angle corresponding to the beam tilt angle can be recorded (Fig. 1a).


Author(s):  
G.Y. Fan ◽  
J.M. Cowley

In recent developments, the ASU HB5 has been modified so that the timing, positioning, and scanning of the finely focused electron probe can be entirely controlled by a host computer. This made the asynchronized handshake possible between the HB5 STEM and the image processing system which consists of host computer (PDP 11/34), DeAnza image processor (IP 5000) which is interfaced with a low-light level TV camera, array processor (AP 400) and various peripheral devices. This greatly facilitates the pattern recognition technique initiated by Monosmith and Cowley. Software called NANHB5 is under development which, instead of employing a set of photo-diodes to detect strong spots on a TV screen, uses various software techniques including on-line fast Fourier transform (FFT) to recognize patterns of greater complexity, taking advantage of the sophistication of our image processing system and the flexibility of computer software.


Author(s):  
John F. Mansfield ◽  
Douglas C. Crawford

A method has been developed that allows on-line measurement of the thickness of crystalline materials in the analytical electron microscope. Two-beam convergent beam electron diffraction (CBED) patterns are digitized from a JEOL 2000FX electron microscope into an Apple Macintosh II microcomputer via a Gatan #673 CCD Video Camera and an Imaging Systems Technology Video 1000 frame-capture board. It is necessary to know the lattice parameters of the sample since measurements are made of the spacing of the diffraction discs in order to calibrate the pattern. The sample thickness is calculated from measurements of the spacings of the fringes that are seen in the diffraction discs. This technique was pioneered by Kelly et al, who used the two-beam dynamic theory of MacGillavry relate the deviation parameter (Si) of the ith fringe from the exact Bragg condition to the specimen thickness (t) with the equation:Where ξg, is the extinction distance for that reflection and ni is an integer.


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