Quantitative determination of the specific heat and the glass transition of moist samples by temperature modulated differential scanning calorimetry

2001 ◽  
Vol 217 (1-2) ◽  
pp. 173-181 ◽  
Author(s):  
Markus Schubnell ◽  
Jürgen E.K Schawe
1982 ◽  
Vol 60 (14) ◽  
pp. 1853-1856 ◽  
Author(s):  
Eva I. Vargha-Butler ◽  
A. Wilhelm Neumann ◽  
Hassan A. Hamza

The specific heats of five polymers were determined by differential scanning calorimetry (DSC) in the temperature range of 300 to 360 K. The measurements were performed with polymers in the form of films, powders, and granules to clarify whether or not DSC specific heat values are dependent on the diminution of the sample. It was found that the specific heats for the bulk and powdered form of the polymer samples are indistinguishable within the error limits, justifying the determination of specific heats of powders by means of DSC.


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