In-situ HIP synthesis of TiB2/SiC ceramic composites

1999 ◽  
Vol 89-90 ◽  
pp. 457-461 ◽  
Author(s):  
Zhu Degui ◽  
Liu Shikai ◽  
Yin Xiandong ◽  
Yang Liu ◽  
Xiao Chuanchun ◽  
...  
Keyword(s):  
Ceramic Composites ◽  
Sic Ceramic

A study on in-situ synthesis of TiB2–SiC ceramic composites by reactive hot pressing

2014 ◽  
Vol 40 (1) ◽  
pp. 2305-2313 ◽  
Author(s):  
Guolong Zhao ◽  
Chuanzhen Huang ◽  
Hanlian Liu ◽  
Bin Zou ◽  
Hongtao Zhu ◽  
...  
Keyword(s):  
Hot Pressing ◽  
Ceramic Composites ◽  
In Situ Synthesis ◽  
Sic Ceramic ◽  
Reactive Hot Pressing

Synthesis and Properties of Ti3SiC2/SiC Ceramic Composites

2005 ◽  
Vol 475-479 ◽  
pp. 1243-1246 ◽  
Author(s):  
Tong Wei Lin ◽  
Wen Bin Cao ◽  
Jiang Tao Li ◽  
Chang Chun Ge
Keyword(s):  
Phase Composition ◽  
Active Carbon ◽  
Hot Pressing ◽  
Ceramic Composites ◽  
Displacement Reaction ◽  
Starting Mixture ◽  
Sic Ceramic ◽  
Different Content

Ti3SiC2/SiC ceramic composites with different content of SiC were synthesized through in-situ solid displacement reaction by hot pressing from starting mixture powders of TiC, Si and active carbon. The densities of the specimens were measured, the phase composition of the specimens was identified by XRD, and the microstructures were observed by SEM.

Oxidation Behavior of Ti3SiC2-SiC Ceramic Composites

2007 ◽  
Vol 561-565 ◽  
pp. 687-691
Author(s):  
De Gui Zhu ◽  
Zhi Gang Wang
Keyword(s):  
Oxidation Resistance ◽  
Hot Isostatic Pressing ◽  
Ceramic Composites ◽  
Temperature Oxidation ◽  
Parabolic Law ◽  
Sic Ceramic ◽  
Long Time ◽  
Better Than ◽  
Oxidation Behaviors

The high temperature oxidation behaviors of the Ti3SiC2-SiC ceramic composites fabricated by in situ synthesis under hot isostatic pressing were studied by DSC. The results show that the growth of the oxide scales on Ti3SiC2-SiC ceramic composites obeys a parabolic law in air. The oxidation resistance at 1400°C is better than that at 1200°C for long time. The oxidation resistance of the Ti3SiC2-SiC ceramic composites is much higher than that of monolithic Ti3SiC2. The mechanism of oxidation of Ti3SiC2-SiC ceramic composites is discussed.

scholarly journals Multiphysics Model Development and the Core Analysis for In Situ Breeding and Burning Reactor

2013 ◽  
Vol 2013 ◽  
pp. 1-14 ◽  
Author(s):  
Shengyi Si
Keyword(s):  
Power Distribution ◽  
Model Development ◽  
Computer Code ◽  
Ceramic Composites ◽  
Fuel Pellet ◽  
Ceramic Pellet ◽  
Sic Ceramic ◽  
Calculation Results ◽  
Gen Iv

The in situ breeding and burning reactor (ISBBR), which makes use of the outstanding breeding capability of metallic pellet and the excellent irradiation-resistant performance of SiCf/SiC ceramic composites cladding, can approach the design purpose of ultralong cycle and ultrahigh burnup and maintain stable radial power distribution during the cycle life without refueling and shuffling. Since the characteristics of the fuel pellet and cladding are different from the traditional fuel rod of ceramic pellet and metallic cladding, the multiphysics behaviors in ISBBR are also quite different. A computer code, named TANG, to model the specific multiphysics behaviors in ISBBR has been developed. The primary calculation results provided by TANG demonstrate that ISBBR has an excellent comprehensive performance of GEN-IV and a great development potential.

Oxidation Behaviors of TiB2-TiCX and TiB2-TiCX/15SiC Ceramics

2010 ◽  
Vol 105-106 ◽  
pp. 179-183 ◽  
Author(s):  
De Gui Zhu ◽  
Hong Liang Sun ◽  
Yu Shu Wang ◽  
Liang Hui Wang
Keyword(s):  
Oxidation Resistance ◽  
Effective Temperature ◽  
Hot Isostatic Pressing ◽  
Ceramic Composites ◽  
Optical Micrograph ◽  
Different Temperatures ◽  
The Mean ◽  
Mean Time ◽  
Oxidation Behaviors

Fully dense samples of TiB2-TiCX and TiB2-TiCX/15SiC ceramic composites were fabricated by in-situ synthesis under hot isostatic pressing from TiH2, B4C and SiC powders. Their oxidized behaviors at different temperatures were tested. Optical micrograph studies and thermo-gravimetric analyses show that the highest effective temperature of oxidation resistance is 700°C for TiB2-TiCX, and 1100°C for TiB2-TiCX/15SiC. The weight gain of TiB2-TiCX/15SiC below 1100°C is quite low, and it rises up suddenly when the temperature reaches 1200°C. Thus, the highest effective temperature of oxidation resistance is 1100°C for TiB2-TiCX/15SiC. The oxidation dynamic curves of TiB2-TiCX/15SiC ceramics accord with the parabola’s law. The activation energy of TiB2-TiCx/15SiC (189.87kJ.mol-1) is higher than that of TiB2-TiCx (96.44kJ.mol-1). In the oxidation process of TiB2-TiCx/15SiC, TiB2 reacts with oxygen and generates TiO2 and B2O3 at first. A layer of whole homogeneous oxide film cannot be formed, in the mean time, the oxidation of TiC begins. When temperature goes up to 1000°C, TiC phase is totally oxidized. SiC is oxidized to SiO2 at about 900°C, Meanwhile, TiO2 forms denser film than B2O3, which grows and covers the surface of the material, and gives better property of oxidation resistance.

Analysis of Toughening Mechanisms of ZrO2/Nano-SiC Ceramic Composites

2004 ◽  
Vol 38 (3) ◽  
pp. 227-241 ◽  
Author(s):  
Ai Kah Soh ◽  
Dai-Ning Fang ◽  
Zhao-Xu Dong
Keyword(s):  
Ceramic Composites ◽  
Toughening Mechanisms ◽  
Sic Ceramic

Polymer-derived SiC ceramic aerogels with in-situ growth of SiC nanowires

2021 ◽  
Author(s):  
Debao Liu ◽  
Baolu Shi ◽  
Chenqi Wang ◽  
Zeshuai Li ◽  
Xianbo Wang ◽  
...  
Keyword(s):  
In Situ Growth ◽  
Sic Nanowires ◽  
Sic Ceramic

Strengthening Effect of In-Situ Dispersed Hexagonal Boron Nitride in Ceramic Composites

2006 ◽  
Vol 317-318 ◽  
pp. 163-166
Author(s):  
Guo Jun Zhang ◽  
Hideki Kita ◽  
Naoki Kondo ◽  
Tatsuki Ohji
Keyword(s):  
Grain Size ◽  
Boron Nitride ◽  
Hexagonal Boron Nitride ◽  
High Strength ◽  
Ceramic Composites ◽  
Strengthening Effect ◽  
Mechanical Shock ◽  
Metallic Particles ◽  
Reactive Hot Pressing

High strength particulate ceramic composites are in general reinforced by strong dispersoids, such as strong ceramic particles (SiC, TiB2, ZrO2, et al) and strong metallic particles (Mo, W, et al). In this work high strength ceramic composites with in-situ synthesized hexagonal boron nitride (h-BN) have been prepared and characterized. As an example, we manufactured mullite-BN composites by reactive hot pressing (RHP) using aluminum borates (9Al2O3·2B2O3 and 2Al2O3·B2O3) and silicon nitride as starting materials. The obtained material RHPed at 1800°C showed a strength of 540 MPa, which was 1.64 times higher than that of the monolithic mullite ceramics. TEM observation revealed that the composite had an isotropic microstructure with a fine mullite matrix grain size of less than 1 μm and a nano-sized h-BN platelets of about 200 nm in length and 60∼80 nm in thickness. The high strength was suggested to be from the reduced matrix grain size and the small toughening effect by the h-BN platelets. In addition, this kind of ceramic composite demonstrates low Young’s modulus that is beneficial to the thermal/mechanical shock resistance, and excellent machinability.

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