scholarly journals A microfluidic methodology to identify the mechanical properties of capsules: comparison with a microrheometric approach

Flow ◽  
2021 ◽  
Vol 1 ◽  
Author(s):  
Xing-Yi Wang ◽  
Adlan Merlo ◽  
Claire Dupont ◽  
Anne-Virginie Salsac ◽  
Dominique Barthès-Biesel

We present a microfluidic method to measure the elastic properties of a population of microcapsules (liquid drops enclosed by a thin hyperelastic membrane). The method is based on the observation of flowing capsules in a cylindrical capillary tube and an automatic inverse analysis of the deformed profiles. The latter requires results from a full numerical model of the fluid–structure interaction accounting for nonlinear membrane elastic properties. For ease of use, we provide them under the form of databases, when the initially spherical capsule has a membrane governed by a neo-Hookean or a general Hooke's law with different surface Poisson ratios. Ultimately, the microfluidic method yields information on the type of elastic constitutive law that governs the capsule wall material together with the value of the elastic parameters. The method is applied to a population of ovalbumin microcapsules and is validated by means of independent experiments of the same capsules subjected to a different flow in a microrheological device. This is of great interest for quality control purposes, as small samples of capsule suspensions can be diverted to a measuring test section and mechanically tested with a 10 % precision using an automated process.

1992 ◽  
Vol 65 (1) ◽  
pp. 201-210 ◽  
Author(s):  
Larry R. Evans ◽  
David A. Benko ◽  
James G. Gillick ◽  
Walter H. Waddell

Abstract Microcapsules containing rubber antidegradants were formed in a spray-drying process. Studies were carried out to select the proper wall material based on the processing properties, migration rate of the antidegradant through the capsule wall, thickness of the capsule wall, and overall capsule diameter. The resulting capsules were incorporated into a rubber article, providing a reservoir of antidegradant during the exposure lifetime. Testing of the rubber compounds with microcapsules having diameters less than 50 µm containing AN-(l,3-dimethylbutyl)-N′-phenyl-p-phenylenediamine in a matrix of cellulose acetate showed a significant increase in the crack-free lifetime of the rubber when flexed in exposure to ozone.


2015 ◽  
Vol 52 (1) ◽  
pp. 107-130 ◽  
Author(s):  
Oksana Shishkina ◽  
Stepan V Lomov ◽  
Ignaas Verpoest ◽  
Larissa Gorbatikh

Geophysics ◽  
2010 ◽  
Vol 75 (5) ◽  
pp. 75A165-75A176 ◽  
Author(s):  
Miguel Bosch ◽  
Tapan Mukerji ◽  
Ezequiel F. Gonzalez

There are various approaches for quantitative estimation of reservoir properties from seismic inversion. A general Bayesian formulation for the inverse problem can be implemented in two different work flows. In the sequential approach, first seismic data are inverted, deterministically or stochastically, into elastic properties; then rock-physics models transform those elastic properties to the reservoir property of interest. The joint or simultaneous work flow accounts for the elastic parameters and the reservoir properties, often in a Bayesian formulation, guaranteeing consistency between the elastic and reservoir properties. Rock physics plays the important role of linking elastic parameters such as impedances and velocities to reservoir properties of interest such as lithologies, porosity, and pore fluids. Geostatistical methods help add constraints of spatial correlation, conditioning to different kinds of data and incorporating subseismic scales of heterogeneities.


Author(s):  
Takahiro Nagata ◽  
Takaya Kobayashi

Improving the reliability on solder joints is one of the major tasks to achieve downsizing of electronics products. Taking the molten solder profile as an object of study, a new procedure to model solder liquid with a structural FEM has been developed, which enables us to solve an issue of predefining the geometrical profile of solder liquid drops in a state of static equilibrium taking the surface tension into account, and also a problem concerning dynamic stability of the liquid drops. Molten solder liquid is treated as viscous fluid. Deformation of the material due to its viscosity can be represented by the structural analysis using rheological approach. Two types of the constitutive laws, creep model or viscoelasticity model, can be applied. Such a simple case as the Newtonian fluid, either constitutive law may be employed. Using these types of the constitutive laws in the analysis with time incremental steps, it becomes possible not only to obtain the stabilized shape of liquid drops, but also to analyze problems involved with transient (including dynamic effect) stability. As the size of a liquid drop is microscopic in a range of 100 to 1000 μm, the effect of the surface tension must become so predominant in the loading conditions. In most of the conventional theoretical researches, it is found that the surface tension is treated as the pressure difference varying according to the surface curvature. However, this method is not only so complicated, but also may lead to numerical instability particularly in the transient analysis subjected to large deformations. In this study, an effective method has been developed in which the surface tension can be represented with good accuracy through simplified input data with allocating the shell element generating a constant membrane force over the surface of a liquid drop.


2014 ◽  
Vol 44 (7) ◽  
pp. 1304-1311 ◽  
Author(s):  
Pablo Teixeira da Silva ◽  
Leadir Lucy Martins Fries ◽  
Cristiano Ragagnin de Menezes ◽  
Augusto Tasch Holkem ◽  
Carla Luisa Schwan ◽  
...  

Microencapsulation is a process in which active substances are coated by extremely small capsules. It is a new technology that has been used in the cosmetics industry as well as in the pharmaceutical, agrochemical and food industries, being used in flavors, acids, oils, vitamins, microorganisms, among others. The success of this technology is due to the correct choice of the wall material, the core release form and the encapsulation method. Therefore, in this review, some relevant microencapsulation aspects, such as the capsule, wall material, core release forms, encapsulation methods and their use in food technology will be briefly discussed.


2015 ◽  
Vol 770 ◽  
pp. 137-143
Author(s):  
E.G. Soboleva ◽  
A.L. Igisheva ◽  
T.B. Krit

The given article considers acoustic analogues of elasticity theory ratios determining Poisson’s ratios of Sm1-xYxS alloy by their elastic parameters. The article discusses behavior of sound velocities, elastic moduli, Poisson’s ratios, Grüneisen parameter and brittleness-plasticity criterion ratios depending on the concentration of alloy components including valence transition from semiconductors into the metal phase.


Author(s):  
V. Е. Kosarev ◽  
◽  
E. R. Ziganshin ◽  
I. P. Novikov ◽  
A. N. Dautov ◽  
...  

Laboratory studies of the geomechanical properties of rocks are an important and integral part in building a geomechanical model. This study resulted in a set of data on geomechanical and elastic properties of the rocks that compose the lower part of the Middle Carboniferous section of the Ivinskoye oilfield (Russia). Relationships between various elastic parameters were also established. The distribution of geomechanical properties correlates with structural/textural features of the rocks under study and their lithological type. This information can be used as a basis for geomechanical modeling and in preparation for hydraulic fracturing. Keywords: geomechanics; elastic properties; carbonate rock; laboratory core studies.


Author(s):  
L. Angela Mihai ◽  
Thomas E. Woolley ◽  
Alain Goriely

The problem of the Rivlin cube is to determine the stability of all homogeneous equilibria of an isotropic incompressible hyperelastic body under equitriaxial dead loads. Here, we consider the stochastic version of this problem where the elastic parameters are random variables following standard probability laws. Uncertainties in these parameters may arise, for example, from inherent data variation between different batches of homogeneous samples, or from different experimental tests. As for the deterministic elastic problem, we consider the following questions: what are the likely equilibria and how does their stability depend on the material constitutive law? In addition, for the stochastic model, the problem is to derive the probability distribution of deformations, given the variability of the parameters. This article is part of the theme issue ‘Rivlin's legacy in continuum mechanics and applied mathematics’.


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