Instrumentation for detecting channelling radiation in the high-voltage electron microscope

Author(s):  
J. H. Butler ◽  
C. J. Humphreys

Electromagnetic radiation is emitted when fast (relativistic) electrons pass through crystal targets which are oriented in a preferential (channelling) direction with respect to the incident beam. In the classical sense, the electrons perform sinusoidal oscillations as they propagate through the crystal (as illustrated in Fig. 1 for the case of planar channelling). When viewed in the electron rest frame, this motion, a result of successive Bragg reflections, gives rise to familiar dipole emission. In the laboratory frame, the radiation is seen to be of a higher energy (because of the Doppler shift) and is also compressed into a narrower cone of emission (due to the relativistic “searchlight” effect). The energy and yield of this monochromatic light is a continuously increasing function of the incident beam energy and, for beam energies of 1 MeV and higher, it occurs in the x-ray and γ-ray regions of the spectrum. Consequently, much interest has been expressed in regard to the use of this phenomenon as the basis for fabricating a coherent, tunable radiation source.

1985 ◽  
Vol 62 ◽  
Author(s):  
S. Suzuki ◽  
T. Honda ◽  
Y. Bando

ABSTRACTThe dependence of the characteristic and bremsstrahlung X-ray counts, the peak to background (P/B) ratio and the spatial resolution on the incident beam energy between 100 keV and 400 keV were measured using a high voltage electron microscope (HVEM). The bremsstrahlung count decreases much faster than that of the characteristic count with the increase of the incident beam energy. The decrease rate depends on Z number. It is ascertained that the P/B ratio and the spatial resolution at 400 keV were 2 or 3 and 2.5 times better than those at 100 keV, respectively.


Author(s):  
N. J. Zaluzec

The ultimate sensitivity of microchemical analysis using x-ray emission rests in selecting those experimental conditions which will maximize the measured peak-to-background (P/B) ratio. This paper presents the results of calculations aimed at determining the influence of incident beam energy, detector/specimen geometry and specimen composition on the P/B ratio for ideally thin samples (i.e., the effects of scattering and absorption are considered negligible). As such it is assumed that the complications resulting from system peaks, bremsstrahlung fluorescence, electron tails and specimen contamination have been eliminated and that one needs only to consider the physics of the generation/emission process.The number of characteristic x-ray photons (Ip) emitted from a thin foil of thickness dt into the solid angle dΩ is given by the well-known equation


Author(s):  
C.J. Rossouw ◽  
L.J. Allen ◽  
P.R. Miller

An Einstein model for thermal diffuse scattering (TDS) has enabled quantitative calculation of the absorptive potential V'(r). This allows anomalous absorption to be accounted for in LACBED contrast. Fourier coefficients Vg-h of the absorptive component from each atom α are calculated from integrals of the formwhere fα is the scattering amplitude and M(Q) the Debye-Waller factor. Integration over the Ewald sphere (dΩ) requires the momentum transfer q to have values up to 2ko (the incident beam momentum). Dynamical ‘dechannelling’ is accounted for by the terms g ≠ h. The crystal absorptive potential is obtained by coherently summing over these atomic absorptive potentials within the unit cell. Unlike the elastic potential, the absorptive potential is a strong function of incident beam energy Eo, since the range of momentum transfer q and associated solid angles dΩ change with the Ewald sphere radius.Fig. 1 shows a LACBED pattern of the zeroth order beam from Si aligned along a <001> zone axis.


Author(s):  
Niraj Kumar Rai ◽  
Aman Gandhi ◽  
M T Senthil Kannan ◽  
Sujan Kumar Roy ◽  
Saneesh Nedumbally ◽  
...  

Abstract The pre-scission and post-scission neutron multiplicities are measured for the 18O + 184W reaction in the excitation energy range of 67.23−76.37 MeV. Langevin dynamical calculations are performed to infer the energy dependence of fission decay time in compliance with the measured neutron multiplicities. Different models for nuclear dissipation are employed for this purpose. Fission process is usually expected to be faster at a higher beam energy. However, we found an enhancement in the average fission time as the incident beam energy increases. It happens because a higher excitation energy helps more neutrons to evaporate that eventually stabilizes the system against fission. The competition between fission and neutron evaporation delicately depends on the available excitation energy and it is explained here with the help of the partial fission yields contributed by the different isotopes of the primary compound nucleus.


1997 ◽  
Vol 3 (S2) ◽  
pp. 881-882 ◽  
Author(s):  
Dale E. Newbury

Throughout the history of electron-beam X-ray microanalysis, analysts have made good use of the strong dependence of electron range on incident energy (R ≈ E1,7) to optimize the analytical volume when attacking certain types of problems, such as inclusions in a matrix or layered specimens. The “conventional” energy range for quantitative electron beam X-ray microanalysis can be thought of as beginning at 10 keV and extending to the upper limit of the accelerating potential, typically 30 - 50 keV depending on the instrument. The lower limit of 10 keV is selected because this is the lowest incident beam energy for which there is a satisfactory analytical X-ray peak excited from the K-, L-, or M- shells (in a few cases, two shells are simultaneously excited, e.g., Fe-K and Fe-L) for every element in the Periodic Table that is accessible to X-ray spectrometry, beginning with Be (Ek =116 eV) and extending to the transuranic elements. This criterion is based upon establishing a minimum overvoltage U = E0/Ec > 1.25, which is the practical minimum for useful excitation.


Instruments ◽  
2019 ◽  
Vol 3 (1) ◽  
pp. 8 ◽  
Author(s):  
Johanna Peeples ◽  
Sang-Hyon Chu ◽  
James O’Neil ◽  
Mustafa Janabi ◽  
Bruce Wieland ◽  
...  

Boron nitride nanotubes (BNNTs) were investigated as a target media for cyclotron production of 11C for incident beam energy at or below 11 MeV. Both the 11B(p,n)11C and 14N(p,α)11C nuclear reactions were utilized. A sweep gas of nitrogen or helium was used to collect recoil escape atoms with a desired form of 11CO2. Three prototype targets were tested using an RDS-111 cyclotron. Target geometry and density were shown to impact the saturation yield of 11C and percent of yield recovered as carbon dioxide. Physical damage to the BNNT target media was observed at beam currents above 5 μA. Additional studies are needed to identify operating conditions suitable for commercial application of the method.


1. When reading a recent paper before the Royal Society, and also in the Press, Dr. Edridge Green has stated that he can find no connection between the luminosity and the colour sense of persons having either normal or abnormal colour sensations. Since I feel that to allow such a statement to go unchallenged might be interpreted as meaning that no such connection could be shown to exist, I propose in the following paper to place before the Society some of the evidence which indicated that there is in reality a very intimate relation between luminosity and colour sense. The results given include a small part of those which have been obtained in a series of experiments which have occupied the last two years and form part of investigation which is still in progress. The term “luminosity” as used in this paper has the following meaning: Suppose that light from some source, such as the electric arc, is admitted to a spectroscope by means of which a real pure spectrum is produced, and that a slide in the plane in which the spectrum is formed carries a slit of fixed width. Light of sensibly one wave-length, i. e. monochromatic light, will pass through this slit, and by means of a lens placed in the beam of this light an image of the first face of the prism which is used to from the spectrum can be formed on a screen. In this way a monochromatic patch of light is obtained, the brightness of which depends on the nature of the source of light, the width of the collimator slit, the width of the slit placed in the spectrum, which for short will be called the movable slit, and the dimensions of the lenses employed. Further, if alongside this coloured patch is formed a white patch of light produced by light which proceeds from the same source but has not undergone dispersion, and that by some means or other the intensity of this white light is altered till the coloured and white light, measured in any arbitrary units, measure the luminosity of the light of that colour which is passing through the movable slit. Since the unit in which the white light is measured is arbitrary, we are not concerned with the absolute intensity of illumination of the white patch, and may use any device we like to alter the quantity of white light which falls on the screen so long as we are able to measure the ratio of the quantity of light employed in different experiments. It will further be observed that for any given person the measurement of the luminosity of a given coloured light in the spectrum involves the comparsion of the brightness of the coloured patch as it appears to him with the brightness of the white patch as it appears to him.


1975 ◽  
Vol 53 (2) ◽  
pp. 117-122 ◽  
Author(s):  
J. P. Labrie ◽  
E. E. Habib ◽  
Z. Preibisz

Excited levels of 70Ge and proton holes in 69Ga have been investigated by means of the 69Ga (3He, d)70Ge reaction at an incident beam energy of 22.5 MeV. Angular distributions were measured and are compared with the prediction of the distorted-wave-Born-approximation (DWBA) theory in order to obtain the spectroscopic strengths of each level.The number of proton holes in 69Ga was obtained from the sum rule of the spectroscopic strengths. The vacancy probability UJ2 and the center of gravity energy EJ for the 2p3/2, 1f5/2, and 2p1/2 subshells are[Formula: see text]These are compared with the pairing model calculations.


When a parallel pencil of monochromatic light falls at nearly the critical angle on the plane boundary between two media of differing refractive index, and emerges in the rarer medium in a direction almost parallel to the surface of separation, the aperture of the emergent pencil becomes greatly restricted. A study of the diffraction phenomena observed in this limiting case of oblique emergence seems of interest, especially in view of the fact that in the Lummer-Gehrcke interference spectroscope we have an actual case of importance in which such obliquely emergent pencils determined the observed phenomena. Some preliminary work on this subject was carried out by Prof. C. V. Raman, and at his suggestion the author of the present paper undertook a detailed experimental investigation of the case with a view to establishing its principal features. So far as the writer is aware, though the theory of the parallel-plate interferometer in its essentials is well known, the special character of the diffraction phenomena observed with pencils very obliquely refracted at a plane surface had not been discussed previously. It is proposed in the present paper to describe the results obtained by the writer, some of the observations (to be mentioned below) having special reference to the theory of the Lummer-Gehrcke plate. 2. Experimental Methods and Results . The general features of the case may be observed on an ordinary spectrometer. It is well known that an ordinary prismatic spectroscope may be so adjusted as to give very large dispersions, by putting the prism on the table of the instrument in such a position that the light incident on the first face, after passing through it, falls at nearly the critical angle of incidence on the second face and emerges nearly grazing the surface. The lines in the spectrum then appear very widely separated, and also strongly curved, owing to the fact that pencils of light from different points on the slit of the collimator do not all pass through the principal plane of the prism. In his investigation of the optical power of spectroscopes, Lord Rayleigh has remarked that the resolving power of the prism in the position referred to above is no greater than at other positions. The width of the beam emerging from the prism tends to zero as the grazing position is approached, and the spectrum lines are much widened by diffraction. This sets off the effect of the increased dispersion on the resolving power. Owing to the great dispersion and the enfeeblement of the light in oblique transmission, a very powerful source of monochromatic light is necessary for satisfactory observation of the diffraction phenomena. A Westinghouse quartz silica lamp is most suitable, though visual observations may also easily be made with a glass Cooper-Hewitt mercury-vapour lamp. Observations are made on the green line of the spectrum. In order to secure an extended diffraction-pattern, it is advantageous to use something less than the full aperture of the prism to start with, cutting it down by one or more slits having their edges parallel to the slit of the collimator. The position of the slits is a matter of indifference, so long as the aperture of the beam is cut down before it emerges or just as it emerges from the second surface of the prism, and not after it has emerged. The simplest arrangement is to limit the aperture of the beam by a slit or slits immediately before entry into the prism. Another arrangement would be to use a hollow prism, filled with liquid, and to put the slit or slits inside the prism, so as to limit the aperture of the beam just before incidence on the second face. A third arrangement is to use a glass prism the aperture of the second face of which has been reduced by grinding down to the desired width with parallel edges. All the arrangements give identical results.


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