Defect clusters in heavy-ion irradiated nickel and nickel alloys

Author(s):  
T.M. Robinson ◽  
M.L. Jenkins

Low-dose (≲1012ions/cm2) heavy-ion irradiation gives a convenient method of studying some aspects of fast-neutron radiation damage and has now been studied using transmission electron microscopy in a wide variety of metals and alloys (e.g. see the reviews by Eyre 1973 and Wilkens 1975). From these studies a consistent picture of the development of the damage structure has emerged. In most cases small vacancy loops are observed, produced heterogeneously at the sites of displacement cascades by the collapse of vacancy-rich ‘depleted zones’. The interstitial component of the damage is usually lost to the foil surfaces and is not observed. There have been surprisingly few investigations of heavy-ion damage in materials of technological importance. However, it has been noted that cascade collapse appears to take place less readily in complex alloys such as steels than in pure metals such as copper (e.g. Williams and Eyre 1976) but few attempts have been reported to explore this effect systematically.

1996 ◽  
Vol 439 ◽  
Author(s):  
S. Müller ◽  
M. L. Jenkins ◽  
C. Abromeit ◽  
H. Wollenberger

AbstractStereo transmission electron microscopy has been used to characterise the distribution in depth of disordered zones and associated dislocation loops in the ordered alloys Ni3Al and Cu3Au after heavy ion irradiation, most extensively for Ni3Al irradiated with 50 keV Ta+ ions at a temperature of 573 K. The Cu3Au specimen was irradiated with 50 keV Ni+ ions at an incident angle of 45° at a temperature of 373 K. In Ni3Al the defect yield, i.e. the probability for a disordered zone to contain a loop was found to be strongly dependent on the depth of the zone in the foil, varying from about 0.7 for near-surface zones to about 0.2 in the bulk. The sizes and shapes of disordered zones were only weakly dependent on depth, except for a small population of zones very near the surface which were strongly elongated parallel to the incident ion beam. In Cu3Au the surface had a smaller but still significant effect on the defect yield. The dependence of the tranverse disordered zone diameter d on ion energy E for Ta+ irradiation of NiA was found to follow a relationship d = k1, E1/α with k, = 2.4 ± 0.4 and α = 3.3 ± 0.4. A similar relationship with the same value of α is valid for a wide variety of incident ion/target combinations found in the literature.


1998 ◽  
Vol 540 ◽  
Author(s):  
Y. Yan ◽  
T. Walther ◽  
M.A. Kirk

AbstractStudies of defects generated by high energy (>1 GeV) heavy ion irradiation in high-Tc superconductors have been performed by transmission electron microscopy (TEM). Our study shows that high dose irradiation leads to the formation of nano-twins, by which the columnar defects are connected. An analysis of the local Fourier components of the image intensity in [001] lattice images indicates that these new "twin" boundaries are much more diffuse than preexisting twin boundaries in YBCO. The mechanism of the formation of nano-twin boundaries on {110} planes and their possible relation to superconducting properties are discussed.


Author(s):  
A. Sprague ◽  
K.B. Roarty ◽  
R.A. Johnson ◽  
F.A. Smidt

High energy heavy ion irradiation has been widely applied as a tool to study radiation damage in materials, both in attempts to simulate neutron damage and to investigate radiation effects mechanisms. Two important aspects of such studies are the effects of alloying elements on a metal’s irradiation response and the influence of damaging particle type and dose rate on these alloying effects. The present experiments examined these aspects by studying the microstructures of a series of low-concentration binary nickel alloys following neutron and nickel-ion irradiation.


1997 ◽  
Vol 481 ◽  
Author(s):  
A. Meldrum ◽  
L. A. Boatner ◽  
R. C. Ewingt

ABSTRACTSeveral perovskite-structure oxide compounds, including CaTiO3, SrTiO3, BaTiO3, KNbO3, and KTaO3 were irradiated by 800 keV Kr+ ions in order to investigate and compare their response to heavy-ion irradiation. The critical amorphization temperature Tc, above which amorphization could not be induced, was found to increase in the order SrTiO3 → CaTiO3 → BaTiO3 → KNbO3 → KTaO3. No single physical parameter explains the observed sequence, although Tc correlates well with the melting temperatures. The well-known solid state phase transformations in these materials did not have a significant effect on the dose required for amorphization. Domain boundaries were observed in the pristine samples; however, after only a low dose, the boundaries became poorly defined and, with increasing dose, eventually disappeared. Dislocation loops were observed to aggregate at the domain boundaries.


1981 ◽  
Vol 43 (4) ◽  
pp. 999-1015 ◽  
Author(s):  
T. M. Robinson ◽  
M. L. Jenkins

2002 ◽  
Vol 82 (11) ◽  
pp. 2333-2339
Author(s):  
G. Schumacher ◽  
R. C. Birtcher ◽  
D. P. Renusch ◽  
M. Grimsditch ◽  
L. E. Rehn

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