High Spatial Resolution Soft X-Ray Microscopy and Microanalysis of Thick and Hydrated Materials

1998 ◽  
Vol 4 (S2) ◽  
pp. 352-353
Author(s):  
W. Meyer-Ilse ◽  
J. T. Brown ◽  
C. Magowan ◽  
J. Yeung ◽  
K. E. Kurtis ◽  
...  

The Center for X-ray Optics (CXRO) built and operates a high-resolution soft x-ray microscope (XM-1) at the Advanced Light Source in Berkeley. We report on the use of this instrument in a variety of scientific fields, including biology, civil engineering and environmental sciences.The microscope is a conventional (full field) x-ray microscope, which uses zone plate lenses to provide high resolution transmission images. The optical setup is similar to the Göttingen x-ray microscope, operated at the BESSY synchrotron radiation facility in Berlin, Germany. A condenser zone plate, fabricated by the Göttingen group, is illuminating the sample and an objective zone plate, fabricated by Erik Anderson (CXRO), is forming an enlarged image on an x-ray CCD camera. While the optical path of the microscope is in vacuum, the sample is at atmospheric pressure, flushed by helium. The spatial resolution of our microscope is 43 nm, measured as the distance from 10%-90% intensity in the image of a knife-edge.

Nanomaterials ◽  
2020 ◽  
Vol 10 (9) ◽  
pp. 1721
Author(s):  
Heon Yong Jeong ◽  
Hyung San Lim ◽  
Ju Hyuk Lee ◽  
Jun Heo ◽  
Hyun Nam Kim ◽  
...  

The effect of scintillator particle size on high-resolution X-ray imaging was studied using zinc tungstate (ZnWO4) particles. The ZnWO4 particles were fabricated through a solid-state reaction between zinc oxide and tungsten oxide at various temperatures, producing particles with average sizes of 176.4 nm, 626.7 nm, and 2.127 μm; the zinc oxide and tungsten oxide were created using anodization. The spatial resolutions of high-resolution X-ray images, obtained from utilizing the fabricated particles, were determined: particles with the average size of 176.4 nm produced the highest spatial resolution. The results demonstrate that high spatial resolution can be obtained from ZnWO4 nanoparticle scintillators that minimize optical diffusion by having a particle size that is smaller than the emission wavelength.


2007 ◽  
Author(s):  
Courtney A. Brewer ◽  
Fernando Brizuela ◽  
Dale Martz ◽  
Georgiy Vaschenko ◽  
Mario C. Marconi ◽  
...  

2014 ◽  
Vol 86 (21) ◽  
pp. 10892-10899 ◽  
Author(s):  
Francesco Paolo Romano ◽  
Claudia Caliri ◽  
Luigi Cosentino ◽  
Santo Gammino ◽  
Lorenzo Giuntini ◽  
...  

1984 ◽  
Vol 86 ◽  
pp. 80-83
Author(s):  
S.M. Kahn ◽  
S.D. Vrtilek ◽  
L. Chiappetti ◽  
N.E. White

The presence of objective transmission gratings on the two recent X-ray telescope experiments, the Einstein and EXOSAT Observatories, has opened up a new avenue of research in X-ray astronomy by enabling us, for the first time, to obtain moderate-to-high resolution spectra of cosmic sources in the soft X-ray band (λ ~ 5–200 Å). Both experiments incorporated gold bar transmission gratings with line densities of 500 1/mm and 1000 1/mm which could be inserted into the X-ray optical path at the exit from a grazing incidence mirror. At short wavelengths, the resolution was determined principally by the spatial resolution of the detector-telescope combination. For Einstein, this was Δλ ~ 0.4 Å for the 1000 1/mm grating and ~ 0.8 Å for the 500 1/mm grating. For EXOSAT, the resolution was somewhat worse: Δλ ~ 1.5 Å for the 1000 1/mm grating, and ~ 3 Å for the 500 1/mm grating. (More complete descriptions of these instruments can be found in Seward et al. 1982 and de Korte et al. 1981.)


1998 ◽  
Vol 4 (S2) ◽  
pp. 190-191
Author(s):  
Patrick Echlin

Although high resolution (2nm), low voltage (lkV), SEM of bio-organic materials can now be performed more or less routinely using instruments fitted with a field emission source, virtually no low voltage x-ray microanalysis has been carried out on this type of specimen. Boyes and Nockolds showed that quantitative microanalytical information could be obtained from polished inorganic samples at a spatial resolution of l00nm at 5kV and Johnson et al obtained similar type of data at a spatial resolution of 150nm at 3kV. High spatial resolution (l0nm) microanalysis can be achieved in frozen dried or chemically compromised sections of biological material examined at high voltage in the TEM but frozen hydrated chemically unfixed sections are damaged. The other approach is to use the SEM with frozen hydrated, chemically uncompromised samples, usually at about 10-15kV, in order to obtain sufficient signal from the elements of interest which typically lie in the range Na (Z=l 1) to Ca (Z=20).


2017 ◽  
Vol 17 (3) ◽  
pp. 514-531 ◽  
Author(s):  
Yongchao Yang ◽  
Charles Dorn ◽  
Tyler Mancini ◽  
Zachary Talken ◽  
James Theiler ◽  
...  

Detecting damage in structures based on the change in their dynamics or modal parameters (modal frequencies and mode shapes) has been extensively studied for three decades. The success of such a global, passive, vibration-based method in field applications, however, has long been hindered by the bottleneck of low spatial resolution vibration sensor measurements. The primary reason is that damage typically initiates and develops in local regions that need to be captured and characterized by very high spatial resolution vibration measurements and modal parameters (mode shapes), which are extremely difficult to obtain using traditional vibration measurement techniques. For example, accelerometers and strain-gauge sensors are typically placed at a limited number of discrete locations, providing low spatial resolution vibration measurements. Laser vibrometers provide high-resolution measurements, but are expensive and make sequential measurements that are time- and labor-consuming. Recently, digital video cameras—which are relatively low cost, agile, and able to provide high spatial resolution, simultaneous, pixel measurements—have emerged as a promising tool to achieve full-field, high spatial resolution vibration measurements. Combined with advanced vision processing and unsupervised machine algorithms, a new method has recently been developed to blindly and efficiently extract the full-field, high-resolution, dynamic parameters from the video measurements of an operating, output-only structure. This work studies the feasibility of performing damage detection using the full-field, very high spatial resolution mode shape (of the fundamental mode) blindly extracted from the video of the operating (output-only) structure without any knowledge of reference (healthy) structural information. A spatial fractal dimension analysis is applied on the full-field mode shape of the damaged structure to detect damage-induced irregularity. Additionally, the equivalence between the fractal dimension and the squared curvature (modal strain energy) of the mode shape curve, when of high spatial resolution, is mathematically derived. Laboratory experiments are conducted on bench-scale structures, including a building structure and a cantilever beam, to validate the approach. The results illustrate that using the full-field, very high-resolution mode shape enables detection of minute, non-visible, damage in a global, completely passive sensing manner, which was previously not possible to achieve.


1997 ◽  
Vol 3 (S2) ◽  
pp. 907-908
Author(s):  
R. Medenwaldt ◽  
J. Abraham ◽  
E. E.UggerhØj ◽  
F. Vollrath ◽  
E. SØgaard

X-ray microscopy with soft X-rays is well suited for investigations of aqueous samples of some microns thickness when the resolution is required to be better than in visible light microscopy an not better than 30 nm. Sample preparation is as simple as for light microscopy, i.e. no fixation or metal coating is needed.In Aarhus, an X-ray microscope is used for investigations in fields as biology, medicine and soil sciences. A ray diagram of the Aarhus X-ray microscope is shown in Fig.l. Synchrotron radiation at a wavelength of 2.4 nm from the Aarhus Storage Ring is focused by a condenser zone plate onto an object. Another zone plate as an objective behind the object forms the image on a CCD camera. Objects are located under atmospheric pressure. For dry samples, almost any kind of holder can be mounted in the microscope. Wet samples are placed between thin silicon foils in a sealed chamber. With typical liquid layer thickness of 5-15 µm, samples can be kept in the chamber for many hours without drying out.


The last few years have seen great advances in the instrumentation used to obtain X-ray spectra of the Sun. These new observations reveal a wealth of multiplet structure containing many lines which allow us to understand more of the nature of the coronal plasma. Three areas of interest are examined. (1) The temperature sensitive satellite lines to helium —like resonance lines. (2) The strong lines of neon —like iron, Fexvii. (3) The combination of high spectral and high spatial resolution (Skylab) observations.


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