scholarly journals In-Situ Low Energy Ion Milling with a FIB-SEM for TEM lift-out Sample Preparation of Copper Damascene Structures Fabricated with Low k porous SiLKTM Semiconductor Dielectric

2003 ◽  
Vol 9 (S02) ◽  
pp. 874-875
Author(s):  
E. R. Beach ◽  
S. J. Rozeveld ◽  
C. J. Wood ◽  
M. V. Moore ◽  
J. Waeterloos
2009 ◽  
Author(s):  
Heiko Stegmann ◽  
Yvonne Ritz ◽  
Dirk Utess ◽  
René Hübner ◽  
Ehrenfried Zschech ◽  
...  

2009 ◽  
Vol 15 (S2) ◽  
pp. 170-171 ◽  
Author(s):  
H Stegmann ◽  
Y Ritz ◽  
D Utess ◽  
H-J Engelmann ◽  
E Zschech
Keyword(s):  

Extended abstract of a paper presented at Microscopy and Microanalysis 2009 in Richmond, Virginia, USA, July 26 – July 30, 2009


2006 ◽  
Vol 26 ◽  
pp. 223-226 ◽  
Author(s):  
J Scott ◽  
F T Docherty ◽  
M MacKenzie ◽  
W Smith ◽  
B Miller ◽  
...  

2016 ◽  
Vol 850 ◽  
pp. 722-727 ◽  
Author(s):  
Hui Wang ◽  
Shang Gang Xiao ◽  
Qiang Xu ◽  
Tao Zhang ◽  
Henny Zandbergen

The preparation of thin lamellas by focused ion beam (FIB) for MEMS-based in situ TEM experiments is time consuming. Typically, the lamellas are of ~5μm*10μm and have a thickness less than 100nm. Here we demonstrate a fast lamellas’ preparation method using special fast cutting by FIB of samples prepared by conventional TEM sample preparation by argon ion milling or electrochemical polishing methods. This method has been applied successfully on various materials, such as ductile metallic alloy Ti68Ta27Al5, brittle ceramics K0.5Na0.5NbO3-6%LiNbO3 and semiconductor Si. The thickness of the lamellas depends on the original TEM sample.


Author(s):  
P. Nowakowski ◽  
M.L. Ray ◽  
P.E. Fischione

Abstract Conventional mechanical sample preparation is a difficult and uncontrolled process that does not allow targeting of a specific depth or layer. Because of the difficulties presented by mechanical sample preparation, there has been an emergence of beam-based techniques for device delayering applications. Cross-sectioning is another commonly used technique used in microelectronics industry investigations; when combined with delayering, one can gain complete knowledge about a device's faults. This paper presents a development in semiconductor device investigation using low energy, broad-beam argon ion milling. The results highlight that broad-beam Ar ion milling produces excellent surface quality, which allows high resolution scanning electron microscope observation and energy dispersive spectrometry analyses, even at low energy.


1998 ◽  
Vol 4 (S2) ◽  
pp. 862-863 ◽  
Author(s):  
B. Foran ◽  
F. Shaapur ◽  
V. Blaschke

Sample preparation for transmission electron microscopy (TEM) has been a source of speculation with regards to potential for the creation of artifacts which may confound data gleaned from TEM analysis. For semiconductor integrated circuit (IC) materials characterization, the most common sample preparatory methods are based on final thinning by ion beam milling. The latest shift towards Copper / low dielectric constant (k) composite systems in the semiconductor IC industry provides several challenges for TEM sample preparation resulting from differences in milling rates and materials properties for neighboring features.In conjunction with process development for integration of Cu / low-k materials, conducted at SEMATECH, we have systematically studied the effects of TEM sample preparation by ion milling in order to search for artifacts that could result from sample thinning procedures. For this purpose we have studied wafers with patterned copper lines isolated by a low-k polymer. One sample was stressed by thermal and electronic bias, while a second was subjected to only thermal stress.


2006 ◽  
Vol 12 (6) ◽  
pp. 545-548 ◽  
Author(s):  
Kazutaka Mitsuishi ◽  
Masayuki Shimojo ◽  
Miyoko Tanaka ◽  
Masaki Takeguchi ◽  
Minghui Song ◽  
...  

A new TEM sample preparation technique using electron-beam-induced deposition combined with low-energy ion milling was used to fabricate for two different shapes of sample, conical and plate. High-quality HREM images can be obtained from samples prepared by this technique. A desired sample position can be obtained with high accuracy, and the total sample preparation time can be much less than conventional techniques. Because the gas deposition system used can easily be integrated in a conventional SEM, the method can be performed in any laboratory equipped with a SEM and an ion milling machine.


2008 ◽  
Vol 14 (S2) ◽  
pp. 976-977 ◽  
Author(s):  
JR Michael ◽  
PG Kotula

Extended abstract of a paper presented at Microscopy and Microanalysis 2008 in Albuquerque, New Mexico, USA, August 3 – August 7, 2008


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