Enhanced TEM Sample Preparation Using In-situ Low Energy Argon Ion Milling

2009 ◽  
Author(s):  
Heiko Stegmann ◽  
Yvonne Ritz ◽  
Dirk Utess ◽  
René Hübner ◽  
Ehrenfried Zschech ◽  
...  
2009 ◽  
Vol 15 (S2) ◽  
pp. 170-171 ◽  
Author(s):  
H Stegmann ◽  
Y Ritz ◽  
D Utess ◽  
H-J Engelmann ◽  
E Zschech
Keyword(s):  

Extended abstract of a paper presented at Microscopy and Microanalysis 2009 in Richmond, Virginia, USA, July 26 – July 30, 2009


2016 ◽  
Vol 850 ◽  
pp. 722-727 ◽  
Author(s):  
Hui Wang ◽  
Shang Gang Xiao ◽  
Qiang Xu ◽  
Tao Zhang ◽  
Henny Zandbergen

The preparation of thin lamellas by focused ion beam (FIB) for MEMS-based in situ TEM experiments is time consuming. Typically, the lamellas are of ~5μm*10μm and have a thickness less than 100nm. Here we demonstrate a fast lamellas’ preparation method using special fast cutting by FIB of samples prepared by conventional TEM sample preparation by argon ion milling or electrochemical polishing methods. This method has been applied successfully on various materials, such as ductile metallic alloy Ti68Ta27Al5, brittle ceramics K0.5Na0.5NbO3-6%LiNbO3 and semiconductor Si. The thickness of the lamellas depends on the original TEM sample.


Author(s):  
P. Nowakowski ◽  
M.L. Ray ◽  
P.E. Fischione

Abstract Conventional mechanical sample preparation is a difficult and uncontrolled process that does not allow targeting of a specific depth or layer. Because of the difficulties presented by mechanical sample preparation, there has been an emergence of beam-based techniques for device delayering applications. Cross-sectioning is another commonly used technique used in microelectronics industry investigations; when combined with delayering, one can gain complete knowledge about a device's faults. This paper presents a development in semiconductor device investigation using low energy, broad-beam argon ion milling. The results highlight that broad-beam Ar ion milling produces excellent surface quality, which allows high resolution scanning electron microscope observation and energy dispersive spectrometry analyses, even at low energy.


2019 ◽  
Vol 25 (S2) ◽  
pp. 548-549
Author(s):  
Mikhail Dutka ◽  
Romaine Isaacs ◽  
Anna Prokhodtseva ◽  
Tomáš Vystavěl

2006 ◽  
Vol 26 ◽  
pp. 223-226 ◽  
Author(s):  
J Scott ◽  
F T Docherty ◽  
M MacKenzie ◽  
W Smith ◽  
B Miller ◽  
...  

2018 ◽  
Vol 24 (S1) ◽  
pp. 1060-1061
Author(s):  
Romaine Isaacs ◽  
Anna Prokhodtseva ◽  
Tomas Vystavel
Keyword(s):  

1997 ◽  
Vol 480 ◽  
Author(s):  
T. Kouzaki ◽  
K. Yoshioka ◽  
E. Ohno

AbstractIt is very difficult to prepare cross-sectional TEM samples for phase-change optical disks by conventional argon ion milling because of the difference of ion milling rates between multilayers and the polymer substrate. We have been successful in preparing samples of those optical disks by ion milling method with dissolution of the polymer substrate in advance. The cross-sectional structure was observed more clearly in this method rather than in ultramicrotome method.


2017 ◽  
Vol 23 (S1) ◽  
pp. 298-299 ◽  
Author(s):  
Anna Prokhodtseva ◽  
Johannes Mulders ◽  
Tomas Vystavel

Sign in / Sign up

Export Citation Format

Share Document