Study of LEAP® 5000 Deadtime and Precision via Silicon Pre-Sharpened-Microtip™ Standard Specimens

2021 ◽  
pp. 1-19
Author(s):  
Ty J. Prosa ◽  
Edward Oltman

Abstract Atom probe tomography (APT) is a technique that has expanded significantly in terms of adoption, dataset size, and quality during the past 15 years. The sophistication used to ensure ultimate analysis precision has not kept pace. The earliest APT datasets were small enough that deadtime and background considerations for processing mass spectrum peaks were secondary. Today, datasets can reach beyond a billion atoms so that high precision data processing procedures and corrections need to be considered to attain reliable accuracy at the parts-per-million level. This paper considers options for mass spectrum ranging, deadtime corrections, and error propagation as applied to an extrinsic-silicon standard specimen to attain agreement for silicon isotopic fraction measurements across multiple instruments, instrument types, and acquisition conditions. Precision consistent with those predicted by counting statistics is attained showing agreement in silicon isotope fraction measurements across multiple instruments, instrument platforms, and analysis conditions.

Radiocarbon ◽  
2020 ◽  
Vol 62 (4) ◽  
pp. 883-889 ◽  
Author(s):  
Frederick Reinig ◽  
Adam Sookdeo ◽  
Jan Esper ◽  
Michael Friedrich ◽  
Giulia Guidobaldi ◽  
...  

ABSTRACTAs the worldwide standard for radiocarbon (14C) dating over the past ca. 50,000 years, the International Calibration Curve (IntCal) is continuously improving towards higher resolution and replication. Tree-ring-based 14C measurements provide absolute dating throughout most of the Holocene, although high-precision data are limited for the Younger Dryas interval and farther back in time. Here, we describe the dendrochronological characteristics of 1448 new 14C dates, between ~11,950 and 13,160 cal BP, from 13 pines that were growing in Switzerland. Significantly enhancing the ongoing IntCal update (IntCal20), this Late Glacial (LG) compilation contains more annually precise 14C dates than any other contribution during any other period of time. Thus, our results now provide unique geochronological dating into the Younger Dryas, a pivotal period of climate and environmental change at the transition from LG into Early Holocene conditions.


Radiocarbon ◽  
2003 ◽  
Vol 45 (1) ◽  
pp. 75-80 ◽  
Author(s):  
Thomas P Guilderson ◽  
John R Southon ◽  
Thomas A Brown

Unleached aliquots of TIRI/FIRI turbidite were analyzed by accelerator mass spectronomy (AMS) over a timespan of 18 months. Individual analyses ranged from 18,090–18,245 yr BP with reported errors between 30–50 yr. The weighted average fraction modern (FM) of these 28 measurements is 0.10378 ± 0.00008 (which equates to 18,199 ± 8 yr BP) and the measurements show a 1 standard deviation scatter of 0.00044 (±35 yr). The fractional error of these results indicates reproducibility of individual measurements at the 4 (1σ) level, which is consistent with the quoted counting-statistics-based errors. Laboratories engaged in the determination of 14C results at reasonably high precision should consider taking advantage of the TIRI and FIRI sample materials in the role of process standards. Additional suites of high-precision data are necessary to refine the accuracy of these sample materials.


2021 ◽  
Vol 336 ◽  
pp. 04007
Author(s):  
Sen Yang ◽  
Zerun Li ◽  
Jinhui Wei ◽  
Zuocheng Xing

The data detector for future wireless system needs to achieve high throughput and low bit error rate (BER) with low computational complexity. In this paper, we propose a deep neural networks (DNNs) learning aided iterative detection algorithm. We first propose a convex optimization-based method for calculating the efficient detection of iterative soft output data, and then propose a method for adjusting the iteration parameters using the powerful data driven by DNNs, which achieves fast convergence and strong robustness. The results show that the proposed method can achieve the same performance as the known algorithm at a lower computation complexity cost.


2005 ◽  
Vol 14 (08) ◽  
pp. 1347-1364 ◽  
Author(s):  
XIULIAN WANG ◽  
BO FENG ◽  
MINGZHE LI ◽  
XUE-LEI CHEN ◽  
XINMIN ZHANG

In the "natural inflation" model, the inflaton potential is periodic. We show that Planck scale physics may induce corrections to the inflaton potential, which is also periodic with a greater frequency. Such high frequency corrections produce oscillating features in the primordial fluctuation power spectrum, which are not entirely excluded by the current observations and may be detectable in high precision data of cosmic microwave background (CMB) anisotropy and large scale structure (LSS) observations.


2020 ◽  
Vol 232 ◽  
pp. 03006
Author(s):  
M. A. Stoyer ◽  
A. P. Tonchev ◽  
J. A. Silano ◽  
M. E. Gooden ◽  
J. B. Wilhelmy ◽  
...  

Fission product yields (FPY) are one of the most fundamental quantities that can be measured for a fissioning nucleus and are important for basic and applied nuclear physics. Recent measurements using mono-energetic and pulsed neutron beams generated using Triangle Universities Nuclear Laboratory’s tandem accelerator and employing a dual fission chamber setup have produced self-consistent, high-precision data critical for testing fission models for the neutron-induced fission of 235,238U and 239Pu between neutron energies of 0.5 to 15.0 MeV. These data have elucidated a low-energy dependence of FPY for several fission products using irradiations of varying lengths and neutron energies. This paper will discuss new measurements just beginning utilizing a RApid Belt-driven Irradiated Target Transfer System (RABITTS) to measure shorterlived fission products and the time dependence of fission yields, expanding the measurements from cumulative towards independent fission yields. The uniqueness of these FPY data and the impact on the development of fission theory will be discussed.


1999 ◽  
Vol 5 (S2) ◽  
pp. 116-117
Author(s):  
T. F. Kelly ◽  
D. J. Larson ◽  
M. K. Miller ◽  
J. E. Flinn

A vanadium-bearing variant of 316 stainless steel that was rapid solidification processed (RSP) by gas atomization and hot extrusion of the powder (10:1 extrusion ratio at 900°C) has been studied previously by conventional atom probe field ion microscopy (APFIM). The mechanical properties of this steel were markedly improved by RSP and aging (600°C for 1000 hours). High nitrogen (0.45 at% (0.2 wt%)) and oxygen (0.16 at% (0.05 wt%)) contents were intentionally introduced by melting under 80% nitrogen/20% oxygen gas and atomizing in nitrogen gas. A nominal boron concentration of 0.04 at% (0.01 wt%)) is present as a tramp element. As a result, a large number density (˜ 2 × 1021 m-3) of 25 nm plate-like vanadium-rich nitrides precipitate during aging of the alloy and these precipitates contribute a major portion of the strengthening. Previous efforts to locate the oxygen in the structure using APFIM were inconclusive largely due to poor counting statistics.


2019 ◽  
Vol 625 ◽  
pp. A145
Author(s):  
Geza Kovacs

We investigate the optimization of dataset weighting in searching for the orbital period of transiting planets when high-precision space-based data with a single transit event are combined with (relatively) low-precision ground-based (wide-field) data. The optimization stems from the lack of multiple events in the high-precision data and the likely presence of such events in the low-precision data. With noise minimization, we combined two types of frequency spectra: (i) spectra that use two fixed transit parameters (moment of the center of the transit and duration of the event) derived from the space data alone; (ii) spectra that result from the traditional weighted box signal search with optimized transit parameters for each trial period. We used many mock signals to test the detection power of the method. Marginal or no detections in the ground-based data may lead to secure detections in the combined data with the above weighting. Depending on the coverage and quality of the ground-based data, transit depths of ~0.05% and periods up to ~100 days are accessible by the suggested optimum combination of the data.


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