A Procedure for the Simultaneous Quantitative Determination of Glycerol and Fatty Acid Contents of Fats and Oils.

1964 ◽  
Vol 36 (3) ◽  
pp. 587-590 ◽  
Author(s):  
M. E. Mason ◽  
M. E. Eager ◽  
G. R. Waller

Author(s):  
Hartmut Frank ◽  
Manfred Wiegand ◽  
Dietmar Thiel


1972 ◽  
Vol 55 (6) ◽  
pp. 1288-1293
Author(s):  
Eugene C Coleman ◽  
David Firestone

Abstract A simplified Halphen procedure was developed for the quantitative determination of cyclopropene fatty acids in fats and oils. Butanol, dimethyl sulfoxide (DMSO), and mixtures of butanol and DMSO were used as reaction media in a closed system. Higher sample absorbances were produced in butanol than in mixtures of butanol and DMSO. Butanol was superior to the other solvent systems for both quantitative and qualitative analyses. The lower limit of sensitivity for the tube-butanol system for quantitative and qualitative analyses was 18 and 15 μg cyclopropene fatty acids/g oil, respectively.



2003 ◽  
Vol 88 (6) ◽  
pp. 2552-2555 ◽  
Author(s):  
Veera Vihma ◽  
Aila Tiitinen ◽  
Olavi Ylikorkala ◽  
Matti J. Tikkanen


2008 ◽  
Vol 19 (8) ◽  
pp. 1475-1483 ◽  
Author(s):  
Maria Cristina Milinsk ◽  
Makoto Matsushita ◽  
Jesuí V. Visentainer ◽  
Cláudio C. de Oliveira ◽  
Nilson E. de Souza




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